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121.
122.
Hamid Javaherian Naghash Ahmad Reza Momeni Hamid Alian Ahmad Reza Massah Shahla Ataie 《Polymer International》2005,54(11):1564-1571
Poly(methyl methacrylate) (PMMA) gels with varying amounts of silicone and solvent and constant amounts of crosslinker were prepared by solution free radical crosslinking copolymerization of methyl methacrylate (MMA), ethylene glycol dimethacrylate (EGDM), tetraethoxysilane (TEOS) and vinyltriethoxysilane (VTES) comonomer systems. They were then studied in benzene at a total monomer concentration of 3.5 mol L?1 and 70 °C. The conversion of monomer, volume swelling ratio, weight fraction and gel point were measured as a function of the reaction time, silicone concentration and benzene content up to the onset of macrogelation. Structural characteristics of the gels were examined by using equilibrium swelling in benzene, gel fraction and Fourier‐transform infrared (FTIR) analysis. The morphology of the copolymers was also investigated by SEM. Based on the obtained results, it was concluded that the FTIR data did not have the capacity to show the presence of the VTES or TEOS moiety in these kinds of copolymers. On the other hand, the variation of weight fraction of gel, Wg, and its equilibrium volume swelling ratio in benzene, qv, exhibited the same behaviour as that of MMA/EGDM copolymers. Also, the dilution of the monomer mixture resulted in an increase in the gel point and swelling degree and a decrease in the percent of conversion and gel fraction. Finally, TEOS is not an ideal silicone compound for reaction in the MMA/EGDM copolymerization system, whereas VTES is a suitable silicone comonomer for this system and it has been proved useful. Copyright © 2005 Society of Chemical Industry 相似文献
123.
An investigation of crack closure and the propagation of semi-elliptical fatigue cracks in Q1N (HY80) pressure vessel steel 总被引:1,自引:0,他引:1
The results of an experimental investigation of the effect of crack closure on the propagation of semi-elliptical fatigue cracks are presented. Load-shedding fatigue threshold tests were carried out at stress ratios of 0.2, 0.35, 0.5 and 0.7. Crack closure was measured at the surface and depth positions using backface strain gauges, near-tip gauges, and a clip gauge. Differences between the surface and depth growth behaviour are explained by considerations of the effects of the transition from plane stress conditions at the surface to plane strain conditions at the depth. The effects of stress ratios are attributed largely to differences in the crack opening displacement, which result in asperities coming into contact to induce roughness-induced crack closure. 相似文献
124.
To investigate the change in the manner of plastic deformation at a fatigue crack tip under different loading conditions, the fresh surface area which is produced in one fatigue cycle at the crack tip was measured by an electrochemical method under various load ratios. The fresh surface area produced in each fatigue cycle is in proportion to the crack propagation rate in the Paris regime. This indicates that the crack tip geometry at Kmax maintains a similar profile through the Paris regime. Furthermore, the fresh surface area is independent of load ratio at a given da/dN in the Paris regime. This suggests that the shape of the fatigue crack tip at Kmax should be independent of load ratio at a given da/dN, and that the shape at Kmin is also independent of load ratio, whereas the size of the deformed region at the crack tip is in proportion to da/dN. 相似文献
125.
126.
钢筋混凝土框架梁截面的优化确定 总被引:1,自引:0,他引:1
以梁的配筋和截面有效高度为优化设计变量 ,导出了 RC框架梁的优化配筋率和优化设计高度 ,并给出了各种荷载作用下 ,不同设防烈度和场地类别条件下的截面优化设计高度表达式 ,为设计人员提供了方便 . 相似文献
127.
128.
岩屑泊松比实验测定仪 总被引:1,自引:0,他引:1
针对目前地层泊松比测定方法的局限 ,提出了利用上返岩屑压实测定地层泊松比的设想 ,并研制出岩屑泊松比实验测定仪。某油田已有的压实岩屑泊松比与实际声波测井资料计算泊松比对比发现 ,运用岩屑泊松比实验测定仪所得的实验结果与原始地层的泊松比有很好的一致性(两者的误差在± 5 %之间 )。利用该测定仪 ,可实现对钻井过程中上返岩屑的连续快速测定 ,大大降低工程取心所增加的钻井成本 ,还可为钻井施工在第一时间提供相关的地层信息 相似文献
129.
130.
钢纤维聚合物混凝土抗压本构关系 总被引:2,自引:0,他引:2
钢纤维聚合物混凝土是由聚合物混凝土基体和钢纤维共同组成的纤维增强复合材料,它的力学行为不仅依赖于聚合物混凝土基体的行为,而且与钢纤维的掺量、分散特征以及钢纤维的几何尺寸有关,本文将基于损伤力学原理研究在不同纤维掺量下的钢纤维聚合物混凝土的全程压力-应变曲线及其本构模型。 相似文献