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141.
142.
相转移法制备高纯超细TiO2技术研究 总被引:9,自引:0,他引:9
报道了用相转移法制备高纯超细TiO2的新技术;探讨了Ti(Ⅳ)从有机相转移到水相发生水解反应的机理 ;通过TG-DTA分析以及XRD物相分析对水解产物的组成、热分解机理,晶型转变规律进行了研究,建立了水解产物焙烧的最佳温度。 相似文献
144.
F. Cœuret E. Oliveira Vilar E. Bezerra Cavalcanti 《Journal of Applied Electrochemistry》2002,32(10):1175-1182
The paper deals with carbon fibre cloth electrodes, employed in the fabrication of composite materials. The electrical conductivity of single bundles, groups of bundles and cloth is studied. Ohm's law applies to the electrical conduction in the direction of the fibre length, but bundle conductivity decreases with the number of fibres in the bundle. Electrochemical mass transfer between a flowing electrolyte and a cloth arranged as a flow-through or a flow-by porous electrode indicates the existence of double porosity in the material. Due to double porosity, only the external surface of the cloth works as an electrode. This finding shows that the material is not suitable for such an application. 相似文献
145.
Ricardo Garcia-Padron Dan Loyd Stefan Sjökvist 《Subsurface Sensing Technologies and Applications》2002,3(2):125-150
One promising method of locating buried objects, such as land mines, is to use optical systems for detecting contrasts in surface temperature. With enhanced knowledge about the interacting physical processes behind these temperature contrasts, it is possible to improve detection precision. In such a context, moisture movement in the soil and moisture evaporation from the surface have been found to be of particular interest. This study was based on indoor experiments on wet and dry sand exposed to radiation from a solar panel. Simulations of heat and moisture transfer conducted with a one-dimensional model are also presented for the experiments. The calculations were successful in accurately predicting surface temperatures for both wet and dry sand, making it possible to predict surface temperatures under different conditions. These findings will contribute to increasing the probability of successful detection of buried objects under real conditions using optical methods. 相似文献
146.
The hydrodynamic characteristics and mass transfers of halide quaternary salts between two immiscible phases in a stirred membrane permeation cell were investigated. The concentration of quaternary salt, temperature, solvent and the four kinds of halide quaternary salts were evaluated to achieve the extractive optimum condition. The diffusivity, overall mass‐transfer coefficients and individual mass‐transfer coefficients were determined and correlated in terms of the conventional Sh‐Re‐Sc relationship. The transfer time of quaternary salts across the membrane and the thickness of the hydrodynamic diffusion boundary layer were determined as well, so as to characterize the extractive phenomenon of quaternary salts between the two phases that is useful in phase‐transfer catalysis. 相似文献
147.
Mao Ze yu Chen Chang zhi Department of Hydraulic Engineering Tsinghua University Beijing P.R.China 《水动力学研究与进展(B辑)》1999,(3)
1. INTRODUCTIONThesimulationofstreamwatertemperatureissignificantlyimportantforthestudyofnumericalmodelingofrivericeprocesses[1] .Historically,themathematicalmodelingofthetransportandfateofheatinawaterbodyhasbeenthesubjectofextensivestudyforvariousre… 相似文献
148.
149.
Optical measurements of thermal diffusivity of a material 总被引:2,自引:0,他引:2
The measurement of thermal diffusivity of a material (in particular, a thin film) is important for various reasons, e.g., to predict the heat transfer in the solid subjected to a thermal process, to monitor surface composition or morphology, or to detect invisible subsurface defects like delaminations. This measurement can be done in a noncontact manner using various photothermal methods. Such methods typically involve pulsed heating of the surface by small amounts using a laser source; the decay of the surface temperature after this pulsed photothermal heating is then probed to provide the thermal diffusivity. Various probing methods have been developed in the literature, including the probing of reflection, refraction, and diffraction from the pulsed heated area, infrared thermal radiometry, and surface deformation. This paper provides an overview of such techniques and some examples of their applications. 相似文献
150.
A computer model was extended and adapted to simulate the hygrothermal behavior of building envelope-wood components. The model was used to predict moisture movement in wood planks forming the decks of nonvented flat roofs insulated with cellulose. The gradient of water potential was considered as the driving force for moisture movement in wood. The model required the determination of convective heat- and mass-transfer coefficients, the sorption curves, the effective water conductivity for different wood species, and the hygrothermal conditions within the assembly to characterize the mass-conservation equation. Once these parameters were integrated in the computer model, this approach was then validated by carrying a simulation of the drying process of wood planks using experimental data from a large-scale test. 相似文献