Effect of drag reducer and pour point depressant on the wax deposition of crude oil pipeline

In this paper, the data of wax precipitation before and after the addition of the additives showed that the addition of the drag reducing agent (DRA) and the pour point depressant (PPD) cannot change the wax appearance temperature (WAT) of crude oil. When the dosage of DRA is small, the DRA cannot increase, stop, or slow down the precipitation of wax crystals. The addition of PPDs has no influence on the amount of precipitated wax crystals. From the GPC analysis, the molecular weight of the wax deposit samples in Linpu pipeline is from 500 to 76,800, which indicates that there is no enrichment of DRA in wax deposit samples. The results of IR show that the C?O group was not detected in the wax deposit sample of the Wei Jing pipeline, which indicates that there is no enrichment of the PPDs in wax deposit samples. The results showed that the DRA and PPD have no obvious effect on crude oil pipeline wax deposition.     

Analysis for surface coke deposition in used Mo-Co/γ-Al2O3 catalyst for diesel hydrodesulfurization

The coked Mo-Co/γ-Al₂O₃ catalysts were Soxhlet extracted with the solvent of tetrahydrofuran. Experimental techniques like FT-IR, GC-MS, XPS, H₂-TPR, BET, etc. were applied for the characterization of coke and catalysts to make a comparison of their physical properties. The results showed that the active components of the catalyst were slightly less after the reaction. The specific surface area and the pore volume had recovered to some degree. These results indicated that the main cause of deactivation of Mo-Co/γ-Al₂O₃ catalysts is carbon deposit. The principal components of the soluble carbon deposit on Mo-Co/γ-Al₂O₃ catalysts were alkyl aromatics with 1–4 rings and C₁₉–C₂₉ long-chain alkane compounds.     

彩电合格焊点及其激光检测

激光／红外印制电路板焊点检测系统，是８０年代中期出现的世界上最先进的焊点质量检测手段，其检测速度、检测精度、检测可靠性和重复性、自动化程度，都是人工目视等其它方法远远不可比拟的。笔者对大量试验结果进行分析，可以认为：焊点激光红外检测数据、润湿角大小、焊点外形及抗拉强度数值、焊料重量值和合金层，可以作为判断焊点合格与否的标准。     

一种8毫米波变张角,半径突变多模圆锥馈源

我们研制了一种8毫米波变张角、半径突变的多模圆锥馈源。计算出其模比并推导出其辐射方向图公式;给出其在两个主平面——E平面与H平面上的辐射方向图和波束场分布特性的测试结果以及电压驻波比VSWR的测量结果;同时给出频带和旁瓣特性。分析与测试共同表明,在34.5GHz～37GHz频带里,该多模馈源的辐射图在大于24dB范围内获得幅度等化且不出现旁瓣,因此具有一定的应用价值。     

半球陀螺金属化膜层的均匀性模拟分析

该文将光学模拟技术与镀膜工艺结合,采用光线追踪程序来模拟溅射粒子在振子表面膜层的分布状态。通过模拟和相关实验验证,当设备相对角度β=10°、φ=60°时,振子表面膜层的均匀性最高,模拟值与实际测试值匹配度较好,误差在7%以内。     

Characterization of electrical properties and photosensitivity of SnS thin films prepared by the electrochemical deposition method

Using the electrochemical deposition (ECD) method, we prepared tin sulfide thin films, which are suitable for the absorption layer in solar cells because of its bandgap energy (1 eV). We first optimized pulse-form biasing for ECD by characterizing deposited samples with scanning electron microscope, Auger electron spectroscopy and X-ray diffraction measurements. Then, we investigated the electrical properties of deposited SnS thin films and the properties of contacts with several different metals. Furthermore, we observed the photoconductivity of the films by means of photoelectrochemical measurements. From these results, we confirmed that the SnS thin films show p-type conduction.     

Photo-rechargeability of film electrodes prepared by pulsed laser deposition

The film electrodes of TiO₂, which have two functions of opto-electric conversion and storage of electrochemical energy, were prepared by pulsed laser deposition. To investigate the relationship between the photo-rechargeability and the surface structure, the TiO₂ film electrodes with different surface morphology were prepared by changing the inert gas pressure during the deposition. The photo-charged quantity was found to be proportional to the third power of the rms of surface roughness. The results suggest that not only the surface but also the interstices between crystal grains near the surface contribute to the photo-charging with low photo-emf.     

Analytical characterization of cadmium cyanamide in CdS thin films and bulk precipitates produced from CBD process in pilot plant

CdS thin films and bulk precipitates were obtained by chemical bath deposition (CBD) in a well-closed reactor. X-ray diffraction spectroscopy, Fourier transform infrared spectroscopy, thermal analysis, elemental analysis and leaching have been used to characterize solids and thin films. It has been shown that the proportion of cadmium cyanamide in solids may vary from about 50% to 2% according to physicochemical conditions in solution (time after CBD, ammonia concentration) and that CdO results from CdCN₂ after air annealing of thin films. This last step also increases the crystallinity of the films.     

Design optimization of a large scale rooftop photovoltaic system

This paper presents the optimization process of a grid connected photovoltaic (PV) system, which is intended to replace a large-scale thermal solar system on the rooftop of a Federal office building. A PV energy conversion model is described. Based on this model, array surface tilt angle and array size are optimized. The optimization method is based on maximizing the utilization of the array output energy, and, at the same time, minimizing the electricity power sold to grid. An effectiveness factor is introduced that takes into account both of these parameters. The array configuration and the output parameters are determined by comparing several PV modules. A 43.2 kW PV system is designed and operational problems such as harmonic effects and anti-islanding are discussed. Finally, the system performance is simulated and through economic analysis it has shown that the cost of PV system can be recouped in 13 years under the current renewable energy incentive program by the state of Illinois.     

An experimental study of film cooling in a negatively bowed cascade with a large turning angle

Transverse measurements are carried out at the outlet of the straight and negatively bowed turbine cascades with a 106° turning angle respectively with and without cooling air injection. The air injection is from single or multiple rows of ten holes (26 schemes in all). Experimental results show that the negatively bowed cascade produces more energy loss than the straight one without cooling air injection. Cooling air injection from the holes on both the pressure and the suction surface near the trailing edge can reduce energy losses in both the straight and the negatively bowed cascades. The increase in loss is less in the negatively bowed cascade than that in the straight one with cooling air injection from holes of multiple rows at the leading edge, whereas cooling air injection from holes of multiple rows at the trailing edge reduces the energy loss in the negatively bowed cascade. © 2004 Wiley Periodicals, Inc. Heat Trans Asian Res, 34(1): 1–8, 2005; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/htj.20042