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61.
The bonding of β'-Al2O3 and pyrex glass to Al matrix composites by anodic bonding process is achieved. The microstructure of the bonded interface and the joining mechanisms are analyzed with scanning electron microscope (SEM), energy dispersive X-ray fluorescence spectrometer (EDX). It is observed that the bonding region across the interface consists of the metal layer, oxide transitional layer and the ceramic layer, with the transitional layer composed of surface region and sub-surface region. The bonding process can mainly be categorized into anodic bonding process and solid state diffusing process. The pile-up of the ions and its drift in the interface area are the main reasons for anode oxidation and joining of the interface. The temperature, voltage and the drift ions in the ceramic or glass during the bonding process are the essential conditions to solid state diffusing and oxide bonding at the interface. The voltages, temperature, pressure as well as the surface state are the main factors that influence the anodic bonding. 相似文献
62.
Poly[2‐methoxy‐5‐(2′‐ethyl‐hexyloxy)‐para‐phenylene vinylene] (MEH‐PPV)/silica nanoparticle hybrid films were prepared and characterised. Three kinds of materials were compared: parent MEH‐PPV, MEH‐PPV/silica (hybrid A films), and MEH‐PPV/coupling agent MSMA/silica (hybrid B films), in which MSMA is 3‐(trimethoxysilyl) propyl methacrylate. It was found that the hybrid B films could significantly prevent macrophase separation, as evidenced by scanning electron and fluorescence microscopy. Furthermore, the thermal characteristics of the hybrid films were largely improved in comparison with the parent MEH‐PPV. The UV‐visible absorption spectra suggested that the incorporation of MSMA‐modified silica into MEH‐PPV could confine the polymer chain between nanoparticles and thus increase the conjugation length. The photoluminescence (PL) studies also indicated enhancement of the PL intensity and quantum efficiency by incorporating just 2 wt% of MSMA‐modified silica into MEH‐PPV. However, hybrid A films did not show such enhancement of optoelectronic properties as the hybrid B films. The present study suggests the importance of the interface between the luminescent organic polymers and the inorganic silica on morphology and optoelectronic properties. Copyright © 2004 Society of Chemical Industry 相似文献
63.
Colour Centres and Energy Transfer in BaF2-xClx:Eu2+ Phosphors 总被引:1,自引:1,他引:0
The optical absorption spectra of BaF2-xClx:Eu2 after ultraviolet (UV) light excitation were investigated.The differences between the absorption spectra after and before excitation (DAS) were observed.The DAS increase at both the high and the low energy side of F band in BaF2-xClx:Eu2 after 245 nm UV light excitation.The bleach effect of UV light and the absorption of electrons in the valence band may account for the former and the formation of Fa centres (association of F(Cl-) centres), whose absorption band matches the HeNe laser better, may explain the latter.In the write-in process, the transfer of electrons is via tunneling.In the readout process, the transfer of electrons captured in F(F-) and Fa centres is more likely via tunneling, and that of F(Cl-) centres is more likely via conduction band. 相似文献
64.
孙耀华 《石油地球物理勘探》2003,38(1):17-21
地震勘探技术应用可以分为以二维地震研究构造为主的地震勘探初级阶段、以地震地层学为主的地震勘探中级阶段、以三维地震油藏静态描述为主的地震勘探高级阶段、以地震储层研究为主的开发地震妆级阶段和以四维地震进行油藏监测为主的开发地震高级阶段。针对5个不同阶段的地质条件和地质任务,选择使用合理的地震勘探技术是有效提高勘探开发效益的重要途径。焉耆盆地的勘探开发体现了以地震勘探为主的思路,在勘探开发过程中重视了针对不同勘探开发阶段和不同的地质 地震技术,因此,在早期勘探开发中取得了很好的经济效益。 相似文献
65.
用化学还原法合成了FeBP非晶态合金超细微粒,用电感耦合等离子体光谱(ICP)、X射线粉末衍射(XRD)、透射电子显微镜(TEM)和差热分析(DSC)等手段对其进行了物性表征,并用微型催化反应装置考察了其对PH3分解的催化作用,结果表明,非晶态合金FeBP对PH3的分解具有良好的催化作用,能使PH3的分解温度从800℃以上降到500℃左右。490℃时分解率超过90%,540℃时达100%。 相似文献
66.
LB11820M是日本SANYO(三洋)公司开发的三相直流无刷电机驱动芯片。它具备开环三相电机控制所需的全部有效功能,并且具有比较完善的保护电路。文中介绍了LB11820M的特点、功能和工作原理,给出了其典型应用电路。 相似文献
67.
O. Khamman 《Materials Letters》2007,61(3):639-643
The solid-state mixed oxide method via a rapid vibro-milling technique is explored in the preparation of single-phase nickel niobate (NiNb2O6) powders. The formation of the NiNb2O6 phase in the calcined powders has been investigated as a function of calcination conditions by TG-DTA and XRD techniques. Morphology, particle size and chemical composition have been determined via a combination of SEM and EDX techniques. It has been found that the minor phases of unreacted NiO and Nb2O5 precursors and the Ni4Nb2O9 phase tend to form together with the columbite NiNb2O6 phase, depending on calcination conditions. More importantly, it is seen that optimization of calcination conditions can lead to a single-phase NiNb2O6 in an orthorhombic phase. 相似文献
68.
2-环戊基环戊酮香料的制备与应用 总被引:2,自引:0,他引:2
以尼龙酸副产物2-亚环戊基环戊酮为原料,液体镍为催化剂,催化加氢制得了2-环戊基环戊酮。经元素分析、GCMS、IR、^1HNMR、^13C NMR检测,认为结构正确,色谱纯度大于99.9%。大鼠口服LD50雄性5381.5mg/kg,雌性5087.5mg/kg。具有留兰香样的香气,可用作食用和日用香料。 相似文献
69.
The switchable optical properties of Pd-protected RCo2-type Ho0.6Mm0.4Co2 alloy thin films have been investigated in a KOH electrolyte. The reversible optical switching has been carried out simultaneously by measuring transmitted light through the thin film during electrochemical charging–discharging of hydrogen. The dependence of switching speed and cyclic durability of the film on the charging and discharging current density as well as concentration of KOH electrolyte has been studied. In addition, cyclic voltammetric measurements have been performed to examine the hydride formation and decomposition reactions. 相似文献
70.
Takayuki Honma Yuichiro Kuroki Tomoichiro Okamoto Masasuke Takata Yukihiro Kanechika Masanobu Azuma Hitofumi Taniguchi 《Ceramics International》2008,34(4):943-946
Aluminum nitride ceramics were prepared by sintering with 0–4.8 mass% of Ca3Al2O6 (C3A) as a sintering additive. The transmittance in the range of 260–550 nm increased with increasing amount of C3A. The cathodoluminescence intensity attributed to oxygen-induced defects decreased with increasing amount of C3A. From the results, the increase of the transmittance in the range of 260–550 nm was considered to be related to the decrease of the oxygen-induced defect density. 相似文献