Estimation of true dihedral angles and relative grain boundary energies in polycrystals using the disector

Relative grain boundary energies can be simply related to true dihedral angles, which are the angles between grain boundary planes meeting at triple edges in polycrystals. Some limited efforts in the measurement of true dihedral angles have used the technique of serial sectioning, which is usually cumbersome and time consuming. In this study the three‐dimensional probe called the ‘disector’ has been employed to evaluate true dihedral angles. This probe, combined with automated image processing, introduces precision as well as efficiency, overcomes the disadvantages of the two‐dimensional probe and is far less tedious and less complicated than serial sectioning. It is shown that the technique is relatively simple and therefore can be applied to obtain a significantly large and accurate statistical sample of true dihedral angles. The application of this method is demonstrated by evaluating the triple junction geometry and the associated relative grain boundary energies in polycrystalline 316L austenitic stainless steel.     

Surface designing of polypropylene by critical monitoring of the grafting conditions

The grafting of acrylic acid onto electron beam‐irradiated polypropylene was carried out using preirradiation method. The stability of peroxy radicals was investigated by electron spin resonance. It was found that the decay of peroxy radicals is much faster at 70°C than at 40°C and ambient temperature. The grafting has been observed to be strongly dependent on the monomer dilution in the reaction medium. The grafting was ascertained by attenuated total reflectance (ATR). The distribution of grafts across the samples was monitored by infrared microscopy. It was found that the graft management is considerably influenced by composition of the grafting medium. The grafting involving pure monomer leads to the surface enrichment with the polyacrylic acid chains. The samples grafted in pure monomer led to much lower contact angles as compared to the diluted monomer solution. The swelling of the grafted samples also showed a trend that was governed by the graft management. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 546–553, 2006     

舰船导航信号发生器虚拟化设计

介绍了基于PC总线的便携式舰船导航信号发生器虚拟化设计，着重叙述该仪器硬件设计、基于虚拟仪器开发平台LabWindows／CVI的软件设计。     

Structural and magnetic properties of Co1+ySnyFe2-2y-xCrxO4 ferrite system

The samples of the series Co_1+ySn_yFe_{2- 2y- x}Cr_xO₄ ferrites with x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 and y = 0.05, were prepared by the usual double sintering ceramic technique. The single- phase spinel structure of the samples was confirmed by using X- ray diffractometry technique. The lattice parameter ’a’ with an accuracy of ± 0.002 Å were determined using Bragg peaks of XRD pattern. The lattice parameter ’a’ decreases with concentration, x, which is due to the difference in the ionic radii of Cr³⁺ and Fe³⁺ ions. The X- ray intensity calculations were carried out in order to determine the possible cation distribution amongst tetrahedral (A) and octahedral [B] sites. The X- ray intensity calculations show Cr³⁺ ions occupying B site. The saturation magnetization, σ_s, and magneton number, n_B (the saturation magnetization per formula unit), measured at 300 K determined from high field hysteresis loop technique decrease with increase in concentration, x, suggesting a decrease in ferrimagnetic behaviour. Thermal variation of low field a.c. susceptibility measurements from room temperature to about 800 K exhibits almost normal ferrimagnetic behaviour and the Curie temperature, T_C determined from a.c. susceptibility data decreases with increase in x.

     

基于AutoCAD2000的图解法确定工艺转角

提出了基于AutoCAD2 0 0 0的图解法求解机械加工过程中工艺转角的问题 ,并针对具体的应用实例给出了圆满的解答 ,并验证了其精度。     

一种新型悬臂棒条筛的设计与应用

介绍了一种新型悬臂棒条筛分机械,论述了其结构、工作原理和技术特性。从理论和实践两方面论证了它的结构、处理能力、筛分效率、返矿率都明显优于普通悬臂棒条筛分机械,可广泛应用于高炉槽下烧结矿的筛分作业。     

保证跌落试件姿态的方法

进行包装件的自由跌落试验时,必须保证试件姿态符合标准规定。笔者在实践中总结出一种保证试件姿态和检验试件姿态误差的具体方法。     

Thermogravimetry and wide angle X-ray diffraction study on the structure of irradiated and thermally treated kodar film

The degradation behaviour of Kodar [poly(1,4-cyclohexylene dimethyl-eneterephthalate)] was investigated in air using thermogravimetry, differential thermal analysis and wide angle X-ray diffraction studies. The rates of crystallization and degradation were influenced by thermal exposure and polychromatic irradiation (Λ > 290 nm) for different time intervals. The crystallinity changes (X_c%) and activation energies (ΔE) for the systems have been determined.     

轴测投影非轴向伸缩系数及与轴测轴的夹角

导出了正轴测图中投影面平行线的伸缩系数及其与轴测投影轴的夹角计算公式,使得各种形状形体的轴测投影画法更简单、尺寸量取更精确.     

覆膜滤料的滤尘性能测试方法研究

由于覆膜滤料的结构和性能有别于普通滤料，因而普通滤料的滤尘性能测试方法不完全适用于覆滤料。本文作者在总结实践经验的基础上，提出了在覆膜滤料的滤尘性能测试中应注意的一些问题和应增加的测试项目。