如何延长高压液相色谱柱的使用寿命

分析了液相色谱柱失效的诸多现象和原因，并论述了极性溶剂冲洗法等一些使色谱柱恢复活性的方法。     

Phase equilibria in InAsSbP quaternary alloys grown by liquid phase epitaxy

The quaternary alloy InAs_1−x−ySb_xP_y, lattice-matched to InAs, is a promising material for the production of infrared light sources for the detection of gases in the 2–4 μm region of the spectrum. In this work, thermodynamic phase equilibrium calculations have been carried out to determine the compositions required for liquid phase epitaxial growth and the extent of the miscibility gap in the solid material. For high band gap materials, the desired growth temperature is found to be intermediate between a low temperature required to grow P-rich solids and higher temperatures required to avoidspinodal decomposition. Conventional LPE growth at an intermediate temperature of 583°C is found to produce good material with high luminescence efficiency and excellent optical characteristics. Problems with phosphorus loss from the melt are also discussed and lower growth temperatures are found to considerably reduce this problem. Growth in the metastable region between the binodal and spinodal lines has been achieved with the production of phosphorus-rich solids with concentrations up to y = 0.445.     

MIS型单晶硅液晶光阀

详细介绍了一种新颖、快速响应的金属－绝缘层－半导体构成的MIS型单晶硅液晶光阀的结构、工作机理、制作工艺和性能参数测试。液晶采用45°扭曲向列型混合场效应工作模式。所得到的光阀的极限分辨率为40lp／mm，口径40mm，最大对比度＞100：1，在930nm（△λ＝40nm）写入光灵敏度为20μW／cm2，响应时间为15ms。报道了该光阀在大屏幕投影显示中的应用。     

热致液晶性纤维素衍生物及其热塑性塑料复合物熔体流变行为的研究

用毛细管流变仪研究了乙基纤维素（ＥＣ）及其高密度聚乙烯（ＨＤＰＥ）复合物，纤维素芳族酯（ＣＡＥ）及其聚碳酸酯（ＰＣ）复合物的剪切流变特性和机理。结果表明，ＥＣ对ＨＤＰＥ／ＥＣ复合物的粘度影响不大，而少量（５％）ＣＡＥ的加入使ＰＣ／ＣＡＥ复合物粘度大大下降，且复合物流变曲线呈现新的特征。     

Two dimensional deformation characteristics of bloom CC with liquid core reduction

A two-dimensional model was applied to simulate the liquid core reduction(LCR) technology of bloom CC using ANSYS software.The deformation characteristics of bloom under different liquid fraction and reducing amount are obtained.The results indicate that the main deformation condition of bloom shell is compressive strain,mainly undertaken by the liquid core,which increases with the enhancement of reducing amount.Solidified shell takes minor deformation.The longitudinal section of bloom appears sunken and the narrow side bulges,which grow serious when the liquid fractionincreases.     

胆甾相液晶的光学特性

基于胆甾相液晶的特殊分子结构，综合阐述了胆甾相液晶的旋光性、选择性光散射和偏振光二色性等光学特性，揭示了它的光学特性主要源于它螺旋状的分子结构及其光学各相异性。     

高合金铁基烧结材料在轧钢导位中的应用研究

本文研究了高合金铁基烧结材料在轧钢导位中的应用。实验表明,通过粉末冶金液相烧结技术,可以获得具有优良综合性能的制品,材料密度ρ≥7.5 g/cm3,硬度≥55 HRC,抗弯强度≥1 000 MPa,冲击韧度αk≥3.9 J/cm2,满足了轧钢导位辊的工作要求。材料利用率可达95%以上、降低了制备成本。使用寿命是普通轧辊寿命的3~6倍,适用于线材和小型型材的轧钢生产。     

铸件浸渗系统脱液机故障树的建立和分析

利用FTA方法对脱液机的各种故障进行系统分析,建立了脱液机的故障树,并对故障树进行定性分析.找出了影响脱液机可靠性的主要因素,提出了提高脱液机可靠性的相应措施.     

固液相变蓄能的数学模型和自然对流换热系数的实验研究

引入自然对流换热系数 ,将固液蓄能数学模型简化为仅用能量方程加以描述。并通过实验测得相变过程的实际温度场 ,证明了自然对流固液相变换热的影响不可忽略 ,验证了固液相变界面移动速率随自然对流换热系数的增大而增大的定性关系     

Liquid crystalline polymers as additives to enhance the device properties of low molecular mass liquid crystals

Magnetic and electric fields have been used to determine the splay (k₁₁) and bend (k₃₃) elastic constants in a series of polymer/monomer liquid crystal solutions using the well known Freedericksz transition technique. Measurements have been carried out as a function of concentration and temperature. The polymer used was a smectogenic polysiloxane side chain liquid crystal with both cyanobiphenyl and benzoate ester side groups. The monomeric solvent was the nematogen 4-n-pentyl-4′-cyanobiphenyl. All of the solutions studied were nematogenic up to a concentration of 40% w/w. It has been shown that k₁₁, k₃₃ and $\text{k}{}_{33}\text{k}{}_{11}$ all decrease with increasing polymer concentration and that at high enough concentrations $\text{k}{}_{33}\text{k}{}_{11}$ tends to become independent of temperature. The implications of these results are discussed in terms of the performance of the most common liquid crystal display, i.e. the twisted nematic device.