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241.
添加稀土引致的磷化膜变化与促进机制 总被引:1,自引:0,他引:1
邝钜炽 《腐蚀科学与防护技术》2006,18(3):190-191
用能谱与SEM分析,发现加入稀土硝酸盐(REN)后明显提高了无定形晶体Zn2Fe(PO4)2在磷化膜表面的覆盖率,而使得膜的耐蚀性能提高.此时膜内相关元素含量比例发生了变化:P增大,Zn减小,可见磷对膜耐蚀性的贡献比锌大.讨论认为,稀土硝酸盐是一个有良好载氧能力的催化剂,具有良好的成核促进作用和阴极去极化作用,从而能加速磷化并使膜的耐腐蚀性能提高.
相似文献
242.
TiN/SiNx multilayer coatings were deposited on stainless steel by Chemical Vapor Deposition in a Fluidized Bed Reactor at Atmospheric Pressure (AP/FBR-CVD) by reaction of TiCl4 and SiCl4 with NH3 at 850 °C. Due to the immiscibility of crystalline TiN and amorphous SiNx, interdiffusion between layers is avoided even at the high working temperature. The thickness of the individual layer was in the nanometer range. Coatings were characterized by means of SEM, TEM, GD-OES, SIMS, XRD and nanoindentation. A mechanism for the growth rate and diffusion of Ti and Si into the steel is discussed. 相似文献
243.
The ceramic coating formed on AZ91 magnesium alloy by micro-arc oxidation (MAO) was characterized. The results show that the ceramic coating (3.4-23 μm in thickness)on the surface ofAZ91 alloy was attained under different micro-arc oxidation treatment conditions, which consist mainly of MgO, Mg2SiO4 and MgSiO3 phases. Nano-hardness in a cross-sectional specimen was determined by nano-indentation experiment. The MAO coatings exhibit higher hardness than the substrate. Dry sliding wear tests for the MAO coatings and AZ91 alloy were also carded out using an oscillating friction and wear tester in a ball-on-disc contact configuration. The wear resistance of the MAO coatings is improved respectively under different treatment time as a result of different structures of ceramic coatings formed on AZ91 alloy. 相似文献
244.
245.
小波分析在火箭发动机包覆质量检测中的应用 总被引:1,自引:0,他引:1
将小波分析方法应用到固体火箭发动机包覆层胶接质量检测中,利用小波分析的多分辨率特征,对超声检测信号的小波系数进行特征提取,从而获得包覆层胶接状态的灰度图像,图像效果很好,而且与试件情况基本吻合。 相似文献
246.
Influence of expandable graphite on fire resistance and water resistance of flame-retardant coatings 总被引:1,自引:0,他引:1
Expandable graphite (EG) coating and ammonium polyphosphate-pentaerythritol-melamine (APP-PER-MEL) coating were prepared. Thermal degradation and char formation of the coatings were investigated by differential thermal analysis (DTA), thermogravimetry (TG), X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The results have shown that the anti-oxidation and fire-resistant properties of expandable graphite coating containing EG with size of 74 μm are better than those of APP-PER-MEL coating. The static immersion test was applied to study water resistance of the coatings, and the fire protection test and mechanical test were used to analyse heat insulation and mechanical properties of coatings before and after water immersion. The fire-resistant and mechanical properties of APP-PER-MEL coating were severely damaged by water immersion, whereas EG coating containing 8.5% EG with size of 74 μm could retain the good fire resistance even after 500 h water immersion. 相似文献
247.
K. A. Khor F. Y. C. Boey Y. Murakoshi T. Sano 《Journal of Thermal Spray Technology》1994,3(2):162-168
There has been increasing use of Al-Li alloys in the aerospace industry, due mainly to the low density and high elastic modulus
of this material. However, the problem of low ductility and fracture toughness of this material has limited its present application
to only weight- and stiffness-critical components. Development of Al-Li/ceramic composites is currently being investigated
to enhance the service capabilities of this material. The Ti-Al alloy is also of interest to aerospace-type applications,
engine components in particular, due to its attractive high-temperature properties. Preparation of fine powders by plasma
melting of composite feedstock and coatings formed by plasma spraying was carried out to examine the effect of spray parameters
on the microstructure and properties of these materials. Characterization of the powders and coatings was performed using
the scanning electron microscope and image analyzer. Examination of the plasma-sprayed powders and coatings has shown that
in the Al-Li/SiC composite there is melting of both materials to form a single composite particle. The SiC reinforcement was
in the submicron range and contributed to additional strengthening of the composite body, which was formed by a cold isostatic
press and consolidated by hot extrusion or hot forging processes. The plasma-sprayed Ti-Al powder showed four categories of
microstructures: featureless, dendritic, cellular, and martensite-like. 相似文献
248.
Aluminum coatings were sprayed on the substrate of steel Q235 by arc spraying. The test samples of Q235, Al coatings and Al coatings with seal coat were placed in box type electric resistance furnace at 400, 500,600, 650 ℃ when their oxidation behaviors were studied. And their oxidation kinetics curves were protracted. Microstructure, microhardness, bond strength and distribution of section elements were investigated by optical microscope(OM), Vickers microhardness instrument, electric tensile test machine and EPMA. Al coatings and Al coatings with seal coat can enhance the oxidation-resistance of substrate under 500 ℃. The latter has the best corrosion resistance. The coatings can't protect the substrate against oxidation above 600 ℃. After a long time corrosion there is enriched oxygen element at interface. 相似文献
249.
通过对380kW电动机磨损主轴失效原因的分析,提出了修复该零件的新工艺.采用镀覆特殊镍-Ni-金刚石复合镀层体系,提高了镀层与基体,镀层与工作层的结合力,增加了修复层的硬度,改善了主轴配合面的耐磨性,使修理质量得到了提高. 相似文献
250.
1 INTRODUCTIONAluminumindustryhasbeendevelopingrapidlyinChinainrecentyears ,soderbergcellshavebeenre placedwithmodernprebakecellsinmanyaluminumsmelters,theaveragecelllifehowever ,forprebakecellsinourcountrywasonlyabout130 0d ,muchlowerthantheaveragecelllife ,i.e .above 2 5 0 0d ,forthecellsindevelopedcountries .TiB2 cathodecoating (TCC)couldbeoneofthesolutionstoreducegreatlytheopportunitytotheearlyfailureofcellsandextendthecelllifeofprebakecell[14 ] .Theconceptoftitaniumdiboride (TiB2 … 相似文献