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91.
《Ceramics International》2022,48(4):4821-4828
We have successfully synthesized multi-layer graphene oxide and graphene oxide based magnetic nanocomposite (M/GO) by microwave-assisted modified Hummers’ method for removal of toxic lead (Pb2+) and cadmium (Cd2+) ions from aqueous solution. The X-ray diffraction spectra of synthesized graphene oxide and M/GO confirm increased interlayer spacing along c-axis. Raman spectra revealed the good quality of synthesized GO and M/GO. The wrinkles were seen in the SEM images of synthesized graphene oxide. The presence of conjugated double bond (CC) and carbonyl (CO) were confirmed by using the UV–Vis spectroscopic spectra. Brunauer–Emmett–Teller (BET) analysis showed high (126 m2/g) surface area M/GO composite which accounts for large number of active binding sites for the adsorption of heavy metal ions. The adsorption studies revealed that Pb2+ ions were efficiently adsorbed on GO sheets. Interestingly, M/GO showed better adsorption for cadmium ions. 相似文献
92.
93.
Alternative hydrocarbon solvents for cottonseed extraction 总被引:3,自引:0,他引:3
P. J. Wan D. R. Pakarinen R. J. Hron Sr. O. L. Richard E. J. Conkerton 《Journal of the American Oil Chemists' Society》1995,72(6):653-659
Hexane has been used for decades to extract edible oil from cottonseed. However, due to increased regulations affecting hexane
because of the 1990 Clean Air Act and potential health risks, the oil-extraction industry urgently needs alternative hydrocarbon
solvents to replace hexane. Five solvents,n-heptane, isohexane, neohexane, cyclohexane, and cylopentane, were compared with commercial hexane using a benchscale extractor.
The extractions were done with a solvent to cottonseed flake ratio of 5.5 to 1 (w/w) and a miscella recycle flow rate of 36
mL/min/sq cm (9 gal/min/sq ft) at a temperature of 10 to 45°C below the boiling point of the solvent. After a 10-min single-stage
extraction, commercial hexane removed 100% of the oil from the flakes at 55°C; heptane extracted 100% at 75°C and 95.9% at
55°C; isohexane extracted 93.1% at 45°C; while cyclopentane, cyclohexane, and neohexane removed 93.3, 89.4, and 89.6% at 35,
55, and 35°C, respectively. Each solvent removed gossypol from cottonseed flakes at a different rate, with cyclopentane being
most and neohexane least effective. Based on the bench-scale extraction results and the availability of these candidate solvents,
heptane and isohexane are the alternative hydrocarbon solvents most likely to replace hexane.
Presented in part at the AOCS Annual Meeting & Expo, Atlanta, Georgia, May 1994. 相似文献
94.
95.
土壤有效磷测试方法浅析 总被引:2,自引:0,他引:2
对有效磷的两种测定方法进行比较,讨论了两种方法之间的相关性及相关系数,为土壤有效磷的测定寻求更省时,省力的测试方法。 相似文献
96.
97.
98.
《Expert systems with applications》2014,41(2):331-341
Time plays important roles in Web search, because most Web pages contain temporal information and a lot of Web queries are time-related. How to integrate temporal information in Web search engines has been a research focus in recent years. However, traditional search engines have little support in processing temporal-textual Web queries. Aiming at solving this problem, in this paper, we concentrate on the extraction of the focused time for Web pages, which refers to the most appropriate time associated with Web pages, and then we used focused time to improve the search efficiency for time-sensitive queries. In particular, three critical issues are deeply studied in this paper. The first issue is to extract implicit temporal expressions from Web pages. The second one is to determine the focused time among all the extracted temporal information, and the last issue is to integrate focused time into a search engine. For the first issue, we propose a new dynamic approach to resolve the implicit temporal expressions in Web pages. For the second issue, we present a score model to determine the focused time for Web pages. Our score model takes into account both the frequency of temporal information in Web pages and the containment relationship among temporal information. For the third issue, we combine the textual similarity and the temporal similarity between queries and documents in the ranking process. To evaluate the effectiveness and efficiency of the proposed approaches, we build a prototype system called Time-Aware Search Engine (TASE). TASE is able to extract both the explicit and implicit temporal expressions for Web pages, and calculate the relevant score between Web pages and each temporal expression, and re-rank search results based on the temporal-textual relevance between Web pages and queries. Finally, we conduct experiments on real data sets. The results show that our approach has high accuracy in resolving implicit temporal expressions and extracting focused time, and has better ranking effectiveness for time-sensitive Web queries than its competitor algorithms. 相似文献
99.
100.
D. Wiesenborn Z. Zbikowski H. Nguyen 《Journal of the American Oil Chemists' Society》1995,72(2):183-188
Extract of purple sunflower hulls is a potential red food colorant; however, suitable process conditions must still be identified.
Selected process variables were studied using bench-scale units to prepare, clarify, concentrate and spray dry extracts. Concentration
by evaporation at 32°C and addition of maltodextrin to 15% (wt/dry wt) prior to drying largely eliminated pigment degradation
during those steps. Relative to water extracts, extracts prepared with 5 to 15% ethanol in water generally yielded more pigment
with similar levels of degradation and loss during subsequent processing. Use of 5% ethanol/2% citric acid reduced yield by
about half relative to water, but gave a powder with a lower degradation index and wetting time. Percentage recovery of pigment
during concentration and drying was not greatly affected by solvent type or extraction temperature. 相似文献