纳米Fe_2O_3作为润滑油添加剂的摩擦磨损性能

采用烧结方法制备得到纳米α-Fe_2O_3,利用X射线衍射仪(XRD)和透射电镜(TEM)对样品进行了表征,研究了纳米α-Fe_2O_3作为液体石蜡添加剂的摩擦磨损性能。结果表明,添加纳米添加剂后,润滑油摩擦系数改变不明显,但磨损率显著降低。磨损率与纳米α-Fe_2O_3添加剂的表面积和添加量密切相关,当纳米材料的表面积为47m~2/g时磨损率最低,磨损率值降低为3.78×10~(-15) m~2/g;添加量为1.0wt%,润滑油磨损率最低。     

A class of aggregation functions encompassing two-dimensional OWA operators

In this paper we prove that, under suitable conditions, Atanassov’s K_α operators, which act on intervals, provide the same numerical results as OWA operators of dimension two. On one hand, this allows us to recover OWA operators from K_α operators. On the other hand, by analyzing the properties of Atanassov’s operators, we can generalize them. In this way, we introduce a class of aggregation functions - the generalized Atanassov operators - that, in particular, include two-dimensional OWA operators. We investigate under which conditions these generalized Atanassov operators satisfy some properties usually required for aggregation functions, such as bisymmetry, strictness, monotonicity, etc. We also show that if we apply these aggregation functions to interval-valued fuzzy sets, we obtain an ordered family of fuzzy sets.     

On global solutions to fractional functional differential equations with infinite delay in Fréchet spaces

In this paper, we investigate global uniqueness results for fractional functional differential equations with infinite delay in Fréchet spaces. We shall rely on a nonlinear alternative of Leray-Schauder type in Fréchet spaces due to Frigon and Granas. The results are obtained by using the α-resolvent family (S_α(t))_t≥0 on a complex Banach space X combined with the above-mentioned fixed point theorem. As an application, a controllability result with one parameter is also provided to illustrate the theory.     

Necessary optimality conditions for fuzzy variational problems

The main aims of this study are to derive the fuzzy Euler-Lagrange conditions for both fuzzy unconstrained and constrained variational problems based on the concepts of differentiability and integrability of a fuzzy mapping that may be parameterized by the left and right-hand functions of its α-level sets.     

牦牛α-乳白蛋白基因单核苷酸多态性分析

为明确牦牛乳中α-乳白蛋白遗传多样性,以α-乳白蛋白基因(LAA)的Ⅰ、Ⅱ、Ⅲ和IV外显子为研究对象,采用聚合酶链反应-单链构象多态性(PCR-SSCP)方法对麦洼牦牛的LAA进行分析,旨在从分子水平揭示LAA在牦牛乳中遗传多样性分布. 牛属不同来源的α-乳白蛋白基因的编码序列被用于构建系统发育树. 结果表明,牦牛乳中LAAⅠ外显子区域以杂合体形式存在,并发现了一个新变异体JN084189. 不同来源LAA的系统发育树分析表明,LAA在进化上存在一定的物种特异性.     

α-酮酸酯合成研究进展

对α-酮酸酯的不同合成方法进行了总结,归纳为Grignard试剂与草酸衍生物反应、特殊氧化反应、过渡金属催化反应、重排反应以及负碳离子引起的亲核反应等方法,并对每种合成方法涉及的反应机理进行了讨论,评价了各种工艺路线的优缺点,对α-酮酸酯类医药中间体的分子设计与有效合成提供了理论参考。     

作用于酪氨酸激酶的抗肿瘤小分子抑制剂γ-氟代Goniothalamin类似物的设计与合成

蛋白酪氨酸激酶在肿瘤细胞的增殖、分化、转移、侵蚀等信号通路中具有重要的调控功能,已成为肿瘤靶向治疗的重点研究对象。基于靶点导向原则和构效关系研究基础,以抗肿瘤活性天然产物Goniothalamin为母体化合物,修饰合成了一系列γ,γ-二氟取代Goniothalamin类似物（4a-4i,6a-6i）和γ-单氟取代Goniothalamin类似物（7a,7b,7h）。γ,γ-二氟取代的Goniothalamin类似物可从具有光学活性的二氟亚甲基取代的锡试剂出发,经Stille偶联和1,5-氧化关环两步关键反应合成。γ-单氟取代Goniothalamin类似物则经Sharpless不对称环氧化、环氧开环亲核氟化、Lindlar氢化、HWE反应和1,5-氧化关环等反应制备。对所合成的这两类Goniothalamin含氟类似物进行了体外肿瘤细胞抑制活性和酪氨酸激酶抑制活性评估研究,结果表明在Goniothalamin分子的γ位引入一个氟原子进行修饰是较为合理的修饰方式。     

基于ZigBee的动态WSN节点定位

针对因障碍物影响而无法实现动态无线传感网MWSN (mobile wireless sensor network)高精度定位的问题,提出了基于RSSI信号传播模型的α-驱动更新的质心定位算法α- drive renewing weighted centroid localization(α-DRWCL).根据WCL (weighted centroid localization)的距离计算公式,建立了路径衰减因子α的计算模型,利用边界探测装置的探测结果适时改变α的值,得到较接近实际情况的各参考节点权重,达到了减小定位误差的目的.在实验环境中对α-DRWCL算法进行定位仿真,仿真结果表明了该算法的精确性和有效性.     

Synthesis and Characterization of Nanocapsules of a-Fe(NiCoAl) Solid-solution

α-Fe(NiCoAl) solid-solution nanocapsules were prepared with pure powders of Fe, Ni, Co and Al by the plasma arc-discharging using a copper crucible. The shapes of the nanocapsules are in polyhedrons with the core/shell structure. The body centered cubic (BCC) phase is formed in the core. The size of the nanocapsules is in the range of 10~120 nm and the thickness of the shell is 4~11 nm. Saturation magnetization Js=150 Am2/kg and coercivity iHC=24.3 kA/m are achieved for the nanocapsules.