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71.
72.
Helen L. Ngo Alberto Nuñez Wenbin Lin Thomas A. Foglia 《European Journal of Lipid Science and Technology》2007,109(3):214-224
Branched‐chain (bc) saturated fatty acids (SFA) have potential as oleochemical intermediates since they have better oxidative stability than linear unsaturated fatty acids (UFA) and have better low‐temperature properties than linear SFA. Previous studies in converting UFA to bc‐FA using clay catalysts have resulted in only modest yields and conversions. Recent reports, however, have suggested that certain zeolites can be effective catalysts for converting UFA to bc‐FA in higher yields and conversions. In this work, we examined the scope and potential of the zeolite‐catalyzed synthesis of bc‐FA starting from readily available monounsaturated linear FA. Our results show that common UFA such as oleic acid can be converted to bc‐isomers using modified Ferrierite zeolite catalysts with high conversions (98%) and high selectivity (85%) and that the zeolite catalysts are reusable for at least three cycles. The positions of branching (methyl) on the FA chain were determined from the GC‐MS spectra of the picolinyl esters of the bc‐FA. 相似文献
73.
We have observed, for the first time, that when the initial chain conformation changed from coil to globule, the association of linear poly(N-vinylcaprolactam-co-sodium acrylate) chains could gradually change from a reaction limited to diffusion limited process, reflected in a change of the fractal dimension of the resultant aggregates from ∼2.5 to ∼1.6. Such an influence of the initial chain conformation has been overlooked in past studies of the formation of the mesoglobule phase in a dilute heteropolymer solution. 相似文献
74.
Radical copolymerization is considered theoretically taking into account the effect of complexing on the configurational statistics of macromolecules formed. Akinetic model has been developed that considers, apart from the ordinary addition of single monomer units to a propagating chain, the possible addition of monomer unit pairs along with a complexing agent in the form of a ternary complex. Within the framework of this model, the problem of calculating the probabilities of formation of any sequences of monomer units (taking into account their microtacticity) in a macromolecule has been rigorously solved as well as the problem of finding the composition distribution of the copolymer formed. It has been shown that this distribution is described by a conventional Gauss law and the appropriate parameters are given. Possible generalizations of the suggested approach are indicated. 相似文献
75.
We consider the behaviour of a stochastic system composed of several identically distributed, but non independent, discrete-time absorbing Markov chains competing at each instant for a transition. The competition consists in determining at each instant, using a given probability distribution, the only Markov chain allowed to make a transition. We analyse the first time at which one of the Markov chains reaches its absorbing state. When the number of Markov chains goes to infinity, we analyse the asymptotic behaviour of the system for an arbitrary probability mass function governing the competition. We give conditions that ensure the existence of the asymptotic distribution and we show how these results apply to cluster-based distributed storage when the competition is handled using a geometric distribution. 相似文献
76.
The main purpose of this paper is to investigate the optimal replenishment lot size of supplier and optimal production rate of manufacturer under three levels of trade credit policy for supplier–manufacturer–retailer supply chain. The supplier provides a fixed credit period to settle the accounts to the manufacturer, while the manufacturer gives a fixed credit period to settle the account to the retailer and the retailer, in turn, also offers a credit period to each of its customers to settle the accounts. We assume that the supplier supplies the raw material to the manufacturer and sends back the defective raw materials to the outside supplier after completion of inspection at one lot with a sales price. The system always produces good items in the model. Also, we consider the idle times of supplier and manufacturer. Finally, numerical examples are provided to illustrate the behaviour and application of the model with graphical simulation. 相似文献
77.
Bo-Chao Zheng 《International journal of systems science》2014,45(10):1999-2011
In this paper, based on sliding mode control approach, the robust stabilisation problem for a class of continuous-time Markovian jump linear uncertain systems with partly unknown transition rates is investigated. The transition rate matrix under consideration covers completely known, boundary known and completely unknown elements. By making use of linear matrix inequalities technique, sufficient conditions are presented to derive the linear switching surface and guarantee the stochastic stability of sliding mode dynamics. Then a sliding mode control law is designed to drive the state trajectory of the closed-loop system to the specified linear switching surface in finite time in spite of the existing uncertainties and unknown transition rates. Finally, an example is given to verify the validity of the theoretical results. 相似文献
78.
79.
80.
In this paper, we discuss the design of a new Medium Access Control (MAC) protocol, SRI-MAC (Synchronous Receiver Initiated MAC), for wireless sensor networks whose goal is to extend the lifetime of the network by avoiding major energy waste causes, such as collisions, overhearing and idle listening. 相似文献