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41.
A series of new alternating aromatic poly(ester‐imide)s were prepared by the polycondensation of the preformed imide ring‐containing diacids, 2,2′‐bis(4‐trimellitimidophenoxy)biphenyl (2a) and 2,2′‐bis(4‐trimellitimidophenoxy)‐1,1′‐binaphthyl (2b) with various aromatic dihydroxy compounds in the presence of pyridine and lithium chloride. A model compound (3) was also prepared by the reaction of 2b with phenol, its synthesis permitting an optimization of polymerization conditions. Poly(ester‐imides) were fully characterized by FTIR, UV‐vis and NMR spectroscopy. Both biphenylene‐ and binaphthylene‐based poly(ester‐imide)s exhibited excellent solubility in common organic solvents such as tetrahydrofuran, m‐cresol, pyridine and dichloromethane. However, binaphthylene‐based poly(ester‐imide)s were more soluble than those of biphenylene‐based polymers in highly polar organic solvents, including N‐methyl‐2‐pyrrolidone, N,N‐dimethylacetamide, N,N‐dimethylformamide and dimethyl sulfoxide. From differential scanning calorimetry thermograms, the polymers showed glass‐transition temperatures between 261 and 315 °C. Thermal behaviour of the polymers obtained was characterized by thermogravimetric analysis, and the 10 % weight loss temperatures of the poly(ester‐imide)s was in the range 449–491 °C in nitrogen. Furthermore, crystallinity of the polymers was estimated by means of wide‐angle X‐ray diffraction. The resultant poly(ester‐imide)s exhibited nearly an amorphous nature, except poly(ester‐imide)s derived from hydroquinone and 4,4′‐dihydroxybiphenyl. In general, polymers containing binaphthyl units showed higher thermal stability but lower crystallinity than polymers containing biphenyl units. Copyright © 2005 Society of Chemical Industry 相似文献
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In this paper, the test results of liquid injection impact on the performance of new alternative refrigerant mixtures such as: R-410A, R-507, R-407C and R-404A are discussed, analysed and presented. The test results were obtained using an air-source heat pump set-up with enhanced surface tubing under various liquid injection ratios. Performance tests were conducted according to the ARI/ASHRAE standards. The performance data demonstrated that as liquid injection ratio increases, compressor head pressure and discharge temperature decrease. This has a positive effect in protecting the compressor. The effect of liquid injection on mixture behaviour varies from one mixture to another depending upon the mixture's composition. Furthermore, liquid injection appears to have a significant influence on R-410A behaviour compared to the other mixtures in question. Copyright © 2002 John Wiley & Sons, Ltd. 相似文献
44.
如何利用循环体诸如初值、终值、步长和下标式等数学对象的诸如恒等、正负、单调性一类的数学特征,按照严格推导出来的简单规则,绕过各种复杂的数据依赖关系图及其上诸如拓扑排序或等价变换等复杂的操作,直接从事向量化处理,这是极富实用价值的研究方向.文献[2,3,5]给出的可原形/准原形算法,以及本文的可反原形与拟离散性,正是这样的捷径.它们能使相当部分的常见循环,直接向量化. 相似文献
45.
注射成形Fe-50%Ni软磁合金的研究 总被引:3,自引:0,他引:3
Fe-50 %Ni合金是一种典型的高磁导率和低矫顽力的软磁材料,有着广阔的应用前景.本次实验采用注射成形方法制取Fe-50 %Ni,研究了在注射成形工艺中烧结工艺对最终产品性能及微观组织的影响,并分析了影响产品磁性能的一些主要因素.实验表明,烧结温度的提高和烧结时间的延长能够较好改善产品的力学性能;密度是影响产品磁性能的主要因素,杂质(主要指(C、O、N)的含量和晶粒尺寸对剩磁、磁导率和矫顽力也有较大的影响;通过注射成形方法制取的Fe-50 %Ni,其性能要优于采用传统粉末冶金方法制造的Fe-50 %Ni. 相似文献
46.
研究了不同温度下PTT(聚对苯二甲酸丙二醇酯)直接酯化反应动力学。建立了零级和一级反应动力学模型。用实验数据进行的检验表明,一级动力学模型更为接近该反应过程。 相似文献
47.
低渗透油田合理注采井距的确定--以纯41块沙4段低渗透油田为例 总被引:3,自引:1,他引:2
以纯41块沙4段低渗透油田为例,从低渗透油田渗流机理出发,分析了造成低渗透油田开发效果差的主要原因。在计算注水井最大井底流压、油井最小井底流压、油水井之间可建立的最大注采压差的基础上,结合室内试验确定的最小启动压力梯度公式计算油田技术极限注采井距,并结合经济合理井距计算结果,确定了油田合理注采井距,并提出了下二步调整方案,实施后取得了显著的效果。该方法为低渗透油田合理井距的确定、提高低渗透油田的开发效果提供了理论依据。 相似文献
48.
H.J. Bolink E. Coronado D. Repetto M. Sessolo E.M. Barea J. Bisquert G. Garcia‐Belmonte J. Prochazka L. Kavan 《Advanced functional materials》2008,18(1):145-150
A new type of bottom‐emission electroluminescent device is described in which a metal oxide is used as the electron‐injecting contact. The preparation of such a device is simple. It consists of the deposition of a thin layer of a metal oxide on top of an indium tin oxide covered glass substrate, followed by the solution processing of the light‐emitting layer and subsequently the deposition of a high‐workfunction (air‐stable) metal anode. This architecture allows for a low‐cost electroluminescent device because no rigorous encapsulation is required. Electroluminescence with a high brightness reaching 5700 cd m–2 is observed at voltages as low as 8 V, demonstrating the potential of this new approach to organic light‐emitting diode (OLED) devices. Unfortunately the device efficiency is rather low because of the high current density flowing through the device. We show that the device only operates after the insertion of an additional hole‐injection layer in between the light‐emitting polymer (LEP) and the metal anode. A simple model that explains the experimental results and provides avenues for further optimization of these devices is described. It is based on the idea that the barrier for electron injection is lowered by the formation of a space–charge field over the metal‐oxide–LEP interface due to the build up of holes in the LEP layer close to this interface. 相似文献
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