微膨胀钢管混凝土双肢柱试验研究与数值模拟

通过试验研究与数值模拟的方法,确定微膨胀C50圆端形钢管混凝土的应力应变关系,并结合工程实例,用泊松比的变化来模拟核心混凝土的微膨胀效应,分析施工中圆端形钢管混凝土双肢柱在轴心受压和偏心受压两种情形下的受力性能.分析结果表明,在考虑混凝土泊松比变化情况下,极限承载力比不考虑混凝土泊松比变化时的计算值高;这种结构在轴心受压时,应力变化很小;在承受偏心荷载时,应力增幅较大,且能充分利用其结构形式上的特点.     

钢管混凝土梁柱节点受力性能有限元分析

采用大型有限元分析软件ANSYS,对深圳福田大型地下车站主体结构标准段的钢管混凝土柱顶-横纵梁、柱脚-底纵梁以及柱-地下1层梁等节点在梁端及柱端的弯矩、剪力和轴力等荷载作用下的力学性能进行模拟和分析.从钢管混凝土梁柱节点的受力状态出发,分析在梁端及柱端的弯矩、轴力和剪力等荷载作用下节点模型各组成构件(包括柱钢管、梁、加强环梁、承台、抗拔桩等部位)的主应力及切应力分布情况、变形情况和各个截面的内力分布情况等,与各个构件所对应的设计强度值进行对比分析,根据分析结果建议了更合理的节点结构设计与加固方案.     

同一强度等级不同统计参数混凝土制成短柱的可靠性分析

同一强度等级的混凝土可能有不同的概率统计参数,对于都服从正态分布、fcu,k相同、σcu不同的两组同一强度等级的混凝土制成的短柱,采用均值一次二阶矩法进行了可靠性计算分析,得出σcu小的可靠度大,σcu大的可靠度小.     

黄瓜中溴离子的离子色谱法测定

在优化前处理方法的基础上,研究了以水为提取溶剂,SAX-SPE柱净化,AS 9-HC柱分离,电导检测器测定黄瓜中溴离子含量的离子色谱分析方法。Br-标准溶液浓度0.5~300 mg.L-1,标准曲线方程为Y=-306 756+2 639 978X,r=0.998 4,方法的最低检出浓度为0.2 mg.kg-1。样品(低于方法最低检出浓度)添加1,100 mg.kg-1Br-的平均回收率分别为98.6%,90.6%;相对标准偏差为13.47%,9.67%,准确度和精密度符合要求。测定的青岛5个菜市场黄瓜样品中溴离子浓度均低于方法的最低检出浓度。     

钢筋混凝土柱-H型钢斜梁结构有限元分析

钢筋混凝土柱-H型钢斜梁结构由混凝土和钢两种性能差异较大的材料构成,其受力性能相对复杂.针对大部分设计人员采用PKPM进行该结构设计的现状,笔者将ANSYS考虑大变形、非线性的计算结果引入.分析表明,因PKPM未考虑非线性等因素,故导致相同条件下水平推力和水平位移的计算结果存在较大偏差.     

梁削弱式节点连接的侧移钢框架柱计算长度系数

根据框架柱计算长度理论,通过引入梁削弱式节点参数特性,建立了四跨三层的梁削弱式节点连接的侧移钢框架数值模型.利用ANSYS软件对梁削弱式节点连接的侧移钢框架数值模型进行了非线性屈曲分析,得到了梁削弱式节点连接的侧移钢框架柱计算长度系数.结果显示,梁削弱式节点侧移钢框架柱计算长度系数较常规节点增加1.5%～12.9%.最后,经过回归得到了梁削弱式节点连接的侧移钢框架柱计算长度系数建议公式.     

二醇柱高效液相色谱法测定人参提取液中的人参皂苷

采用二醇柱,在等度洗脱条件下,建立了高效液相色谱(HPLC)定量分析人参提取液中人参皂苷的检测方法.优化的色谱条件:LiChrospher100 Diol柱(250 mm x2 mm i.d.,5μm),流动相为乙腈-水(体积比为82∶18),流速为1.0 L.min-1,检测波长为200 nm,柱温为15℃.研究结果表明:在较低温度下,采用二醇柱分析7种主要人参皂苷,具有分析速度快,不需要梯度洗脱程序,方法简单等优点.     

全回流-全馏出与变塔压联合的间歇精馏过程

A novel operation of batch distillation-combination of varying colum pressure and total reflux-total efflux is studied experimentally. In the operation, the product is accumulated at the top of the column under total reflux and then drained off completely, and the column pressure is varying in the whole process. This process has been industrialized successfully with large profits. The conventional mode of batch distillation is improved by this method effectively: the separation eficiency and the yield of product are increased greatly, the operation time is shortened and the production cost is cut down. Moreover, the amount of condensation water is decreased and the over-high reboiler temperature is lowered.     

HYDRODYNAMIC STUDIES IN FISCHER-TROPSCH DERIVED WAXES IN A BUBBLE COLUMN

Gas hold-up and Sauter mean bubble diameter measurements were made in a 0.051 m diameter by 3 m long glass bubble column in the system, nitrogen-molten wax, with three different waxes (paraffin wax FT-300, Sasol's Arge wax and Mobil's reactor wax). Paraffin wax has a tendency to foam and gas hold-up is a strong function of gas distributor type, temperature and start-up procedure, whereas the reactor waxes do not foam and are much less affected by these variables, In experiments at 265°C with a 1.85 mm single hole orifice plate distributor the gas hold-ups were nearly the same for all three waxes. However, significant differences in Sauter mean bubble diameters were obtained in experiments with different waxes; FT-300 wax produced the smallest Sauter mean bubble diameters whereas Mobil's reactor wax produced the largest bubbles. Addition of 1-octadecanol and octadecanoic acid (up to 10wt%) to the FT-300 paraffin wax caused an increase in gas hold-up and a delay in the foam break-up in runs at 265°C with the 1.85 mm orifice plate distributor.     

Prediction of dispersed phase holdup in a modified multi‐stage bubble column scrubber

This paper reports on the experimental investigation carried out to evaluate fractional dispersed phase holdup for a gas‐liquid mixture in a modified multi‐stage bubble column (with contraction and expansion disks), which has been conceived, designed and fabricated as a wet scrubber for control of air pollution; in addition it has versatile use as a gas‐liquid contactor in chemical process industries. A correlation developed for predicting fractional dispersed phase holdup has been found to be encouraging and highly significant from statistical analysis.