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51.
Anthraquinone [1, 2-C] methylisoxazole is synthesized from 2-ethylanthraquinone through nitration and treating with oleum. The different methods of 2-ethylanthraquinone nitrated were discussed. The optimum conditions were determined. The structure of the product was confirmed by MS and 1H NMR. 相似文献
52.
Solid-liquid phase equilibria of the benzene + 2-methyl-2-propanol system have been investigated at temperatures from 278 to 323 K and pressures up to 300 MPa using a high-pressure optical vessel. The uncertainties of the measurements of temperature, pressure and composition are within ±0.1 K, ±0.5 MPa, and ±0.001 mole fraction, respectively. The freezing pressure at a constant composition increases monotonously with pressure. The eutectic point shifts to a higher temperature and benzene-rich composition with increasing pressure. In order to describe the pressure-temperature-composition relation of high-pressure solid-liquid phase equilibria, a new simple equation has been proposed as follows:
相似文献
53.
Discusses retouching of the Kallikak family photographs in H. H. Goddard's (1912) study of mental retardation and heredity, with reference to analyses by R. E. Fancher (see record 1987-31600-001) and S. J. Gould (1981), and concurs with Fancher that the retouching was probably not done for deceitful purposes. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
54.
55.
研究了一种制造低电电压氧化锌压敏电阻器的方法。在基本成分的基础上适当加入二氧化钛可降低梯度电压(V1mA/mm),适量掺硼和改进热处理工艺可减小元件的漏电流和提高其稳定性。 相似文献
56.
1 INTRODUCTIONTheorthorhombicalloysareofgreattech nolog icalinterestinhightemperatureapplicationssincetheyhaveagoodbalanceamongst 相似文献
57.
用呋喃树脂石英砂工艺生产牵引电机换向器套筒出现变形、裂纹等铸造缺陷,是由石英砂相变膨胀引起,后用高铬刚玉砂代替石英砂得到解决. 相似文献
58.
Highly conductive transparent aluminium-doped ZnO (ZnO:A1) films were successfully deposited by CW-CO2 laser-induced evaporation. Optimisation of evaporation parameters was based on laser power, substrate temperature, O2 partial pressure in the vacuum chamber and amount of Al in the ZnO source pellet. ZnO:A1 films with an electrical resistivity as low as 6.6 × 10−2Ω·cm and an optical transmission of 80% at 500nm were obtained at laser power of 15 W, substrate temperature of about 200°C, O2 partial pressure of 6—7 × 10−4 Torr and 5wt.% Al. Conductivity of ZnO films can be increased one order via Al-doping in ZnO films. The films obtained by laser-induced evaporation have compared quite favorably with the high quality films obtained by sputtering. 相似文献
59.
针对铝电解原材料中AlF3与Al2O3自动配料不准和难于观察及控制的现象,我厂开发应用了AlF3贮仓料位计,并与微机网络相连,实现了远程测量与在线监控,使AlF3配料更准确更均匀,电解质分子比更稳定,电解槽生产低耗高效。 相似文献
60.
In this paper, the author dipped surface vapor oxidized H13 steel specimens into 700℃ molten aluminum liquid for a certain period of time. Analyze the intermetallic phases formed on the H13 samples surface with optical microscope and X-ray diffraction method. The observation of immersion test sample's cross-section shows that Fe3O4 film will protect die substrate from molten aluminum erosion. The identification of the intermetallic phases reveals that they consist of 2parts, which is named as the composite layer and the compact layer. Further investigations are made in order to know the phase constituents of the 2 layers, they are Al8Fe2Si (outer composite layer), (AlCuMg) and Al5Fe2 (compact layer),respectively. The experimental results show that on the same specimen, a convex surface with bigger radius of curvature is more likely to be molten and the melting loss speed is also faster than a flat and smooth surface. The thickness of compact layer on a smooth surface is much bigger than that of the convex surface. Therefore, the author supposes the compact layer is favorable in stabilizing the die surface material from further melting loss, as their formation on the die surface, the melting loss speed will decrease. 相似文献
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