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91.
92.
A number of methods of surface preparation of tantalum for encapsulation in silicone rubber and for structural adhesive bonding were explored. The only ones which could be generally useful were boiling for 24 hours in distilled water (28% improvement) or boiling for 4 hours in 20% sodium hydroxide solution followed by boiling for 2 hours in dilute hydrochloric acid (34% improvement). An alternative, which could sometimes be used, was heating in air for at least 2 hours at 100°C. 相似文献
93.
In this paper, manufacturing technology of the tubular single lap adhesive joint was studied to obtain reliable and optimal joint quality. In addition, a surface preparation method and a bonding process for the joint were devised. The effect of the adhesive thickness and the adherend roughness on the fatigue strength of the joint was experimentally investigated. From experiments, it has been found that the fatigue strength of the joint increased as the adhesive thickness decreased and the optimal arithmetic surface roughness of the adherends was about 2 μm. 相似文献
94.
The surface chemistry of methoxide (CH3O-) on the Ni(111) surface has been studied in the presence of hydrogen pressures up to 2 Torr. During heating in vacuum methoxide decomposes to H2 and CO, which desorb at 380 and 445 K, respectively. The CH3O-decomposition process is rate limited by CH bond breaking and exhibits a strong deuterium kinetic isotope effect in CD3O-. In the presence of ambient hydrogen pressures of 0.02–2.0 Torr both CH3O- and CD3O-are hydrogenated directly to methanol at 310 K. Methoxide is hydrogenated by adsorbed hydrogen, which nearly saturates the surface at these pressures and temperatures. 相似文献
95.
96.
Symmetry is a common characteristic in natural and man‐made objects. Its ubiquitous nature can be exploited to facilitate the analysis and processing of computational representations of real objects. In particular, in computer graphics, the detection of symmetries in 3D geometry has enabled a number of applications in modeling and reconstruction. However, the problem of symmetry detection in incomplete geometry remains a challenging task. In this paper, we propose a vote‐based approach to detect symmetry in 3D shapes, with special interest in models with large missing parts. Our algorithm generates a set of candidate symmetries by matching local maxima of a surface function based on the heat diffusion in local domains, which guarantee robustness to missing data. In order to deal with local perturbations, we propose a multi‐scale surface function that is useful to select a set of distinctive points over which the approximate symmetries are defined. In addition, we introduce a vote‐based scheme that is aware of the partiality, and therefore reduces the number of false positive votes for the candidate symmetries. We show the effectiveness of our method in a varied set of 3D shapes and different levels of partiality. Furthermore, we show the applicability of our algorithm in the repair and completion of challenging reassembled objects in the context of cultural heritage. 相似文献
97.
Micron‐sized polymer particles were coated with layers of nickel compounds by plating electrolessly in the presence of aqueous solutions of nickel chloride, sodium hypophosphite, sodium citrate, and ammonium chloride at elevated temperature. The uniform functional polymer particle could be obtained by seeded polymerization. To investigate the effect of surface functionality on the conditions for nickel deposition, the polymer particle was functionalized with the thiol group. From morphological observation, it was found that the mode of nickel deposition was greatly dependent on the surface functionality of the polymer particle. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 87: 420–424, 2003 相似文献
98.
研究具有外部不确定性R¨ossler 混沌系统的鲁棒跟踪控制问题. 基于动态面控制原理设计自适应鲁棒控制器, 给出了系统参数的自适应更新律, 使得被控闭环系统的各误差变量一致有界. 系统输出曲线渐近跟踪任意期望轨道, 且跟踪误差能被控制在任意小的范围内, 而无须知道系统的参数及外部不确定性的界限. 基于稳定理论给出了具体的稳定性分析, 并通过数值仿真验证了该方法的有效性及鲁棒性.
相似文献99.
Fuel injection rate shaping is a strategy to improve fuel efficiency and reduce harmful emissions in diesel engines. Due to their fast response, piezoelectric fuel injectors are capable of rate shaping operation. This paper describes a model-based closed-loop controller of injection flow rate for a piezoelectric fuel injector. This within-an-engine-cycle control strategy utilizes a dynamic surface control scheme and shows an injection flow rate tracking capability. Practical issues with LabVIEW FPGA control implementation are also addressed. The performance of the controller is verified with simulation and experimental results at different rail pressures and desired injection rates. The experiments show a maximum error of total fuel per one injection event of 2.5%. A stability analysis is also included. 相似文献
100.
E. D. Goddard 《Journal of the American Oil Chemists' Society》1994,71(1):1-16
The field of polymer/surfactant interaction is reviewed in this work. Results from two investigative methods,viz., dialysis and surface tension, are discussed, illustrating the main behavioral patterns and outlining the principles of the
interactions. Next, aspects of the interaction phenomena that appear to have relevance to detergent formulation are presented.
These include solution rheology, solubility control and surface conditioning. Lastly, the importance of surface activity of
the polymer itself is stressed, culminating in a discussion of the properties of hydrophobically modified water-soluble polymers
(“polymeric surfactants”), both alone and in the presence of conventional surfactants.
Based on the Samuel Rosen Memorial Award lecture, given at the AOCS Annual Meeting, Anaheim, CA, April 1993. 相似文献