金刚石刀具银钎焊方法

为了更好地实现金刚石刀头与刀具基体的连接,并保证一定的结合强度,采用银钎焊方法。银钎料的元素成分和含量、钎焊剂类型和作用、加热设备及感应器形状的选择和温度控制、焊缝尺寸大小和装配间隙、钎焊前的预处理等是获得优质钎焊接头的关键因素。通过对获得的银钎焊接头进行试验分析和公式应力计算及无损检测等金刚石刀具银钎焊方法的可靠性评估,结果达到并满足了金刚石刀具的切削强度要求。有效预防或避免了钎焊接头的缺陷产生,从而获得了优质的钎焊接头,保证并延长金刚石刀具的使用寿命。     

Mechanism and prediction of failure of diamond films deposited on various substrates by HFCVD

Diamond films were deposited on the WC-Co cemented carbide and Si3N4 ceramic cutting tool substrates by hot-filament-assisted chemical vapour deposition. The adherence property of diamond films was estimated using the critical load (Pcr) in the indentation test. The adhesive strength of diamond films is related to the intermediate layer between the film and the substrate. Poor adhesion of diamond films to polished cemented carbide substrate is owing to the formation of graphite phase in the interface. The adhesion of diamond films deposited on acid etched cemented carbide substrate is improved, and the peeling-off of the films often happens in the loosen layer of WC particles where the cobalt element is nearly removed. The diamond films' adhesion to cemented carbide substrate whose surface layer is decarbonizated is strengthened dramatically because WC phase forms by reaction between the deposited carbon and tungsten in the surface layer of substrates during the deposition of diamond, which results in chemical combination in the film-substrate interface. The adhesion of diamond films to silicon nitride substrate is the firmest due to the formation of chemical combination of the SiC intermediate layer in the interfaces. In the piston-turning application, the diamond-coated Si3N4 ceramic and the cemented carbide cutting tools usually fail in the form of collapsing of edge and cracking or flaking respectively. They have no built-up edge(BUE) as long as coating is intact.As it wears through, BUE develops and the cutting force on it increases 1 - 3 times than that prior to failure. This can predict the failure of diamond-coated cutting tools.     

D杯形砂轮修整碟形金刚石砂轮试验研究

本文采用了D杯形砂轮与碟形砂轮对磨法来修整大直径树脂结合剂碟形金刚石砂轮。在分析研究杯形砂轮修整碟形砂轮的修整原理及修整方式的基础上，用自行研制的专用修整装置，从主轴转速、修整深度、修整工具结合剂类型等方面进行了对比工艺试验研究，总结了杯形砂轮修整碟形砂轮的不同工艺参数与修整效率、修整质量之间的工艺规律。试验结果表明，在本试验条件下主轴转速500r／min，修整深度0．02mm的修整效率较好；细粒度、中等浓度的青铜结合剂杯形金刚石砂轮与粗粒度、高浓度的杯形砂轮修整碟形砂轮相比，后者具有较好的修形效果和修整效率；D杯形砂轮与GC杯形砂轮交替配合使用可以大大提高碟形金刚石砂轮的修形效率和修锐效果。     

基底材料和温度对CVD金刚石沉积的影响

使用热丝CVD装置在钢渗铬层、三氧化二铝、YG8硬质合盒基底上沉积了金刚石膜、结果表明，在700～900℃温度范围内，热稳定性好的基底材料有利于金刚石晶核的形成。硬质合金和三氧化二铝的热稳定性都比钢港铬层好，在700～900℃能获得10^7cm^-2以上的形核密度，而钢渗铬层超过800℃后．形核密度低于10^6cm^-2。     

磨PCD刀具陶瓷结合剂金刚石砂轮的研究

本文研究制备Na2O-B203-Si02-Al203多元系基玻璃料,并配制成低温陶瓷结合剂,研究发现:耐火度为685℃,流动性为110%～130%,线膨胀系数为5.35×10-6℃-1的低温陶瓷结合剂具有优异的性能.制备的陶瓷结合剂金刚石砂轮在725℃烧成后,磨具的抗弯强度和洛氏硬度达到最佳值,分别58.61 MPa和77.9.用其磨削PCD刀片时锋利性好,磨削中间不需修整,砂轮耐用度高.运用扫描电子显微镜(SEM)分析了陶瓷结合剂金刚石磨具的断面形貌、磨削后磨削面形貌,表明结合剂对磨粒黏结牢固,断面组织均匀.     

稀土对切玻璃金刚石锯片切削性能的影响

金刚石圆锯片可以用于切割玻璃和水晶制品。为了提高切割玻璃金刚石圆锯片的切割寿命和玻璃的切割质量．对切割玻璃金刚石圆锯片的胎体成分进行了优化设计，并在胎体材料中加入稀土化合物La2O3，同时对金刚石表面实施镀钛。本文从胎体材料对金刚石的把持力系数、实际切割的金刚石的脱落度以及锯片的切割速度方面，研究了稀土化合物在金刚石刀头胎体中的作用。结果表明：在胎体金属粉中加入适量的稀土化合物，胎体对金刚石的把持力系数有所改善，同时，增加了刀头胎体材料的脆性，实现了金刚石与胎体的同步磨损，金刚石的脱落度明显减小；切割速度比参比片提高了21．6％。     

钎焊金刚石砂轮磨削石材中金刚石粒度对磨削力的影响研究

本文通过测量不同金刚石粒度的高频感应钎焊金刚石砂轮磨削花岗石过程中的磨削力，对砂轮所受的法向力和切向力进行了研究。对不同粒度条件下磨削深度、进给速度和砂轮线速度对磨削力的影响进行了分析。研究发现磨削力随砂轮线速度的增大而减小，随磨削深度和进给速度的增大而增大，磨削深度对磨削力的影响程度比进给速度大。小粒度金刚石磨削时，磨削三要素对磨削力的影响比大粒度金刚石磨削时大。     

电铸金刚石-镍复合膜微观应力分析

用电铸方法，采用低应力电镀液，研制出了金刚石-金属复合膜。该复合膜的厚度为20-45μm，可用于制作超薄切割刀具。介绍了用X射线衍射法（xRD）测量多晶体微观应力的基本原理和用X射线衍射法测量镍多晶体显微应变的程序。用单波法计算了电铸金刚石-镍复合膜的显微应变，并用扫描电镜（SEM）观察了该复合膜的表面形貌。结果发现：阴极电流密度严重影响复合膜的显微应变，在实验所用电流密度范围内（0．6-3．5A／dm^2），随着电流密度的增加，显微应变减小。     

A study of diamond synthesis by hot filament chemical vapor deposition on Nc coatings

Deposition of diamond films onto various substrates can result in significant technological advantages in terms of functionality and improved life and performance of components. Diamond is hard, wear resistant, chemically inert, and biocompatible. It is considered to be the ideal material for surfaces of cutting tools and biomedical components. However, it is well known that diamond deposition onto technologically important substrates, such as co-cemented carbides and steels, is problematic due to carbon interaction with the substrate, low nucleation densities, and poor adhesion. Several papers previously published in the relevant literature have reported the application of interlayer materials such as metal nitrides and carbides to provide bonding between diamond and hostile substrates. In this study, the chemical vapor deposition (CVD) of polycrystalline diamond on TiN/SiN _x nc (nc) interlayers deposited at relatively low temperatures has been investigated for the first time. The nc layers were deposited at 70 or 400 °C on Si substrates using a dual ion beam deposition system. The results showed that a preliminary seeding pretreatment with diamond suspension was necessary to achieve large diamond nucleation densities and that diamond nucleation was larger on nc films than on bare sc-Si subjected to the same pretreatment and CVD process parameters. TiN/SiN _x layers synthesized at 70 or 400 °C underwent different nanostructure modifications during diamond CVD. The data also showed that TiN/SiN _x films obtained at 400 °C are preferable in so far as their use as interlayers between hostile substrates and CVD diamond is concerned. This paper was presented at the fourth International Surface Engineering Congress and Exposition held August 1–3, 2005 in St. Paul, MN.     

微细电极精密车削技术

对微细电极的精密车削工艺进行了研究，用人造金刚石刀具，加工出直径φ7μm的微细电极，用车削的φ11μm微细电极成功地加工出φ19μm的微细孔。研究结果表明，在微细电极的加工中，切削用量不仅对电极表面质量产生影响，而且关系到能否车削成功。