基于硼酸溶液处理的GaAs/InP低温晶片键合技术

提出了一种基于硼酸溶液的GaAs/InP低温晶片键合技术,实现了GaAs/InP基材料间简单、无毒性的高质量、低温(290℃)晶片键合。GaAs/InP键合晶片解理截面的扫描电子显微镜(SEM)图显示,键合界面整齐,没有裂缝和气泡。通过键合过程,InP上的In0.53Ga0.47As/InP多量子阱结构转移到了GaAs基底上。X射线衍射及荧光谱显示,键合后的多量子阱晶体质量未变。二次离子质谱(SIMS)和Raman光谱图显示,GaAs/InP键合晶片的中间层厚度约为17 nm,界面处B元素有较高的浓度,键合晶片的中间层很薄,因此可以得到较好的电学、光学特性。     

A novel method for evaluating fatigue properties of bonding layers used in bridge deck pavement

A new method was used to evaluate the fatigue properties of the bonding layer used in the bridge deck pavement. The shear fatigue test of three bonding layers was conducted on a dynamic shear rheometer(DSR). The fatigue formulas were gained for these layers. The experimental results indicate that, at the same torque level or at the same frequency, neoprene latex asphalt bonding layer exhibits excellent fatigue performance when compared to other two bonding layers. Funded by the National Natural Science Foundation of China (No. 50878171)     

低温促染剂的制备及在羊毛染色中的应用

采用丙烯酸类、硅类化合物合成制备了一种低温促染剂,并分别应用于羊毛纤维的低温染色和常规沸染,测试了上染率、皂洗牢度、摩擦牢度等技术指标. 结果表明:在85 ℃下染色,当促染剂用量为1.5%(o.w.f)时,染料上染率、色牢度等指标均达到常规沸染水平,而纤维损伤则大大低于常规沸染.     

空冷器复合管束力学建模和数值模拟

对加氢空冷器复合管束进行结构分离和解析,根据弹塑性力学方法获得复合管的力学分析控制方程,对内衬316L不锈钢的复合管进行应力场数值模拟,比较弹性力学和有限元数值模拟方法得到的应力分析结果相互吻合;分析复合管的极限工作载荷以及运行工况下的热应力,提出以结合强度为空冷器复合管束检验的指标,并对实际制造的复合管样品进行结合强度测试,结果满足相关国家标准,工程应用实现了设备长周期运行.     

兆瓦级风电球铁件低温冲击韧性的影响因素

为了获得具有良好低温冲击性能的兆瓦级风电球铁铸件,对实际生产中的附铸试件-20℃ V型缺口冲击性能进行了测试,并对其成分、基体组织、石墨球大小及分布情况进行分析,研究了兆瓦级风力发电机组球铁件低温冲击韧性影响因素.结果表明：在低P、S的前提下,通过合理的熔炼工艺控制,终Si量在2.3%时可以使单位面积的石墨球数量增加,石墨球细小,低温冲击值最佳;Mn在0.2%~0.3%之间变化时对低温冲击韧性影响并不明显;基体组织中珠光体在5%以下时,低温冲击值无明显变化,珠光体大于12.5%时,低温冲击值急剧下降.     

电弧喷涂锡基巴氏合金层的磨损性能

针对电弧喷涂巴氏合金涂层组织的特殊性,研究在润滑条件下巴氏合金涂层的摩擦磨损性能,对该涂层的工程应用具有重要的参考价值.利用环块摩擦磨损试验分别对比了电弧喷涂、铸造以及堆焊方法制备的巴氏合金层与碳钢和铸铁构成摩擦副的磨损表现.借助于扫描电子显微镜、x 射线能谱以及x 射线衍射,分析了巴氏合金涂层的微观组织结构和磨损表面形貌,研究了其组织变化与耐磨性能之间的关系.实验结果表明：在润滑条件下,电弧喷涂巴氏合金涂层具有比铸造巴氏合金更好的减磨性能;选择合适的工艺参数可以制备组织致密、结合强度高,且具有很好磨损性能的巴氏合金涂层.     

Effect of Curing Regime on Bonding Strength of EVA Modified Mortar to Tile

Ethylene-Vinyl Acetate (EVA) redispersible powder and latex were used to modify mortar. Three kinds of curing regimes: standard curing, high temperature curing and freeze-thaw circle curing were adopted to cure the bonded samples. Bonding strength of EVA modified mortar was tested at 28 days. The development of bonding strengths under all three curing regimes were discussed and compared. The experimental results show that bonding strength increases with the increase of EVA content in mortar. The curing regi...     

再生混凝土骨料应用于沥青路面的路用性能试验

为了将再生混凝土用于骨料沥青混合料,提出了再生混凝土骨料应用于沥青混合料时最佳沥青含量的估算方法,并运用马歇尔试验予以验证,试验结果与本文建议的理论估算值吻合较好.试验还研究了不同再生混凝土骨料掺量下的沥青混合料的高温稳定性、低温抗裂性和水稳定性,分析了影响各项性能指标的因素和原因.结果表明:再生混凝土骨料沥青混合料的各项路用性能均满足国内规范要求.     

Oxidation and Fracture Strength of High-Purity Reaction-Bonded Silicon Nitride

Reaction-bonded Si₃N₄ (RBSN) made from high-purity Si powder is unusually resistant to degradation caused by exposures to air for up to 50 h at temperatures up to 1400°C. The weight gain during oxidation of this SiH₄-originating RBSN is approximately 10 times less than conventional RBSN. Contrary to normally observed strength degradations, room-temperature strengths of this high-purity, oxidized RBSN (avg = 435 MPa, max. = 668 MPa) remained at their unusually high, as-processed levels after 1000° and 1400°C oxidizing exposures. Fracture toughness values were unaffected by oxidation ( K _IC= 2.3 to 2.4 MPa · m^1/2). This superior oxidation resistance results from the high purity and the small diameter pore channels (0.01 to 0.06 μm) achieved in this SiH₄-originating RBSN.     

CO变换催化剂的研究进展

介绍了国内外CO中(高)温变换催化剂、低变催化剂及耐硫变换催化剂的现状及研究进展。高效节能型变换工艺将是变换工艺的发展方向,开发低温、高活性和稳定性的变换催化剂将相应成为研究的主要目标。