2-环戊基环戊酮香料的制备与应用

以尼龙酸副产物2-亚环戊基环戊酮为原料，液体镍为催化剂，催化加氢制得了2-环戊基环戊酮。经元素分析、GCMS、IR、^1HNMR、^13C NMR检测，认为结构正确，色谱纯度大于99．9％。大鼠口服LD50雄性5381．5mg／kg，雌性5087．5mg／kg。具有留兰香样的香气，可用作食用和日用香料。     

LW15-252型SF_6断路器存在的问题和对策

国产SF6断路器已在电力系统中得到了广泛的应用,随着时间的推移,这种断路器存在的问题也逐渐地暴露出来。笔者介绍了LW15-252型SF6断路器在实际运用中存在的问题和采取的对策。     

Time dependent crystal-smectic transformation in perylene-containing polyimides

The crystalline conformations of perylene polyimides (PPIs), with alkyl spacers varying in length from C₃ to C₁₂ are discussed. Although modeling of single chains would suggest the possibility that those with odd number of CH₂ groups adopt a flat helical shape, X-ray diffraction suggests that the chains with odd and even spacers have the same conformation, due to the necessity to pack the perylene units. Upon annealing, the UV-vis absorption maximum red-shifts by about 10 nm, indicating enhanced π-stacking between the perylenes. Several changes in the spectra are seen with an increase in annealing time, at a given temperature. With an increase in annealing time, X-ray diffraction patterns show changes in the number of reflections, indicative of a crystal to mesogenic transition. The time required for this transition increases with a decrease in the spacer length, and annealing temperature, suggesting that the dynamics of this transition is very slow.     

Observer design for autonomous discrete-time nonlinear systems

We obtain a necessary and sufficient condition for a discrete-time nonlinear system to be locally state equivalent to the nonlinear observer form. The result looks similar to the continuous counterpart except for the fact that Ad-operation is utilized instead of ad-operation.     

PTA压力离心机转子的改造

介绍了PTA压力离心机的主要性能参数、工作原理、分离效果的影响因素。为了增大沉渣在过渡区及脱水区滞留的时问，同时为达到在过渡区及脱水区对沉渣加入纯净水进行再冲洗的目的，对螺旋送料转子、挡液环、进料管进行了改造。改造后，沉渣在脱水区的停留时间由0．44a增至0．72s，2．5～3t／h的冲洗水对脱水区的沉渣进行冲洗效果较好。产品中的杂质质量分数较改造前减少15％，产品优等品率提高到99％。     

绿色再生混凝土利用途径与评定思路

就再生混凝土骨料进行深入系统的研究 ,建立了一套与现行评价天然骨料标准相一致的评定方法 ,具有工程实际意义 ,为将来实际应用作好了基础理论研究     

土工合成材料在辽宁省水利工程中应用效益分析

截止2003年辽宁省水利工程中应用土工合成材料已达1450万多m^2，尤其在河道护岸、堤(坝)护坡、防渗工程上这种新型工程材料得到了广泛应用。结合辽宁省水利工程上应用的实际，对其效益进行了分析，分析结果表明：采用土工织物软体排护岸比传统柴排护岸节省投资35％～80％；堤坝护坡采用土工织物滤层比传统砂砾料滤层节省投资30％以上；土工膜防渗可比粘土防渗节省投资30％～50％。同时还取得了保护生态平衡、节省能源、促进化纤工业发展等十分显的社会效益。     

HACCP在保健食品西洋参口服液生产中的应用

保健食品行业GMP的实施有利HACCP的应用推广。本文应用HACCP于传统保健食品西洋参口服液生产过程中，将生产及加工过程中危害因素降最低限度，以确保产品的质量与安全。     

Total simulation model of the thermo-mechanical process in shape rolling of steel rods

The production of steel reinforcing bars for civil engineering is investigated by means of FEM-simulation. An integrated system for computing appropriate thermo-mechanical parameters of the rolling process is proposed. Generalized plane strain approach and coupled thermal-mechanical solution are applied. The microstructural model combines both the effect of the recrystallization mechanisms (static, dynamic and metadynamic) upon the austenite grain forming in hot rolling and that of phase transformation upon the final microstructure. The phases are created during interrupted below the temperature of martensite transition cooling. Thus a typical industrial process for thermo-mechanical strengthening of reinforcing bars, known as Tempcor-process is considered. Computational results are validated to experimental measured mechanical properties of the steel. By means of computer simulation the system can perform different solutions, giving the possibility to obtain a reasonable choice of different thermo-mechanical rolling conditions.