Room temperature oxidation of lead-indium alloy films

The kinetics of growth of thin (14 to 40Å) oxide layers on lead-indium alloys was investigated ellipsometrically, using: 3000Å thick films at 23°C; and oxygen exposures at 760 torr for times ranging from five minutes to five days. Assuming that the oxide layer is comprised of a two-phase mixture of PbO and In₂O₃ having a negligible extinction coefficient made it possible to estimate the oxide composition from the ellipsometrically-obtained oxide refractive index. Under these oxidizing conditions, the volume fraction of PbO in the oxide mixture decreases from a value of unity for pure lead to zero for alloys containing more than 30 at. percent In, in agreement with the Auger Electron Spectroscopy results of Chou and coworkers. The oxidation rate equals a exp (X₁/X), where α and X₁ will be seen to vary complexly with alloy composition. A theoretical explanation of these results is also presented.     

合金钢中白点缺陷超声反射波辨析

通过对进口合金钢中白点缺陷超声反射波形的分析研究，为白点缺陷的判定提供借鉴，保证工程材料的使用安全。     

电炉还原熔炼氧化钴矿的生产实践

介绍了刚果(金)钴铜冶炼厂电炉还原熔炼处理钴铜氧化矿工艺的设计特点及生产实践。     

The Effects of Aging Precipitation on the Recrystallization of CuNiSiCr Alloy

The interaction between precipitation and recrystallization and its effect on the properties of the Cu-Ni-Si-Cr alloy during aging were discussed. The results show that the deformation results in much more dispersed precipitation of the phases. The precipitations have accelerating or retarding effects on the recrys allization. On the formation and growth of recrystallization, the precipitated phases are coarsed or dissolved in front of grain boundaries following a re-precipitation in the recrystallization area.     

GH4169合金的X射线荧光光谱分析

采用x射线荧光光谱仪测定GH4169合金中的锰、硅、镍、铬、钼、铝、钛、铌。研究了测量条件及基体 吸收—增强效应的校正。还时测量精度进行了研究,各元素的相对标准偏差分别为0．0466％～O．6777％。与 化学分析结果对照结果良好。     

选择溶解条件--ICP-AES法测定铝合金中10元素

在铝合金中,对常量、微量、痕量元素等的测量,传统上采用化学的方法来分析,手续繁杂,分析时间 亦长,有时不能满足大批量快速分析的要求。ICP-AES分析法,以其优异的分析性能被广泛应用于各种材料 的主要、次要,痕量、超痕量多元素的同时分析。但是,影响等离子炬状态的因素很多,只有在最佳工作状态下 操作,才能充分发挥ICP光源的优越性。     

电热还原高铝粉煤灰制取Fe-Al-Si合金的试验研究

使用碳管电阻炉在1950～2200℃温度范围内，用焦炭粉还原高铝粉煤灰，制取Fe-Al-Si合金。试验结果表明：只有当还原温度高于2050℃时，高铝粉煤灰中的Al2O3才能显著地还原；Al和Si的收得率皆随还原温度升高而增高；在一定高铝粉煤灰和配Fe量的条件下，还原制取的Fe-Al-Si合金中的Al、Si含量均随还原温度升高而增高；在一定还原温度条件下，还原制取的Fe-Al-Si合金中的Al含量随高铝粉煤灰中的Al2O3含量的增高而增高，Si含量随高铝粉煤灰中的Al2O3含量增高（SiO2含量降低）而降低。     

Strain rate sensitivity of the commercial aluminum alloy AA5182-O

The mechanical behavior of the commercial aluminum alloy AA5182-O is investigated at temperatures ranging from −120 to 150 °C and strain rates from 10⁻⁶ to 10⁻¹ s⁻¹. The strain rate sensitivity parameter is determined as a function of temperature and plastic strain, and the strain rate and temperature range in which dynamic strain aging leads to negative strain rate sensitivity is mapped. The effect of dynamic strain aging on ductility and strain hardening is investigated. The sensitivity of the measured quantities to the experimental method employed and their dependence on grain shape are discussed. The experimental data are compared with the predictions of a model constructed based on a recently proposed mechanism for dynamic strain ageing. The mechanism is based on the effect solute clustering at forest dislocations has on the strength of dislocation junctions. The model is shown to reproduce qualitatively the experimental trends.     

添加Al2O3和SiO2的大晶粒UO2芯块制备研究

研究了Al2O3和SiO2添加剂对UO2芯块晶粒尺寸的影响.结果表明:加入少量的Al2O3和SiO2,可有效促进烧结过程中UO2芯块的晶粒度长大,过量加入则会阻碍烧结过程中UO2芯块的致密化;在添加量一定的情况下,添加不同比例的Al2O3和SiO2,对芯块晶粒尺寸有较大影响,只添加SiO2,对芯块晶粒尺寸影响不大,Al2O3添加量增加,芯块晶粒尺寸随之增加;添加Al2O3和SiO2促进UO2芯块晶粒长大的机制是在烧结期间发生了液相烧结.