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61.
Bai-Huan Xu Dong-Ya Sun Cong Ding Xue-Zhong Liu Zi-Jing Xiao 《Materials Research Bulletin》2007,42(9):1633-1639
Layered nanocomposite PEG/WS2, intercalating oligomeric poly(ethylene glycol) (PEG6000) into the tungsten disulfide host galleries, was synthesized using the exfoliation-adsorption technique. X-ray diffraction revealed that the intercalated oligomer within the host galleries is in a double-layer arrangement with an interlayer expansion of about 8.8 Å. The optimum conditions were explored to prepare the single-phase product with a composition of Li0.12(PEG)1.51WS2. Thermal analyses suggested that the resulting material shows good thermal stability, with the decomposition of the interacted oligomeric chains within the disulfide galleries occurring at around 258 °C. Despite high conductivity of the host material, those of the PEG/WS2 nanocomposite were found to be high in the order of 1 × 10−2 S cm−1 at ambient temperature, resulted from the host guest-host charge transfers. 相似文献
62.
《Materials and Manufacturing Processes》2007,22(1):5-8
The technological properties of the hot-work tool steels depend on their microstructural quality induced by the production process and the heat treatment. One of the frequently applied methods to improve microstructure is preheat treatment. The treatment of carbonitriding X37CrMoV5-1 steel has been investigated in fluidized bed furnaces. Thickness and phase composition have been conducted using optical microscopy Neophot 32 and scanning microscopy, JEOL 5400, after etching in nital. 相似文献
63.
D. L. Cotrell A. J. Kearsley 《Journal of research of the National Institute of Standards and Technology》2007,112(3):153-161
In this work, optimal shaft shapes for flow in the annular space between a rotating shaft with axially-periodic radius and a fixed coaxial outer circular cylinder, are investigated. Axisymmetric steady flows in this geometry are determined by solving the full Navier-Stokes equations in the actual domain. A measure of the flow field, a weighted convex combination of the volume averaged square of the L2-norm of the velocity and vorticity vectors, is employed. It has been demonstrated that boundary shape can be used to influence the characteristics of the flow field, such as its velocity component distribution, kinetic energy, or even vorticity. This ability to influence flow fields through boundary shape may be employed to improve microfluidic mixing or, possibly, to minimize shear in biological applications. 相似文献
64.
Fresh niobium hydroxide was first precipitated from NbF5 solution using an aqueous ammonium hydroxide under basic conditions. Then a simple procedure of mixing lithium and niobium hydroxides together and heating at a low temperature (400 °C) produced pure ultrafine single phase LiNbO3 (LN). In the literature, this is the lowest temperature so far reported on the formation of LN. The phase content and lattice parameters are determined by X-ray diffraction (XRD). The average particle size and morphology were studied by transmission electron microscopy (TEM). 相似文献
65.
小型微/纳米级三坐标测量机的研制 总被引:11,自引:1,他引:10
介绍一套低成本小型三维坐标测量机的研制过程,作为微/纳米级超精密测量设备,整体机台结构采用花岗岩材料;X/Y轴的移动平台利用压电材料摩擦驱动与挠性变形原理,长短两行程可达25mm范围及5nm的微位移,藉自行研发的衍射干涉激光尺,位置回馈测量系统可具有0.025nm的分辨率;测量探头在一般DVD光读取头的自动聚焦原理基础上改装,最佳分辨率可达2.5nm,该雏形机适于测量微机电组件、微型器件及膜厚等。 相似文献
66.
D. K. Burghate V. S. Deogaonkar S. B. Sawarkar S. P. Yawale S. V. Pakade 《Bulletin of Materials Science》2003,26(2):267-271
In this paper the results of thermally stimulated discharge current (TSDC) and dielectric constant for 40PbO-60Bi2O3 glass thermoelectrets are presented. Measurements of TSDC and dielectric constant, ǵe, have been carried out in the temperature
range 30–300°C. The thermoelectrets were prepared at different polarizing fields. The various observed peaks in the thermograms
are discussed on the basis of space charge polarization. The trap energy is evaluated from the Garlick-Gibson plot of initial
rise method. Similarly other parameters such as relaxation time, charge release etc are evaluated. 相似文献
67.
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69.
Sipra Mahapatra Turaga P. Prasad 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1992,53(2):201-203
Hydrolysis of Fe(OH)SO4 was carried out in the presence of metallic iron in order to prevent the formation of iron(III) oxides with strongly bonded sulphate. Under the conditions of the experiment, the products were found to be mixtures of ?-Fe2O3 and α-FeOOH. The occluded sulphate, if any, could be easily washed out with water. The hydrolysis reaction passes through an equilibrium state before coming to completion. The entropy with enthalpy of the hydrolysis corresponding to the equilibrium state were found to be 4 e.u. and 0·5 kJ/mol, respectively. The activation energy of the hydrolysis reaction was found to be 21 kJ/mol. 相似文献
70.
复杂不规则刚体转动惯量的测试原理和方法 总被引:6,自引:0,他引:6
为了测量复杂不规则刚体转动惯量,采用时间常数法,通过A/D卡PS2129的定时/计数器8253高精度测速、计时,能较好地应用于测量转动惯量。 相似文献