大电流监测信号提取的光收发及信号处理

近年来,大电流的监测成了人们十分关心的问题,这是由于大电流有强磁、高压、电流大等一系列的直接监测所不能克服的问题。这就需要把高压大电流的强电信号,经过提取后变成能在实验室中直接观测的弱电信号。为此,如何从高压大电流的信号中提取出随实时信号变化而实时变化的小信号就变成了一个关键问题。详细介绍了监测信号提取的光收发电路原理和后续信号处理电路,分析了各部分的作用,给出了必要的分析结果。     

聚合物-蒙脱石纳米复合材料的制备、结构与性能

从结构与性能的观点出发,将聚合物-蒙脱石纳米复合材料划分为插层型、层离型和混合型(插层型+层离型),探讨了影响蒙脱石纳米化的因素,提出了蒙脱石纳米化中值得注意的几个问题.     

Thermophysical Properties of Binary Mixtures of Methyl Methacrylate+Di-Ethers (Ethyl, Isopropyl, and Butyl) at 298.15 and 308.15 K

Experimental data for the densities, dynamic viscosities, sound speeds, and relative permittivities and for three binary systems of methyl methacrylate (MMA)+di-ethers (ethyl, isopropyl, and butyl) at 298.15 and 308.15 K and at atmospheric pressure are reported. The mixture viscosities are correlated by Grunberg–Nissan, McAllister, and Auslander equations over the complete composition range. The sound speeds for the mixtures are also calculated by using free length and collision factor theories, and Nomoto and Junjie equations. From the measured primary properties, deviation functions such as deviations in viscosities, sound speeds, relative permittivities, molar polarizations, excess isentropic compressibilities, and molar electrical susceptibilities were calculated, and the compositional dependence of each of the functions was expressed with a Redlich–Kister type equation. The variation of the Kirkwood correlation factor was determined over the complete composition range.     

Nonlinear coupled problems in dynamics of shells

The coupled system of three partial differential equations governing a flexible shallow shell dynamics is analysed. No any prior assumptions about the temperature distribution through the shell thickness are applied. The efficiency of the method used here when applied to the solution of integral-differential equations with different dimensions (three-dimensional equations related to the Kirchhoff-Love model) and of different type (heat transfer equations and the hyperbolic equations of shell theory) is demonstrated. Many computational results are reported and discussed.     

圆管流动的二次转捩

利用直接数值模拟方法求解N-S方程来研究空间发展的圆管转捩,计算中雷诺数Re选定为3000。在局部壁面引入的周期性吹吸(PSB)扰动作用下,圆管中首先出现了塞流结构,并向下游迁移,同时有稳定的流向条带结构形成;在塞流结构离开计算域后,随着扰动的不断发展,流向条带结构逐渐破裂失稳,圆管流动出现了第二次转捩,这是一种新的转捩形式,我们称之为“二次转捩”。     

优化锰铁高炉配矿结构

介绍了通过优化高炉锰铁烧结矿原料结构，改善了烧结矿性能，使锰铁冶炼取得了增产、节焦、降成本的明显效果。     

工业化陶瓷超滤膜的表征

以液-液排除法测定工业化陶瓷超滤膜的孔径及孔径分布，比较了两种渗透体系对测定结果的影响；用已知分子量标准物质考察了不同膜的截留行为，获得了各膜的切割分子量值，并分析了截留率与孔径的对应关系，为工业化陶瓷膜的开发提供依据。     

Catalyst instabilities during the liquid phase partial oxidation of methane

A promising catalytic system for the low temperature oxidation of methane to a methanol derivative has been investigated under both batch and semi-continuous operation in two different reactor types. The system comprises of a bimetallic palladium and copper(II) chloride catalyst contained in a trifluoroacetic acid (TFA) and an aqueous phase. Methane, oxygen and a co-reductant carbon monoxide constitute the gas phase. Typical operating conditions were a temperature of 85 °C and a pressure of 83 bar.

The yields of the methyl trifluoroacetate product observed in this present work were less than those obtained in other batch autoclave works, which employed only 4 ml of liquid phase, compared with 50 ml in this study. Furthermore, an encouraging initial product formation rate of ca. 40 mol/m³ h, quickly decreased after the first hour, and came to an apparent end after only 2 h. This observation had not been reported previously.

Work performed in a semi-continuous porous tube reactor (300 ml of re-circulating liquid phase) also showed the same reaction characteristics as in the batch reactor. Thus, the deteriorating product formation rate cannot be attributed to gaseous reactant depletion (batch operation). The results suggest problems associated with catalyst instabilities, e.g. with the previously elucidated Wacker chemistry.     

多模复合制导数据融合器性能评估系统方案设计

从构建多模复合制导数据融合器性能评估系统的需求出发，详细介绍了多模复合制导数据融合器性能评估系统的构建方案，并从软硬件两个方面介绍了构建这样一个系统所需要注意的问题和解决办法．     

原料酸卸车系统技术改进分析

分析了酸卸车系统存在的泵与管路的匹配、鹤管真空损失、酸腐蚀等技术问题，提出了鹤管的改进、卸车泵更新、真空系统水封、管路系统改进等保证真空能力的具体措施，实现了全自动、密闭卸车作业，最大限度地满足安全、快卸、底料少的要求。