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A programmed temperature technique has been developed for the measurement of the self-diffusion coefficients of additives in polymers. This has been applied to the diffusion of three dialkylphthalate plasticizers in poly(vinyl chloride). Values of the self-diffusion coefficients and the calculated activation energies obtained in this way have been compared with values previously obtained from measurements at constant temperature. It has been shown that the programmed temperature technique gives a very rapid method for the estimation of the activation energy of self-diffusion. 相似文献
44.
Pellets containing metronidazole were produced in a centrifugal granulator, with hydroxypropylcellulose (Klucel LF®) as binding agent, and corn starch, microcrystalline cellulose (Vivapur 101®) and lactose as excipients. The wettability of the pharmaceutical powders was assessed by means of contact angle measurements, and the dispersive and polar surface energies were determined. The spreading coefficients, the work of adhesion and the work of cohesion were calculated and correlated with the pellet properties (friability, bulk and tapped density, and porosity). The aim was to investigate the role of the surface free energy of one- and two-component powder compositions in pellet production. The interactions between the particles were found to be connected with the measured pellet parameters. It was concluded that, in the course of the growth of the pellets, the particle sizes of the pharmaceutical powders and the interactions between them are important. If the work of cohesion of the binder is lower than the work of cohesion of the substrate and the work of adhesion, then the optimal amount of the binding agent is that which coats the particles uniformly in minimal quantity and in continuous layer. 相似文献
45.
应用粘弹谱仪考察了不同摩尔质量的聚酯(PET、PBT、PBT/PET)的动态力学性能,结果表明摩尔质量增大将提高其模量,但亦导致结晶速度变慢,使测得的模量反而比摩尔质量较低的试样小. 相似文献
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Satoko Abiko Yoshikazu Satake Xin Jiang Teppei Tsujita Masaru Uchiyama 《Advanced Robotics》2014,28(17):1177-1188
A hybrid motion simulator embeds a hardware experiment in a numerical simulation loop. However, it is often subjected to the inherent problem of an energy increase in the collision of two pieces of hardware in a loop because of the delay time. This paper proposes a delay time compensation method based on contact dynamics model for a collision hybrid motion simulator under delay time and establishes a compensation method for coupled translational and rotational motion. The model developed in this paper describes linear uniform motion of a floating object during the period of the delay time until the force and torque are observed and non-linear motion according to environmental stiffness after the initial delay time period in contact. By using the above model, compensation parameters are designed based on desired coefficient of restitution with iterative calculation. The proposed method achieves accurate delay time compensation and simultaneously realizes a variable desired coefficient of restitution over a wide range of frequencies. Furthermore, the compensation method for multi-dimensional motion is established under the assumption that the friction effect is very small. The efficiency of the proposed method is verified through collision experiments for the coupled motion in two dimensions. 相似文献
48.
针对综合交通网络评价指标权重及属性值具有主观性和随机性的特点,提出了基于模拟运算的布局规划方案排序选优的群体随机决策方法.仿真生成满足集结的多个专家对指标重要性偏好排序统计分布的权重,同时考虑交通需求的不确定性对指标值的影响,结合客观熵权计算方案的综合评价值,由多次模拟得到的排序优势度确定方案的优劣差异.根据设计的仿真流程通过算例说明了方法应用的有效性,评价中考虑了主客观因素及随机性特征,可以为网络布局提供科学决策依据. 相似文献
49.
模拟三相流化床中颗粒尺寸对单气泡传质系数的影响 总被引:1,自引:0,他引:1
本文在模拟三相流化床中,测量了单气泡的传质系数,实验结果表明颗粒直径对气-液传质系数影响显著。颗粒直径较大时,传质系数有明显提高。 相似文献
50.
基于全网能量均衡的WirelessHART图路由算法 总被引:1,自引:0,他引:1
如何均衡使用网络节点能量并生成高可靠路由是WirelessHART网络研究的一个难题,为此提出了一种GRAEB(graph routing algorithm based on energy balancing)图路由算法。首先,网络被初始化为连通的图结构,能够提高丰富的冗余路径。网络管理器根据全网节点剩余能量、通信周期、链路分布等因子生成节点鲁棒系数矩阵,节点通过比较邻居的鲁棒系数来选择最优路径。另外,规定了邻居节点数的上限阈值,每次路由更新只保留鲁棒系数最优的邻居。仿真结果表明GRAEB不仅提高了网络可靠性,而且延长了网络寿命。 相似文献