The synthesis of block copolyetherketones based on 4,4′‐dichlorodiphenylketone,phenolphthaleine, and bisphenol A and investigation of their properties

Block structured polyethers based on phenolphthaleine, 4,4′‐dichlorodiphenylketone, and bisphenol A with different degrees condensation (n = 1, 5, 10, and 20) were synthesized by means of acceptor‐catalytic polycondensation. Equaimolar quantities of chloranhydrides of iso‐ and terephthalic acids were used. Higher molecular masses were obtained from longer oligoketones with higher condensation degrees. Better molecular packing, increased thermal and mechanical properties were obtained with higher condensation degrees of oligoketones. © 2007 Wiley Periodicals, Inc. JAppl Polym Sci, 2008     

A strategy for the electro-organic synthesis of new hydrocaffeic acid derivatives

Electrochemical treatment processes can significantly contribute to the protection of the environment through the minimization of waste and toxic materials in effluents. From a pharmaceutical point of view and due to the existing resemblance between the electrochemical and biological reactions, it can be assumed that the oxidation mechanisms on the electrode and in the body share similar principles. In this paper, the application of electrochemical studies in the design of an environmentally friendly method was delineated for the new hydrocaffeic acid (HCA, 3,4-dihydroxy hydrocinnamic acid) derivatives synthesis at carbon electrodes in an undivided cell. In this cell, the EC mechanism reaction was involved, comprising two steps alternatively; (1) electrochemical oxidation and (2) chemical reaction. In particular, the electro-organic reactions of HCA, an important biological molecule, were studied in a water–acetonitrile (90:10 v/v) mixture in the presence of benzenesulfinic acid (3) and p-toluenesulfinic acid (4). The research included the use of a variety of experimental techniques, such as cyclic voltammetry, controlled-potential electrolysis and product spectroscopic identification.     

浅析铂钯精矿的提取技术

本文简述湿法工艺提取铂钯金属精矿的工艺技术及主要生产过程     

宝钢曲轴用非调质钢的生产与展望

在实验室研究的基础上，开发了屈服强度为520MPa级的曲轴用微合金化非调质钢48MnV。工业生产了6000余吨φ151mm大规格圆钢，其各项性能满足了用户要求。指出了宝钢曲轴用非调质钢开发和努力的方向。     

加油站电气改造应重视的几个问题

由于加油站电气改造工程的质量对加油站的日常经营和安全管理有重大影响，针对改造中存在的一些共性问题，根据国家有关规范和标准，从电气改造工程的设计、配电系统、配电线路，以及防雷、防静电和防过电压等方面提出了要求和建议。     

PLC在采煤机中的应用

介绍引进美国久益公司 12CM18— 10D连续采煤机主要电气组成、控制、操作方式特点 ,提出操作和使用维护应注意的几个问题     

DGPS在可控震源施工中的应用

在可控震源施工中，采用DGPS(差分全球卫星定位系统)实施实时点位监控，对保证施工质量、提高生产效率起着积极的作用。本文主要介绍PELTON ADVANCE Ⅲ GPS系统的安装和使用情况。     

新打包机接地系统改进

针对贵溪冶炼厂建安公司新紫杂铜打包机不良状况及存在的问题进行了改进 ,对整台机组的总配电箱、液压管网、设备的保护接地及建筑主体框架也进行接地。     

鸡传染性喉气管炎的药物治疗对比试验

从流行病学、临床症状、病理变化和实验室检验四个方面对鸡传染性喉气管炎进行了诊断，并做了药物治疗对比试验．结果表明，杀病毒药(消毒王)加清热解毒、止咳平喘中草药配合治疗鸡传染性喉气管炎，效果更好，能较快地制止病鸡死亡，显著降低死亡率及减少药物治疗费用．     

电子工业用高纯氮的生产

生产电子工业用高纯氮的制氮装置 ,其要点和难点是一氧化碳和氢的清除。采用一氧化碳转换炉和特殊的冷箱内流程组织 ,可以生产纯度为 99 9999%以上的高纯氮。对制取电子工业用高纯氮制氮装置与常规制氮装置加氮终端净化器两种流程进行了比较。