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21.
The ElectroScan environmental scanning electron microscope (ESEM) enables wet samples to be observed by eliminating air but allowing water vapour into the sample chamber. However, evaporation from, and condensation on, the sample may occur during the pumpdown sequence used to reach this state, which means that the sample may not be in its natural state when viewed if due care is not taken. In this paper, the pumping system of the ESEM is described mathematically and expressions are derived for the evaporation and condensation. This treatment is then used to calculate the optimum pumpdown sequence. The importance of using the optimized procedure is illustrated by micrographs of fat emulsions. 相似文献
22.
RM Martín‐Aranda E Ortega‐Cantero ML Rojas‐Cervantes MA Vicente‐Rodríguez MA Baares‐Muoz 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2005,80(2):234-238
α,β‐Unsaturated nitriles have been synthesized by Knoevenagel condensation of a carbonylic compound with malononitrile, assisted by sonochemical irradiation. Two alkaline‐promoted clays (Li+‐ and Cs+‐exchanged saponites) have been employed as catalysts. The influence of the carbonylic compound (benzaldehyde or cyclohexanone) and the use of a solvent on the catalytic activity have been studied. Remarkable increase in the conversion values has been found when the reaction is activated by ultrasound, as compared with the thermal activation. In this green, solvent‐free procedure, α,β‐unsaturated nitriles have been produced in very high yields (97%) when the Cs+‐saponite is used as catalyst. Copyright © 2004 Society of Chemical Industry 相似文献
23.
Kurt F. J. Heinrich 《Journal of research of the National Institute of Standards and Technology》2002,107(6):483-485
Quantitative electron probe analysis is based on models based on the physics or x-ray generation, empirically adjusted to the analyses of specimens of known composition. Their accuracy can be estimated by applying them to a set of specimens of presumably well-known composition. 相似文献
24.
This study addresses the rolling and lifting probabilities for sediment entrainment by incorporating the probabilistic features of the turbulent fluctuation and bed grain geometry. The lognormally distributed instantaneous velocity and uniformly distributed initial grain position, along with a relation between lift coefficient and particle Reynolds number, are used to extend the theoretical formulation of the entrainment probabilities in smooth-bed flows. The two threshold conditions identified herein enable us to precisely define the probabilities of entrainment in the rolling and lifting modes. The results obtained in this study coincide well with the published data. The lifting probability increases monotonously with the dimensionless shear stress θ, which is consistent with the earlier results yet displays improved agreement with the experimental data. The maximum value of rolling probability, with a magnitude of 0.25, occurs at θ ≈ 0.15. For θ<0.05 (or θ>0.6), the rolling (or lifting) probability makes up more than 90% of the total entrainment probability and thus can be used as an approximation to the total probability of entrainment. The proposed rolling and lifting probabilities are further linked to the two separate criteria for incipient motion to explore the critical entrainment probabilities. The results reveal that a consistent probability corresponding to the critical state of sediment entrainment cannot be found. 相似文献
25.
以邻氨基苯甲酸为原料,以不同的中间体和不同的脱水剂对2-甲基-3-甲苯基喹唑啉-4-酮的合成进行研究比较,寻找较佳的合成路径。 相似文献
26.
Pierluigi Guerrini De LucaClaudio Scali 《Chemical engineering science》2002,57(11):2077-2087
Applicability of different temperature oscillation calorimetry algorithms, previously proposed in the literature, for the evaluation of the heat transfer coefficient during the course of the reaction, is analysed by referring to the experimental data from a methyl methacrylate polymerisation reactor.Results are coincident in the nominal case (no errors on data), while differences appear in the elaboration of real data. The effect of uncertainty in the experimental data has been simulated in terms of error on the amplitude and on the phase of reactor and jacket temperature profiles.This approach allows to indicate algorithms having the best robustness properties and to give an explanation of phase errors in terms of a lumped parameter which accounts for different phenomena, not included in the basic hypotheses of the method. Based on this observation, a procedure to eliminate this source of errors from experimental data is proposed for the more general algorithm presented to handle oscillating temperature profiles generated by different techniques. 相似文献
27.
28.
Agnieszka J. Klemm Piotr Klemm Kazimierz Rozniakowski Tomasz W. Wojtatowicz 《Building and Environment》2002,37(12):1233-1240
This paper presents the results of the larger study into a potential application of laser radiation for the detection of phase transition processes in low temperatures occurring on the surface layers of cementitious materials. An attempt was made to identify relationships between the environmental conditions—temperature and air humidity, and the selected parameters of the reflected light. Onset of the condensation process and formation of water microdrops on the surface of the material leads to the phase displacement of individual laser rays, which are represented by different speckle images.
Although the analysis of parameters of the reflected light are very difficult in the case of porous materials because of highly developed roughness of the surface structure it has been proved that a dynamic study of the phase transition phenomena can be successfully carried out without mechanical intervention. 相似文献
29.
Agnieszka J Klemm Piotr Klemm Kazimierz Rozniakowski Tomasz W Wojtatowicz 《Building and Environment》2002,37(12):1221-1232
This paper present the results of the investigation into a potential application of laser radiation for the detection of phase transition processes occurring on the surface layers of porous materials. An attempt was made to discuss in the approximation equations, the relationships between coefficients of the reflected light, the temperature and humidity of the surrounding environment. Laser light reflected from the porous surface carries information about the roughness of the structure. The presence of water microdrop on the surface of the porous material, as a result of condensation and thus a phase transition, leads to the phase displacement of individual rays, which is represented by different images. Therefore, a comprehensive analysis of the reflected light parameters allows a dynamic study of the phase transition phenomena without mechanical intervention. 相似文献
30.
蒸发式冷凝在制冷工艺上的应用 总被引:3,自引:0,他引:3
分析对比制冷工艺中几种冷凝方式,指出发展蒸发式冷凝技术对制冷系统节能的重要意义;通过分析蒸发式冷凝的换热机理,在试验和实践的基础上讨论了影响蒸发式冷凝器性能的几个重要因素。 相似文献