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51.
介绍了 6 m大容积焦炉由冷态到转入正常加热温度的烘炉操作过程中 ,按照一定的升温曲线 ,通过对焦炉热工和炉体膨胀的科学管理 ,确保新建焦炉顺利由冷态过渡到生产状态。 相似文献
52.
Carbon Aerogels as Electrode Material in Supercapacitors 总被引:5,自引:0,他引:5
U. Fischer R. Saliger V. Bock R. Petricevic J. Fricke 《Journal of Porous Materials》1997,4(4):281-285
Due to their large specific surface area and their high electrical conductivity carbon aerogels are promising materials for electrodes in electrochemical double-layer capacitors (supercapacitor). The carbon aerogels were made via pyrolysis of resorcinol formaldehyde aerogels. The latter were prepared by supercritical and subcritical drying as well. The important findings of our investigation were, that the highest capacities of 46 F/cm3 were measured for samples with a density of about 800 kg/m3 pyrolyzed at 800°C. Also it was shown that RF-gels with molar resorcinol/catalyst ratios 1000 or higher can be dried subcritically without cracking or significant shrinkage. Carbon aerogels derived from these RF-aerogels have a small mesopore surface area, however an especially large micropore area. They provide electrical capacities which are most suitable for their use in supercapacitors. 相似文献
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54.
低密度泡沫玻璃是利用碎玻璃制造的一种气孔率大于90%的隔热保温材料,它具有强度高、导热系数小、吸水率低、不吸湿、耐腐蚀等特性,在潮湿环境下抗冻性能好,是一种优良的低温、超低温隔热保温材料。该产品用途广泛,所用的原材料简单易得,但生产工艺过程比较复杂,生产过程控制精度要求较高,容易产生各种缺陷而影响产品的质量。本文对低密度泡沫玻璃的生产工艺过程进行详细的分析研究,提出相应的措施,确保产品的低密度和高成品率,提高产品的性能,扩大产品的使用范围。 相似文献
55.
56.
Four cocatalysts, referred to as ethylaluminoxanes, were synthesized by the reaction between triethylaluminium (AIEt3) and water under various molar ratios of H2O/Al at ?78°C. Aluminoxanes were used as cocatalysts for a MgCl2‐supported Ziegler–Natta catalyst for propylene polymerization at temperatures ranging from 70 to 100°C. When the polymerization was activated by AlEt3, the activity as well as the molecular weight and isotacticity of the resulting polymer gradually dropped as the temperature varied from 70 to 100°C. When ethylaluminoxane was employed as the cocatalyst, good activity and high molecular weight and isotacticity were obtained at 100°C. Furthermore, when the cocatalyst varied from AlEt3 to ethylaluminoxane, the atactic fraction and polymer fraction with moderate isotacticity decreased and the high isotactic fraction slightly increased, which indicated that the variation of the cocatalyst significantly affects the isospecificity of active sites. It was suggested that the reactivity of the Al‐Et group and the size of the cocatalyst were correlated to the performance of the Ziegler–Natta catalyst at different temperatures. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 1978–1982, 2006 相似文献
57.
When BaTiO3 ceramics were sintered at relatively low temperatures (≤1250°C), the grains with reentrant edges caused by a (111) double twin grew exclusively. As a result, a microstructure with a bimodal grain-size distribution composed of platelike large grains and fine matrix grains was obtained. In contrast, at the usual sintering temperature between 1250° and 1350°C, grains containing a (111) double twin did not exhibit any growth advantage. In this case, a coarse and uniform microstructure was obtained. When this coarse-grained specimen was further heat-treated at 1365°C, the grains possessing a double twin were observed to grow exclusively again. The results were explained in terms of a coarsening process controlled by two-dimensional nucleation. 相似文献
58.
59.
制备了一种含Zn2+、Mn2+、N i2+三系离子的LC-1磷化液,通过硫酸铜点滴、氯化钠浸蚀、SEM等手段对磷化膜进行了测试,测定了磷化温度、磷化时间对膜层耐蚀性的影响。结果表明,在磷化温度大于65℃,磷化时间大于10 m in的条件下,所形成的磷化膜结晶均匀、致密、黑褐色,耐蚀性良好。LC-1三系磷化液可适用于大批量钢铁工件的磷化生产。 相似文献
60.
大冶硫酸四系列干吸塔结构特点 总被引:1,自引:0,他引:1
以干燥塔为例,介绍大冶公司硫酸四系列干吸塔的结构特点。除捕沫层简体及出气管为316L不锈钢外,其余塔体均为碳钢内衬瓷砖结构。塔底为球形底,中心排酸。采用槽管式分酸器,分酸点密度为43个/m^2,设可调闸板以保证各槽酸量均匀;闸板外设置带孔板的分布板,以消除进口酸的冲击,保证槽内酸液面平稳。比较了该塔与常规塔的不同之处,强调了设备节点的优化设计。 相似文献