宽角扫描相控阵天线测量方法

提出了一种基于坐标变换技术的宽角扫描相控阵天线测量的新方法,用于解决常规平面近场测量方法难以对宽角扫描相控阵天线进行精确测量的问题.在对用于宽角扫描相控阵天线测量的坐标变换技术进行理论分析的基础上,采用计算机模拟对该测试方法进行了数值仿真,制作天线实物进行了试验验证.数值仿真结果和试验结果均表明,该方法用于宽角扫描相控阵天线的测试具有较高的准确性.     

多支化两亲聚合物合成及其原油乳化作用研究

通过自由基胶束共聚法制备了N-苄基-N-n-十六烷基丙烯酰胺/丙烯酰胺/丙烯酸钠三元共聚两亲聚合物-P(AM/BHAM/NaA),并优化了合成方案。该聚合物具有临界聚集浓度(CAC),当该两亲聚合物质量浓度高于700mg/L时,P(AM/BHAM/NaA)在水溶液中形成聚集体,并随着聚合物质量浓度的增加聚集体的流体力学半径增加,表观黏度也随之增加。P(AM/BHAM/NaA)具有良好的原油乳化能力,研究了不同质量浓度的两亲聚合物对原油乳化性能。结果表明,随着两亲聚合物质量浓度的升高,在水溶液中形成聚集体的体积增大,空间网络结构增大,乳化能力升高。     

马钢300 t 铁水预处理倾翻车液压系统优化

介绍了马钢四钢轧300t铁水预处理铁水车倾翻复位过程中经常出现液压缸卡阻故障,此故障不仅制约生产的正常运行,还易造成铁水罐外溢铁水的事故,通过对倾翻油缸缸口块进行重新优化,很好的解决了这一难题。     

A Novel Fluorescence Probe 9-（4-（1,2-diamine）benzeneN 1-phenyl）acridine for Nitric Oxide Determination

A novel fluorescent probe 9-(4-(1,2-diamine)benzene-N1-phenyl)acridine(DABPA) was synthesized for the detection of nitric oxide(NO) and characterized by IR, 1H-NMR and EI-MS spectroscopy. Based on a photoelectron transfer mechanism, the fl uorescence intensities of DABPA were investigated with the different concentrations of NO. Under the optimal experimental conditions, the fl uorescence intensity of DABPA had a good linear relationship(R2=0.9977) with NO concentration in the range from 1×10-7 to 1.5×10-6 mol/L with a detection limit of 1×10-8 mol/L. The cytotoxicity induced by DABPA was evaluated by the MTT(3-(4,5-dimethylthiazol-2-yl)-2,5diphenyl tetrazolium bromide) assay for biological application. Furthermore, the probe DABPA had also been successfully applied to real-time image NO produced in PC12 cells in the presence of L-arginine.     

基于吲哚类半花菁染料的钯比率荧光探针

利用6-羟基萘-2-醛和碘化N-乙基-2,3,3-三甲基-3H-吲哚啉季铵盐的缩合反应生成的羟基半花菁染料2与氯甲酸烯丙酯的反应合成了荧光比率型钯探针1.研究表明:在含水介质中,探针1对钯(Pd0和Pd2+)显示出很高的敏感性、选择性和抗干扰性,其荧光比率增强大约72倍,对Pd2+的最低检测极限为0.23μmol/L.探针1对钯的作用机理是钯催化碳酸烯丙酯断裂导致比率荧光变化.     

强碱三元复合驱结垢现象

采用现场举升系统结垢统计、室内铸体薄片,结合SEM和电子探针分析了强碱三元复合驱过程中垢成分的变化和储层结垢类型与形成机理。结果表明,垢的主要类型随着强碱三元复合驱体系注入PV数的增加发生变化,注入初期以碳酸盐垢为主并含有少量硅垢和有机物,注入中期3种垢成分含量相当,注入后期结垢类型转变为与初期相同类型。铸体薄片分析表明,垢形态为白色云雾状和褐色胶结状,部分孔隙阻塞造成孔隙结构发生变化,面孔隙率平均下降6.45%。研究区垢的类型主要为钙垢和硅垢,含有少量的钡/钛垢和铁垢。由于强碱的溶蚀作用,地层和井筒中容易出现结垢现象,建议在能够实现相同提高采收率幅度的前提下可以考虑采用弱碱三元复合驱。     

基于Halcon的IC测试探针表面质量的机器视觉检测系统

IC测试是集成电路生产中的重要工序,探针表面诸如划痕、凹坑等缺陷对性能测试结果影响大.文章研究了IC探针表面质量的机器视觉检测方法,讨论了灰度变换、均值滤波、区域连通、图像分割等缺陷图像处理和形状识别方法,建立了相应的探针表面质量检测系统,并基于机器视觉软件Halcon开发了探针表面质量检测系统软件.实验表明:开发的检测系统可对直径0.3~0.6 mm的IC测试探针表面质量进行快速检测评估,且系统的稳定性好、检测精度高,能有效缩短检测时间和减少检测成本.     

Behavior of Ni-Al particles in argon: Helium plasma jets

To better understand the plasma spray coating process, an experimental study of the interaction between a subsonic thermal plasma jet and injected nickel- aluminum particles was performed. The velocity, temperature, and composition of the argon/helium gas flow field was mapped using an enthalpy probe/mass spectrometer system. The sprayed particle flow field was examined by simultaneously measuring the size, velocity, and temperature of individual particles. Particle and gas temperatures were compared at the nominal substrate stand- off distance and axially along the median particle trajectory. Temperature and velocity differences between the particle and the gas surrounding it are shown to vary substantially depending on the trajectory of the particles. On the median trajectory, the average particle is transferring heat and momentum back to the plasma by the time it reaches the substrate. Because the exchange of heat and momentum is highly dependent on the particle residence time in the core of the plasma, the condition of particles at the substrate can be optimized by controlling the particle trajectory through the plasma.     

用Kelvin探头技术研究铝合金的大气腐蚀

选择航空工业广泛使用的铝、铝合金及其涂层的试样，利用自行研制的Kelvin探头大气腐蚀测定仪、扫描电镜等设备，研究了纯铝试样随温、湿度变化，其表面电位的变化规律，测定了铝合金及涂层试样大气曝晒试验和周浸试验前后的表面电位、形貌,对铝、铝合金以及涂层的腐蚀规律进行了初步的探讨.结果表明，纯铝试样表面无可见液膜时，腐蚀电位随相对湿度增加逐渐下降；表面有可见液膜时，随着液层蒸发逐渐减薄，电位逐渐正移.铝合金裸材在北京大气环境下电位变化较小，且各个位置的电位基本相同.带涂层的试样优先在缺陷处发生腐蚀，并不断向周围扩展，涂层的剥离面积不断增大.涂层的铝合金，划痕处在腐蚀发生的初期腐蚀电位向负方向变化很快，但是随着时间的延长，腐蚀电位变化的速率减慢，并有向正方向移动的趋势.      

Design of a six-axis high precision machine tool and its application in machining aspherical optical mirrors

The paper presents the design of a six-axis machining system and its application in fabricating large off-axis aspherical mirrors with sub-aperture lapping techniques. The new system is based on computer-controlled optical surfacing (CCOS), which combines the faculties of grinding, polishing, and on-machine profile measuring, has the features of conventional loose abrasive machining with the characteristics of a tool having multiple degrees of freedom moving in planar model. And a novel dual touch-trigger probe profiler is designed, which is composed of a probe, model METRO-MT60 made by HEIDENHAIN Co., is integrated into the system for measuring the shape accuracy of the tested aspherical surface, another probe modeled METRO-MT12 is designed as a calibrating device for minimizing the cosine error caused by assembly inaccuracy. The new CNC machining system with two kinds of moving coordinate systems, dual tool activities and on-machine measuring is presently developed based on the new concept. The general material removal function during machining is analyzed on the basis of the Preston hypothesis. Further, an alignment test of the measuring profiler is carried out using a leveling rule as a specimen. The accuracy of the optical surfaces measured by the dual probe profiler is found to be within 1 μm PV after removing cosine error and error compensating, achieves to the resolving power of the profiler is about 0.2–0.5 μm, so the developed system can be applied to the shape accuracy measuring of aspheric fabrication with micro precision during fine grinding process according to the calibrating results. Finally, the manufacturing experiments are carried out by virtue of an off-axis oblate ellipsoid mirror with rectangular aperture as 770 mm×210 mm and centered 127 mm. The accuracy of the aspherical mirror improved from the initial form error of 17.648 μm rms to the final one of 0.728 μm rms after grinding for 200 h.