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Jing BI Zongyi MA Shengjin WU Yuxiong LU Hongwei SHEN Institute of Metal Research Academia Sinica Shenyang China 《材料科学技术学报》1993,9(1):61-64
The microstructure and tensile properties of Al_4C_3 dispersion strengthened Al composite fabricatedby reaction milling technique were investigated.It is indicated that the rod-like Al_4C_3 dispersoidshaving a diameter of 0.02-0.03 μm and a length of 0.1-0.3μm are formed by reaction of C with Al,and uniformly distributed in the Al matrix.The interface between Al_4C_3 and Al is clean and theinterfacial bonding is good.The matrix consists of the subgrains which have the size of 0.3-0.4μm,and most of the Al_4C_3 dispersoids are distributed on the subgrain boundaries.The 11 vol.-%Al_4C_3/Al composite exhibits an UTS (ultimate tensile strength) of 400 MPa and anelongation-to-failure of 8.0%. 相似文献
74.
将薄膜电容真空计的测量室接于被测密闭容器,静态真空室接于一个比较容器,即组成一台压差式漏率测试仪。首先使两容器压力平衡,真空计读数为零。当被测容器存在漏孔时,真空计薄膜两侧形成压差,真空计指示读数,继而计算出该容器的漏率。应用商品真空计在抽真空测试时,检测的最小可测漏率达10-4~10-5Pa·L/s;而在充压测试时,因受气体温度变化的影响,灵敏度会降低几个量级。该仪器有可能具备寻找漏孔位置和确定漏孔漏率的功能。 相似文献
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Shizuo Arichi Noriyuki Sakamoto Shozo Himuro Mayumi Miki Masafumi Yoshida 《Polymer》1985,26(8):1175-1180
In order to obtain the additional data concerning the unperturbed dimension of poly-4-substituted styrene, light scattering measurements are performed on the twenty-two fractions with molecular weight of (0.91–352)·104 of poly(4-acetoxystyrene) in dioxan at 25°C, from which the molecular weight obtained was found easily to be evaluated with the gel permeation chromatography using THF. Phase separation experiments for this polymer indicate that the theta state is attained in isopropyl acetate at 19.7°C and butyl acetate at 26.8°C. By making viscosity measurements at that state, the value of KΘ is directly evaluated as 5.4·10?4 dl g?1. The limiting viscosity number is also obtained in good solvents, THF and dioxan, at 25°C and constants of the Mark-Houwink-Sakurada equation in each solvent are determined. Further, approximately the same KΘ as above is obtained from these data with the Stockmayer-Fixman plot. The calculated value of steric factor, 2.37, on this polymer may be plausible, compared with those of polyvinylaromatic derivatives. 相似文献
77.
Critical-point drying and freeze drying were compared both quantitatively and qualitatively as preparative procedures for scanning electron microscopy. Isolated hepatocytes were used as model cells. Nomarski differential interference contrast microscopy was used for light microscopic measurements of the hepatocytes in the unfixed, the glutaraldehyde fixed, the glutaraldehyde + OsO4 fixed, the critical-point dried and the freeze dried states. Critical-point dried hepatocytes were found to shrink to 38% of glutaraldehyde + OsO4 fixed volume, whereas optimal freeze dried hepatocytes (frozen in water saturated with chloroform and freeze dried at 183 K for 84 h) were found to shrink to 51% of glutaraldehyde + OsO4 fixed volume. Transmission and scanning electron micrographs of the critical-point dried cells showed well-preserved ultrastructure and surface structure. Micrographs of the freeze dried cells showed ultrastructure destroyed by internal ice crystals and surface structure destroyed by external ice crystals. Double-fixed isolated hepatocytes were shown to swell during storage in buffer and to shrink during storage after critical-point drying. For low magnification scanning electron microscopy (up to about 3000 times) both critical-point drying and freeze drying can be used. However, for high magnification scanning electron microscopy, critical-point drying is superior to freeze drying. 相似文献
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介绍了质量流量计的工作原理有应用效果。这种新型质量流量计精度高,稳定性好,示值计量简便,可直接显示质量、流量、介质温度、密度等,维护量低,但必须正确安装、使用,才能发挥其应有的作用。 相似文献
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