丙烯酸2-乙基己酯与醋酸乙烯酯共聚合成高吸油性树脂的研究

以丙烯酸2－乙基己酯与醋酸乙烯酯为单体，采用悬浮聚合法，以单体自交联制得高吸油性树脂。对影响其吸油性能的多种因素，如单体配比、引发剂、油水相比的用量等，进行了系统的研究，得到的高吸油性树脂吸苯最高达16．1g/g，吸甲苯为14．8g/g，吸环己烷为13．3g/g，吸煤油为12．5g/g，可用于河面、海洋浮油的回收及工厂废水处理等领域.     

哈尔滨炼油厂MTBE装置试生产

介绍了哈尔滨炼油厂ＭＴＢＥ装置的工艺路线、新技术的应用及特点；催化剂的装填及应用情况；总结了生产过程中遇到的一系列问题及解决办法；探索了平稳生产的新徐径，以保证装置安全、平稳、长周期运行；同时对反应器操作温度、催化蒸馏塔操作压力、原料中醇烯比等因素对异丁烯转化率及ＭＴＢＥ产品的影响做了简单的总结。     

Measurements of Stress Intensity Factors of an Interface Crack Under Mixed Mode Loading

The optical method of caustics has been utilised to measure both the stress intensity factor for a crack lying along the interface of an aluminium/epoxy bimaterial specimen, and the mode mixity arising from the difference in the elastic properties across the interface. Measurements were carried out by using a novel modification to the method whereby caustics are produced and measured from both sides of the specimen, so compensating automatically for the distortion induced in the specimen due to misaligned loading fixtures. A flat reflective surface across the interface was obtained by adhering a reflective coating to the specimen. Verification that this coating does not affect measurement accuracy was obtained by comparing stress intensity factors measured from coated and uncoated monolithic aluminium specimens where good agreement was found to exist between both measurements.     

Estimation of bacterial production through the coupling of (methyl 3H) Thymidine incorporation and several parameters over a Microcystis aeruginosa bloom in a hypereutrophic reservoir

The coupling of the changes in bacterial quantitative and metabolic aspects during Microcystis aeruginosa bloom conditions together with several environmental parameters was studied in the hypereutrophic Villerest reservoir, France. Bacterial abundance varied from 5.20 to 21.28 × 10⁶ bacteria-mL^?1, while bacterial biomass ranged between 75 and 507 μg C mL^?1. These results confirmed the highly eutrophic status of the Villerest reservoir. The relative quantitative importance of attached bacteria increased as Microcystis proliferated. Methyl-³H incorporation and D-(U-¹⁴C) glucose uptake varied from 8.99 to 60.57 × 10⁶ cells-mL^?1, and 0.016 to 1.587 μg CL^?1 h^?1, respectively. Correlations between several abiotic and biotic parameters showed that phytoplankton regulated bacterial growth by releasing organic carbon which is directly uptaken by heterotrophic bacteria. In the hypolimnion, the sedimentation of decaying algae represented a substantial substrate for bacterial growth.     

Dielectric Resonators for the Measurement of Superconductor Thin Films Surface Impedance in Magnetic Fields at High Microwave Frequencies

We present the design and realization of cylindrical dielectric resonators operating in the 40–60 GHz frequency range, designed for the measurement of the surface resistance and of the surface reactance shift in High-T _c Superconductors (HTS) thin films in a dc magnetic field. The resonators are single tone, based on the TE ₀₁₁ mode, and multiple tone, the latter allowing in principle to exploit the simultaneous determination of the surface impedance at different frequencies. As an application example, we report the temperature and field dependencies of the effective surface impedance of some cuprate superconductors thin films. The results are compared with those obtained through the use of a standard metal cavity with a similar Q-factor and operating in the same frequency range. The comparison highlights a superior stability and a higher sensitivity, resulting in an increase of about two orders of magnitude in the resolution of the surface impedance measurement. By contrast, the dissipative part of the superconducting transition (above T/T _c = 0.97) is better studied with the metal cavity. We also present measurements in the vortex state in YBaCa₂Cu₃O_7−δ and Tl₂Ba₂CaCu₂O_8+x that show significantly different physics. PACS: 74.25 Nf.     

催化裂化原位降硫助剂的制备及其性能研究

采用溶胶-凝胶法制备具有介孔结构的降硫基质材料，选择具有降硫选择性的活性元素对合成的基质材料进行改性处理，考察不同的改性方法对制得的催化裂化原位降硫助剂性能的影响，并对基质材料和降硫助剂的结构进行表征。采用美国进口的ACE-R小型催化裂化评价装置将降硫助剂与催化裂化催化剂匹配进行性能评价，在不改变原催化裂化产品分布和产品性质的同时，降低原料的总硫含量，总硫降低可达40％以上。     

一种抗干扰能力极强的计算机通信接口电路

设计了一种结构简单，抗干扰能力极强的计算机通信接口电路。该电路利用模拟开关实现了全数字二态电平（1，0）与三态电平(1，0，-1)之间的相互转换；利用模拟开关导通电阻的动态效应以及MOS晶体管开启电压Vτ的衬偏效应，提高了接收电路的抗干扰能力，提出了一种与共模干扰无关的模拟数字混合接收电路。     

树脂悬浮光度法测定微量银

在ｐＨ６．９的缓冲溶液中，银与硫代米Ｃｈｉ酮（ＴＭＫ）形成的螯合物在树脂甘油相中悬浮富集，用光度法测定银在波长４６１ｎｍ处有最大吸收，银在０～６μｇ／１０ｍＬ范围内遵守比尔定律，可用于样品中微量银的测定。     

Kinetic analysis for effect of initial substrate concentration on growth and secondary metabolite production in cultures of Nicotiana tabacum

Suspension cultures of tobacco cells were studied using airlift and rotary-drum bioreactors. The effect of initial concentrations of a major substrate, sucrose, on the growth and production of a secondary metabolite, phenolic compounds, was investigated. The dry weights and total concentrations of the phenolic compounds increased with the initial sucrose concentration in both bioreactors. Both bioreactors were found to have the same tendency for the effect of initial sucrose concentration. The structured model, presented previously was modified by considering that sucrose was hydrolyzed to glucose and fructose by an enzymatic reaction. The previous and the new models were applied to the above two sets of experimental data obtained with two bioreactors, independently. The hydrolysis of sucrose was elucidated to contribute slightly to the overall kinetics of growth and secondary metabolite production in these cultures. Furthermore, the levels of shear damage in each bioreactor were quantitatively compared based on the death rate constant, k_i, which is one of the model constants.     

Design of a robust controller for a supersonic aircraft using H∞ approach

In this paper an H_∞ optimal, robust flight control system design for a supersonic aircraft has been described. Separate controllers are designed for longitudinal and lateral motions. A general two-degrees-of-freedom controller is proposed, where feedback control is designed for robust performance augmentation, while a series compensator is used to ensure that requisite handling qualities. Three alternative methods to achieve performance robustness have been discussed. The results obtained are very encouraging. It is hoped that this will equip the flight control engineers with an alternative to the conventional methods.