高炉法钙镁磷肥探料尺自动跟踪探料技术改造

针对钙镁磷肥生产中高炉探料存在的问题 ,对原自动探料装置的电气控制回路及跟踪装置进行改造 ,增加了探料跟踪最大极限位置 ,获得成功。改造后的自动跟踪探料尺 ,动作准确可靠 ,运行稳定 ,效率高 ,节能降耗 ,直接经济效益每年约 2 5万元 ,提高台时产量间接经济效益每年可达 4 0万元     

铝合金中锌、铁的快速测定--原子吸收分光光度法

样品以盐酸溶解，加入过氧化氢助溶，蒸至近干．加入1 1盐酸提取，移入100mL容量瓶中，分取部分溶液于50mL容量瓶中，调整盐酸酸度为5％，用水稀至刻度，摇匀后，以空气-乙炔火焰水相直接测定锌和铁。为了消除大量基体元素的影响，在标准系列中加入相当量的铝。此方法快捷、简便，亦可用于锰、镁、铜、铅、镍的测定。     

红外吸收法测硅铁中的超低硫

应用高频红外碳硫仪,建立了硅铁合金中超低硫测定方法,对选择适当的测定条件如助熔剂、分析时间等进行了探讨,最佳测定条件:最大工作电流为400～480 mA;载气纯度为99.99%;陶瓷坩埚需经1 100℃灼烧2 h后,可使空白降至最小;硫元素最短分析时间为40 s,比较水平为5.00.     

高吸油性树脂

高吸油性树脂是与一般吸油材料不同的自溶胀型新型吸油材料,它能够吸收从矿物油到天然油脂等各种油。目前国外正在用途、市场两方面进行系统开发。本文仅就其机理、特征、用途作简单介绍。     

一维炉系统的测试实验

一维炉是一种研究煤的热解燃烧和结渣等方面的实验系统,可用于模拟电厂煤粉的燃烧特性。以元宝山褐煤为燃料,介绍了一维炉的结构和功能,并对系统的可靠性进行了验证,利用烟气分析仪及热重分析仪对燃烧后的尾部烟气及灰渣进行了分析测定。结果表明:尾部烟气含氧量与灰渣可燃部分剩余量均在理论计算值的误差允许范围内,说明一维炉密封良好,系统内各部分正常运行,对维炉的调试和研究具有一定的参考意义。     

Dynamic buffering performance of the honeycomb paperboard filled with polyurethane

A new kind of composite buffering material was made by filling the voids of honeycomb paperboard with polyurethane. Drop tests were performed to evaluate the dynamic energy absorption capacity of the material. Based on the tests results, we analyzed the mechanical behaviors of the material under different conditions and obtained the inherent influencing laws of some factors on the material＇s dynamic buffering performance. It was shown that the dynamic buffering performance varied directly with impact velocity, and inversely with the void diameter, thickness and buffeting area of the composite material.     

铜离子印迹改性壳聚糖海绵的制备及应用研究

以醋酸铜为模板,甲醇、氯仿为溶剂,2-乙烯吡啶、丙烯酰胺为功能单体,乙二醇二甲基丙烯酸酯为交联剂,采用本体聚合法制备铜离子印迹聚合物;然后掺入到壳聚糖海绵的制备中,使壳聚糖海绵对铜离子的吸附率由27．1％提高到72．3％。制备的铜离子印迹改性壳聚糖海绵需要2d达到吸附平衡,吸附-解吸5次后,性能稳定。     

用含Pb、As、Sn地方生铁砂型铸造生产D型石墨铸铁的研究

基于Ph、As、Sn等元素有增大铁液过冷倾向的作用，利用含Ph、As、Sn的地方生铁，采用合金化和砂型铸造可以获得D型石墨铸铁，对其工艺方案进行了研究。用正交试验法设计试验方案，得到最佳工艺方案为：在亚共晶成分（WB％：3．2C，2．1si）的铁液中加入适量的铝（0．6％）和钛（0．8％），可以得到含有100％D型石墨的铸铁，其抗拉强度最高可达276MPa。     

High Temperature Oxidation of Steels in Air and CO2–O2 Atmosphere

Three kinds of hot rolled steel slabs, viz. high strength steel, bake hardened steel and low carbon steel, were oxidized isothermally between 1100 and 1250 °C for up to 2 hr in 1 atm of air and an 85%N₂–10%CO₂–5%O₂ gas mixture. The steels were oxidized in a similar fashion in both the atmospheres. The oxidation process followed an initial linear rate law, which then gradually transformed to a nearly parabolic rate law. Thick, porous and nonadherent scales formed rapidly, due to the high oxidation temperature. The scales formed consisted of Fe₂O₃,(Fe₂O₃+Fe₃O₄), (Fe₃O₄+Fe₂O₃ +FeO) and (FeO+Fe₃O₄) from the outer surface. The presence of supersaturated oxygen beneath the scale resulted in grain boundary oxidation and the formation of internal oxide precipitates.     

Solar furnace surface treatment of plasma-sprayed thermal barrier coatings

An original process of superficial thermal treatment is described. This process has been successfully applied to partially stabilized yttria-zirconia coatings (ZrO₂-Y₂O₃) to increase the lifetime of the thermal barriers. A thin superficial layer was melted, and morphological transformations were observed. A microstructural comparison between as-sprayed layers and thermally treated layers is presented.