Methacrylic acid–acrylamide-g-poly(ethyleneterephthalate) fibres for urea hydrolysis

This paper presents the results of urease immobilization onto methacrylic acid–acrylamide grafted poly(ethyleneterephthalate) fibres. The graft yield strongly affected the maximum activity of the immobilized enzyme up to a value of 70·2%. Higher grafting caused a decline in urease activity and led to the degradation of the fibres. The minor changes observed in K_m and V_max demonstrated that the conformational changes existed during immobilization were not extensive. However, 70·2% methacrylic acid–acrylamide-g-fibres containing urease were more stable towards acidic and alkaline pH, high temperature and storage conditions compared with free enzyme. Apart from the increase in stability to heat inactivation, the initial enzymatic activity of the urease–fibre system remained almost unchanged even after 40 repeated assays corresponding to 10 h of operation in 4 months, indicating the excellent durability of the system.     

大小样品在液氮中的淬冷沸腾换热比较研究

分析了大小样品在液氮中的淬冷沸腾换热特性。大小样品的淬冷沸腾换热有着明显的差别，小样品的热流密度比大样品的明显高得多。小样品的淬冷沸腾有一起始段，其温降高达６０Ｋ。从实验结果还可以看到，小样品的Ｌｅｉｄｅｎｆｒｏｓｔ点和临界热流点对应的壁面过热度明显比大样品的高。最后还分析了样品直径对临界热流密度的影响。     

电荷灵敏放大器不用反馈高值电阻的新方法

本文提出了一种电荷灵敏放大器不用反馈高值电阻的新方法。对这种方法作了电路分析以及对实际电路的测量结果作了介绍。     

Effect of site-selective substitution in bulk superconducting Tl2Ba2CaCu2O8

Magnetization measurements were carried out on bulk Tl₂Ba₂CaCu₂O₈ (referred to as Tl-2212) and on various site-selective substituted Tl-2212 samples. At 5K between 0 and 4.5 T, the 5 at. % Mg-doped Tl-2212 (Tl,Mg-2212) samples displayed enhanced pinning as demonstrated by a field dependent increase of the magnetic critical-current density J_c by 18 to 25 percent over that of pristine Tl-2212. Excess Mg (10–15 at. %), however, is deleterious. Rietveld refinement of the x-ray diffraction pattern showed Mg on the Tl sites. Auger electron spectroscopy analysis showed part of the Mg on grain boundaries. The flux-creep activation energies are higher for flux expulsion than for flux penetration in both Tl-2212 and Tl,Mg-2212 samples; the latter displays higher individual values. Our results demonstrate an increase in the number density of flux lines as a result of increased density of atomic-size-structural, defects by Mg (5 at. %) doping. In the Tl_2−yBa₂(Ca_1−zY_z)Cu₂O_8−x(z=0–0.3; single phase; x and y represent oxygen and thallium vacancies) system also studied, the T_c decreases as z increases. At z=0.3, the sample becomes an antiferromagnetic semiconductor.     

管杆漏磁探伤现场应用中的问题及对策

阐述了漏磁探伤漏磁场沿管、杆径向的分布特征 ,分析了影响探伤装置漏磁检测准确性的 4个因素 ,验证了信号提离距离的变化对传感器和探伤装置灵敏度的影响。针对在用的大多数浮动式传感器固定机构存在的两个严重缺点 ,提出采用自定位传感器固定机构 ,可消除机械装置对传感器灵敏度的影响。提出了一套标定和校验检测装置的方法 ,以保证探伤仪器的检测灵敏度始终恒定 ,提高检测结果的准确性和可靠性。     

波浪作用下空心块体稳定性分析初探

通过二维物理模型试验,探讨了暗基床上空心块体在规则波作用下的失稳模式。通过试验观察发现,当空心块体内有一定高度的填料时,波浪正向作用下空心块体首先倾覆失稳。本试验测量了作用在空心块体上的波浪力,并与同尺寸沉箱所受的波浪力进行对比,结果显示在波峰时空心块体所受的总水平波浪力比相同波浪作用下的沉箱所受力小而波谷作用下空心块体所受的总水平波浪力却比相同波浪作用下的沉箱所受波浪力大。鉴于上述实验观察结果,空心块体的主要失稳模式分析方法应作进一步研究。     

Influence of thermal boundary conditions on natural convection in a square enclosure partially heated from below

Natural convection in air-filled 2D square enclosure heated with a constant source from below and cooled from above is studied numerically for a variety of thermal boundary conditions at the top and sidewalls. Simulations are performed for two kinds of lengths of the heated source, i.e., a small and a large source corresponding to 20% and 80% of the total length of the bottom wall, respectively. The Rayleigh number varied from 10³ to 10⁷. Results are presented in the form of streamline and isotherm plots as well as the variation of the Nusselt number and maximum temperature at the heat source surface. Comparisons among the different thermal configurations considered are reported.     

强激光热斑形成及其稳定性研究

在论述热点跟踪及其传热机理时将靶材的比热溶、热传导系、在激光的热藕合系数均考虑成温度和时间的函数，又考虑靶材在运动时将激光辐照物体时热点的建立及其稳定情况作一动态数值模拟，为热点跟踪作准备。     

关于不确定对称组合系统的稳定化

研究不确定对称组合系统的二次稳定化问题,给出这类系统可二次稳定的一些充分条件 及计算反馈控制律的方法.这些条件的检验和反馈控制律的计算都由两个低阶系统关于相应 问题的求解来完成.     

正电子湮没技术在研究合金形状记忆性能中的应用

本文用正电子湮没技术测试了Cu-Zn-Al形状记忆合金100℃母相时效过程中空位的变化。结果发现,随着时效时间的延长,空位浓度不断降低,空位尺寸不断增大。这一结果很好地解释了记忆合金马氏体逆转变温度As的变化规律,从而证明过饱和空位是Cu-Zn-Al形状记忆合金马氏体稳定化的一个主要原因。