超声监测技术在膜分离过程中的应用研究

在膜分离过程中，膜通量总是随运行时间而下降．为了区分膜污染与浓差极化或者可能的膜形变对通量的影响，和选择适宜的清洗过程，对一种只敏感于膜表面状况的超声测量方法进行了广泛研究．通过平板膜(包括微滤膜、超滤膜和反渗透膜)以及卷式反渗透膜过程的应用实例，说明了这种实时、在线的超声时域反射法即Ultrasonic Time-Domain Reflectometry (UTDR)可以利用它的反射波的振幅和回声抵达超声传感器的时间来监测浓差极化、膜污染(例如CaSO4污染)与清洗过程，也可以用来测量膜的压紧度和污染层厚度．超声测量与传统膜性能测量结果有良好的关联，并具有区域性测量的特性．为了实用化目的，新近的研究进展也作了介绍．     

Enantioseparation of catechin and epicatechin in plant food by chiral capillary electrophoresis

The enantiomers of catechin and epicatechin were separated by chiral capillary electrophoresis using modified cyclodextrins as chiral selectors. Various conditions for the separation system were optimized, including the pH value and the concentration of the running buffer. A baseline separation of the catechin and epicatechin enantiomers could be achieved by using 0.1 mol l⁻¹ borate buffer (pH 8.5) with 12 mmol l⁻¹ (2-hydroxypropyl)-γ-cyclodextrin as chiral selector, a fused-silica capillary with 40 cm effective length (75 μm I.D.), +18 kV applied voltage, a temperature of 20 °C and direct UV detection at 280 nm. The method was applied to different plant food samples. (+)-Catechin and (−)-epicatechin could be verified as the most common flavan-3-ols. In the case of guaraná, however, we were able to identify all four enantiomers, both (+)- and (−)-catechin and (+)- and (−)-epicatechin, as naturally occurring compounds. This finding was verified by further isolation and purification of the flavan-3-ols and subsequent LC–MS analysis. This method allows for the identification of the authenticity of guaraná through the analysis of the catechin and epicatechin enantiomers, additionally to the conventional methods like HPLC.     

离心机流场非稳态过程的初步数值模拟

摘要：从非稳态线性离心机流场运动方程出发，利用有限体积法，采用交错网格得到离散方程。通过数值求解得到了存在温度驱动情况下，离心机内形成小扰动流场的过程。从形成小扰动流场的非稳态过程可以看出扰动流场在开始和稳定阶段的影响因素不同，从温度引起的轴向压强的不平衡引起流动逐渐过渡到压强分布不同而引起的轴向环流。数值模拟为更好地研究离心机内流场的非稳态过程提供了依据。     

Performance Characteristics of a Drying Heat Pump Using Superheated Steam

A complete mathematicalhumerical model is proposed, in order to simulate the performance characteristics of a novel concept of a drying heat pump based on the theory of minimum energy cyclcs. The drying heat pump involvcs vapour condensation in a Lava1 nozzle. removal of the liquid phase in a supersonic separator as well as compression of the working medium. which is superheared vapour.     

Study on phase behavior–impact strength relationship of unsaturated polyester/polyurethane hybrid polymer network

The phase behavior of a hybrid polymer network (HPN) composed of poly[(propylene glycol maleate)-co-(propylene glycol phthalate)] crosslinked with styrene and polyester–urethane crosslinked with methylene-bis-ortho-chloroaniline was examined. The correlation between phase separation and impact strength of the HPNs is discussed. The composition of HPNs has an effect on their properties.     

K_2O－B_2O_3－SiO_2玻璃成分对析晶性能的影响

本文利用ＤＴＡ、ＸＲＤ、ＴＥＭ、ＳＥＭ等技术研究了三种Ｋ２Ｏ－Ｂ２Ｏ３－ＳｉＯ２玻璃的析晶性能。结果表明，Ｋ２Ｏ－Ｂ２Ｏ３－ＳｉＯ２玻璃的析晶由分相引起，分相和析晶能力受成分影响较大。随Ｂ２Ｏ３和Ｋ２Ｏ含量增多及Ｋ２Ｏ／Ｂ２Ｏ３比值的降低，析晶加强。析晶中主晶相类别尚未查清，次晶相确定为α－方石英。     

NUMERICAL SIMULATION OF PARTICLE SEPARATION IN AN OIL-SAND SEPARATOR

ＮＯＴＡＴＩＯＮＳＡ　Ａｒｅａｏｆｉｎｌｅｔ ,ｍ2ａ　Ｃｅｎｔｒｉｆｕｇａｌａｃｃｅｌｅｒａｔｉｏｎ ,ｍ2 /ｓｉ　Ｇｒｉｄｏｆａｘｉａｌｄｉｒｅｃｔｉｏｎｍｌ 　ＭａｘｉｍｕｍｇｒｉｄｎｕｍｂｅｒｏｆｒａｄｉａｌｄｉｒｅｃｔｉｏｎＱ　Ｆｌｕｉｄｍａｓｓｒａｔｅ ,ｍ3/ｓＲｃ 　Ｍａｘｉｍｕｍｒａｄｉｕｓｏｆｃｙｃｌｏｎｅ ,ｍＲｅ　Ｒｅｙｎｏｌｄｓｎｕｍｂｅｒｒ　Ｄｉｍｅｎｓｉｏｎｌｅｓｓｒａｄｉａｌｄｉｓｔａｎｃｅｔ　Ｄｉｍｅｎｓｉｏｎｌｅｓｓｔｉｍｅｕ　Ｄｉｍｅｎｓｉｏｎｌｅｓｓａｘｉａｌｖｅｌｏｃ…     

甲醇与碳酸二甲酯共沸液的分离研究进展

综述了DMC-CH_3OH二元共沸液的各种分离方法。讨论了共沸精馏和萃取精馏的工艺流程。     

制氧(全)系统停车的迅速恢复和预防

介绍了安阳钢铁公司制氧厂结合实际总结出的制氧 (全 )系统停车的迅速恢复的操作方案和预防停车的措施 ;分析了经济效益。现机组自启动到送氧只需 2 3个小时 ,比设计值减少约 2 5小时。     

重油催化裂化反应技术的新进展

近十几年来，重油催化裂化技术作为主要的重质油轻质化手段得到了迅速发展，国内外围绕催化裂化装置的提升管反应器也开发了许多新技术。综述了重油催化裂化反应技术的新进展，并对新技术的开发进行了讨论。