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991.
K-S. Park S-H. Park Y-K. Sun K-S. Nahm Y-S. Lee M. Yoshio 《Journal of Applied Electrochemistry》2002,32(11):1229-1233
The structural and electrochemical properties of LiNiO2 powders were investigated as a function of the oxygen flow rate employed in the preparation of lithium nickel oxide. It was found that oxygen played an important role in the synthesis of highly crystallized LiNiO2(R3¯m). In the crystallization process of LiNiO2, a deficiency of oxygen in the calcination reactor induced the formation of impurities and cubic rock-salt structure (Fm3m) in LiNiO2 powders. For LiNiO2 prepared at higher oxygen flow rates, the electrode delivered high discharge capacities with relatively good retention rates. But very low electrode capacity was obtained from LiNiO2 prepared at lower oxygen flow rates. 相似文献
992.
异丁烷与丁烯烷基化反应工艺 总被引:8,自引:1,他引:7
讨论了异丁烷与丁烯烷基化反应工艺在清洁燃料生产过程中的地位、作用和发展趋势;简介了目前石油炼制工业中使用的液体酸烷基化工艺;详细介绍了正在研究开发的固体酸烷基化技术;对在烷基化反应中应用的新型固体酸催化材料和新催化反应工艺的探索和进展进行了综述。 相似文献
993.
994.
995.
Muhammad A. Al-ArfajWilliam L. Luyben 《Chemical engineering science》2002,57(5):715-733
This paper considers the design and control of a reactive distillation column in which one reactant is consumed and two products are formed (A?B+C). The volatilities are αB>αA>αC, i.e. the reactant is intermediate boiling between the two products. The metathesis of 2-pentene is considered as the demonstrative example. The column has a single feed of the intermediate boiling reactant. The distillate contains mostly light component and the bottoms mostly heavy.Three designs are considered: the base case (low-conversion/low-pressure), a low-conversion/high-pressure case and a high-conversion/high-pressure case. The base design is obtained from the literature, and the other two steady-state designs are optimized with respect to the total annual cost. All the designs are found to be openloop stable. Five control structures are studied for the base design. Then the best two structures are applied to the remaining two designs. This category of reactive distillation exhibits less challenging problems than other categories since it uses a single feed, which eliminates the need for the control structure to perfectly balance two fresh feeds.Simulation results demonstrate that effective dynamic control is provided by a control structure that uses two temperatures to maintain the purities of both product streams. No internal composition measurement is required. This structure is found to be robust and stable and rejects loads and tracks setpoints very well. 相似文献
996.
Takakazu Yamamoto Kouichi ShiraishiMahmut Abla Isao YamaguchiL.“Bert” Groenendaal 《Polymer》2002,43(3):711-719
Neutral and non-doped poly(3,4-ethylenedioxythiophene), PEDOTh(Ni), and its hexyl derivative, PEDOTh-C6(Ni), have been prepared by organometallic dehalogenation polycondensation of 2,5-dichloro-3,4-ethylenedioxythiophene and its hexyl derivative with a zerovalent nickel complex. PEDOTh-C6(Ni) was soluble in organic solvents and 1H NMR data indicated that it had an Mn of 11,000. MALDI-TOF mass analysis of PEDOTh(Ni) gave Mn and Mw of about 1700 and 2400, respectively. PEDOTh-C6(Ni) showed a UV-Vis absorption peak at 546 nm in CHCl3. Electrochemical oxidation of PEDOTh-C6(Ni) started at about −0.40 V vs Ag+/Ag and gave a peak at 0.20 V vs Ag+/Ag. Chemical and electrochemical oxidation (or p-doping) of PEDOTh-C6(Ni), both in solutions and in a solid state, led to weakening of the original π-π∗ peaks and rise of new peak(s) in a region of 800-1500 nm. The p-doping of PEDOTh-C6(Ni) caused not only a decrease in the intensity of 1H NMR signals of the bridging ethylene hydrogens but also a decrease in that of the hexyl side chain, suggesting a strong interaction of the p-dopant with the side chain. NMR data of poly(3-methoxythiophene-2,5-diyl) also supported an assumption that p-doping brings about a severe change in electronic state of the substituent attached to the polythiophene main chain. PEDOTh(Ni) had a density of 1.71 g cm−3; the molecular packing mode of PEDOTh(Ni) is discussed based on the density of the polymer and its XRD data. 相似文献
997.
电流模式n阶传输函数的OA-OTA实现 总被引:1,自引:0,他引:1
马云辉 《固体电子学研究与进展》2002,22(3):294-296,360
提出了一种新的实现任意 n阶电流模式传输函数的网络结构。该电路仅含运算放大器 (OA)和运算跨导放大器 (OTA)有源器件 ,因而适于全集成。适当设置 OTA的跨导值能实现任意高阶传输函数 ,且传输函数的系数可独立调整。文中推导了滤波器的设计公式 ,并给出了截止频率为 1 0 0 k Hz的三阶巴特沃斯低通滤波器实例 ,PSPICE仿真结果表明所提电路及设计公式是正确的 相似文献
998.
999.
对完善公司物资供应管理体系的思考 总被引:6,自引:0,他引:6
王立平 《石油化工管理干部学院学报》2007,9(2):50-53
针对经“债转股”和资产重组成立的北京东方石油化工有限公司物资供应管理特点和存在的问题,从供应管理模式、采购方式、采购过程监控、信息化管理、物资储备、人员结构等6个方面,分析了目前供应管理存在的问题和不足,并针对问题通过对物资供应管理体制的分析和思考,提出对策,为新的物资供应体制的建立提供参考。 相似文献
1000.