一种制备磁性粉末的新技术--均匀颗粒成型法

采用均匀颗粒成型法（Uniform Dropler Spray-UDS）制备Fe基合金粉末，该方法制备的颗粒粒度分布均匀，性能一致，大大优于传统的粉末制备方法（如破碎法、气雾化），具有广阔的应用前景。本文分析了粉末制备过程中颗粒尺寸的影响因素，结果表明：颗粒的大小主要取决于坩埚底部小孔、坩埚内外气体压强差以及振荡频率三个独立变量。     

DT型粉状炸药专用蜡的研制

以多种含蜡馏分为基础原料，添加适量DT复合添加剂研制的DT型粉状炸药专用蜡具有优异的分散性和抗水性，可满足各种低梯粉状炸药要求，简化炸药配方，方便操作及其质量控制，以其生产的炸药爆速高，贮存期长，各项性能满足GB12437－2000标准要求。     

利用含钨废催化剂生产钨酸的工业实践

笔者较为详细地阐述了利用含钨废催化剂生产钨酸的工艺流程、各工序反应原理及其操作工艺实践、产品质量情况、原辅材料单耗等。实践证明 ,该工艺实用性强 ,具有显著的经济效益、社会和环保效益。     

Influence of Ti Powder Characteristics on Combustion Synthesis of Porous NiTi Alloy

Porous NiTi shape memory alloy (SMA) is a novel biomedical material used for human hard tissue implant .The influence of elemental titanium powder characteristics such as powder morphology, particle size and specific surface area( SSA) on the minimal ignition temperature ,combustion temperature and final product of porous Ni-Ti SMA fabricated by combustion synthesis method was investigated in this paper by scanning electron microscopy (SEM) and laser diffraction.The preliminary data indicated that the titanium powder characteristics had a strong effect on combustion synthesis of porous NiTi SMA.     

硅粉/酚醛制备低成本碳化硅陶瓷复合材料

以低成本的硅粉和酚醛为原料 ,采用浆料浸渍 热压成型 反应烧结法制备了Cf SiC单向板 ,并对工艺条件进行了探讨。制备得到的单向板的弯曲强度达到 45 6 .8MPa ,断裂韧性达到 7.94MPa·m1 2 。     

焦化干气一步法预处理多功能催化剂的工业侧线试验

对焦化干气一步法预处理工艺催化剂进行了工业侧线试验。考察了温度和体积空速对催化剂的活性及催化剂稳定性和加氢选择性的影响。催化剂为以复合型ZnO和过渡金属氧化物为活性组分的多功能催化剂,用于低温下焦化干气中烯烃加氢和硫化物脱除。试验结果表明,在压力1.6MPa、温度285～350℃、空速100～500h-1的条件下,多功能催化剂能将焦化干气中烯烃的体积分数由8%～14%降至0,总硫含量从10～70μg/g脱除至5μg/g以下;经28d考核,多功能催化剂仍保持良好的烯烃加氢和硫化物脱除性能,可用于精制焦化干气。     

Hazardous waste management problem: The case for incineration

We define the hazardous waste management problem as the combined decisions of selecting the disposal method, siting the disposal plants and deciding on the waste flow structure. The hazardous waste management problem has additional requirements depending on the selected disposal method. In this paper we focus on incineration, for which the main additional requirement is to satisfy the air pollution standards imposed by the governmental restrictions. We propose a cost-based mathematical model in which the satisfaction of air pollution standards is also incorporated. We used the Gaussian Plume equation in measuring the air pollution concentrations at population centers. A large-scale implementation of the proposed model within Turkey is provided.     

纳米NiO粉体的制备及其表征

采用溶胶转化－凝胶法制备了纳米级NiO粉体。Ni(OH)2粉体的TG－DSC分析表明：在升温速率为10℃/min的条件下，粉体在489K时开始显著分解，626K时分解完毕。X－射线衍射分析表明：分解产物为纯净的NiO2。NiO粉体的化学成分分析表明：其纯度高于国家标准。TEM电镜分析表明：NiO粉体呈单分散的球形或棒状颗粒。对NiO粉体的热敏性能有待进一步研究。     

锌精馏余热利用可行性探讨

本介绍了锌精馏精炼的简单原理、设备组成、余热资源及利用方案。     

Oxidation of porous nanocrystalline titanium nitride. II. Scale structure and composition

We have used x-ray phase analysis to study the composition of the products of reaction between oxygen and nanocrystalline powders with particle sizes 15, 40, 55, and 80 nm, and also specimens pressed (and sintered) from them. The powders were oxidized in air at 100°C (400 h) to 500°C (5 min), while the sintered specimens were oxidized at 600–900°C for 15, 120, and 240 min. In all cases, in the initial oxidation step the oxynitride Ti(O_xN_y) is formed, which over time is oxidized to TiO, Ti₂O₃, Ti₃O₅, TiO₂ (anatase) and TiO₂ (rutile). In the range 600–800°C, formation of a continuous oxide layer and conversion of anatase to rutile slows down diffusion of oxygen in the scale. We have established that at 900°C, the growth rate of the scale thickness increases and so the reflections from the oxynitride are barely noticeable on the diffraction patterns taken from the surface of the oxidized specimen. In these diffraction patterns, along with strong reflections from the rutile, we also observed weak reflections from lower oxides and anatase, which may be due to reaction between oxygen and the titanium ions diffused to the scale surface. We have concluded that at T > 850°C, the mechanism for oxidation of TiN changes. This is due to superposition of counterdiffusion of titanium ions on the diffusion of oxygen. __________ Translated from Poroshkovaya Metallurgiya, Nos. 3–4(448), pp. 72–78, March–April, 2006.