Occurrence and Preclusion of Terpene Chlorohydrins in Citrus Essential Oils

ABSTRACT: Screening commercial cold-pressed oils revealed the presence of terpene chlorohydrins, which may have quality and safety implications for end-users. Concentrations of (1R, 2R, 4R)-2-chloro-8- p -menthen-1-ol in some citrus essential oils ranged from less than 1 to 140 ppm. More than half of the oils tested contained less than 2 ppm of (1R, 2R, 4R)-2-chloro-8- p -menthen-1-ol. A pilot plant study used different concentrations of chlorinated water during the oil-recovery process. Cold-pressed oil, produced from a 30-ppm chlorine solution, contained (1R, 2R, 4R)-2-chloro-8- p -menthen-1-ol at detection threshold. The presence of (1R, 2R, 4R)-2-chloro-8- p -menthen-1-ol in citrus essential oils results from processing conditions and can be reduced through the reduction of chlorine levels in treatment water.     

连铸稀土加入工艺试验

对多流大方坯连铸机生产稀土钢的稀土加入工艺进行了试验,分析了钢包、中间包、结晶器喂稀土丝的优缺点,并进行了对比。根据包钢大方坯连铸工艺的特点和实际情况,选出了大方坯连铸稀土钢的稀土加入工艺。     

Fire performance of wood (Pinus radiata) treated with fire retardants and a wood preservative

In this work, we co‐formulated an oil‐borne copper naphthenate/permethrin wood preservative system with synthetic polymer‐based fire‐retardant additives prior to the impregnation of Pinus radiata sapwood. We evaluated what effect, if any, the preservative had upon the fire performance properties of the fire retardants and whether the fire retardants impacted on the fungicidal and termiticidal efficacy of the preservative. The fire retardants included halogenated and phosphorus‐based systems. A mass loss calorimeter, in conjunction with a thermopile, was used to measure the time to ignition and the peak heat release rate (PHRR) from which the fire performance index (FPI) was determined. The preservative properties were evaluated using termite and soil‐block decay bioassays. In summary, we found that the rate of fire growth was reduced when the fire retardants were used in combination with the wood preservative. We also found that the PHRR was a better determinant of fire performance than the FPI. The performance of the wood preservative was enhanced against fungal decay and termite attack when used in combination with the fire retardants. The fire retardants also demonstrated some wood preservative properties of their own. Copyright © 2008 John Wiley & Sons, Ltd.     

蜂胶乙醇浸提液在牛乳制品保鲜中的效果研究

研究了不同浓度的蜂胶对鲜奶的保鲜作用，以及蜂胶对酸奶中酵母菌的抑制作用；同时选择常用化学防腐剂苯甲酸钠作为对照。研究表明，蜂胶能延长鲜奶的保存期。灭菌前加入质量分数为0．1％蜂胶可将鲜奶保存期延长一倍多。0．1％蜂胶可以显著抑制酸奶中酵母的增殖，既可明显延长保存期，又不影响乳制品的自身品质。蜂胶可以代替苯甲酸钠，具有天然保鲜防腐效果。     

粉煤灰和木钙双掺用于胶结充填的正交组合试验

通过粉煤灰和木钙双掺用于尾砂胶结充填的交组合试验，提示了双掺的作用机理，建立了试验指标的二次回归程，得出了双掺时粉煤灰和木钙的最佳掺量。     

CS3000顺控表的组态和应用

介绍CS3000系统顺控表的结构、参数定义和功能块组态,以聚丙烯加氢控制为例,描述顺控表的组态方法、顺控动作和操作步骤等。     

有机磷灭蚊剂投放浓度和时间对水体总磷的影响

为分析新型低毒有机磷杀虫剂“1%双硫磷颗粒”投放对河道水质的影响,设置不同药剂投放浓度和不同反应时间的室内试验,以TP、NH₃-N及S^2-为目标因子,分析该药剂投放后水体污染物浓度。结果表明:不同试验组水样中S^2-质量浓度均小于0.02 mg/L,NH₃-N质量浓度处于0.029~0.036 mg/L之间,均达到地表水Ⅰ类标准;不同浓度药剂投放1 h后,水体TP质量浓度已达到稳定状态,且在60 h内均保持稳定,药剂投加量与水体TP质量浓度呈显著正相关(R²=0.85);不同处理组的药剂在水体中的TP释放量无明显差异,均在1.06~1.30 mg/g之间。“1%双硫磷颗粒”推荐适宜投放量不会使河道水质恶化到劣Ⅴ类,但增加药剂投放量会增加水体TP污染及富营养化风险。     

球团链箅机回转窑工艺中氯和硫元素迁移规律

摘要：对链箅机回转窑工艺中各段球团样品进行实验分析,研究了氯元素和硫元素在链箅机回转窑工艺中的迁移规律,明晰了烟气中HCl的生成机制。结果表明,球团原料中的氯元素主要是以NaCl的形式存在,氯元素有一部分在链箅机抽风干燥段会转变成HCl气体并进入烟气,一部分在链箅机预热Ⅱ段之后以NaCl的形式汽化进入烟气,剩余的氯元素仍以NaCl的形式存在于成品球团矿中。烟气中的HCl气体是在抽风干燥段,由富含SO2的烟气与含水球团料层中的NaCl发生反应生成的,烟气中SO2转变成Na2SO4重新固定于料层中。在预热Ⅰ段和预热Ⅱ段,烟气中的SO2与原料中碳酸钙分解生成的游离CaO反应生成CaSO4,也会重新固定烟气中的SO2。     

炉前包内冲废钢对灰铸铁组织和强度的影响

采用炉前包冲内冲废钢与孕育相结合的方法，研究了炉前包内冲废钢对灰铸铁组织和强度的影响。结果表明：冲废钢可以增加灰铸铁中初生奥氏体的数量，改变初生奥氏体枝晶的分布形态，强化灰铸铁孕育效果，有利于提高灰铸铁的强度。     

稳定态二氧化氯杀菌剂的制备及应用

稳定态二氧化氯(C1O2)是一新型杀菌消毒剂，具有高效、广谱、安全的特性，适用范围广，不产生对人体有害物质。介绍了稳定态ClO2的性质、检测、制备条件及其在有关领域的应用。