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411.
412.
Co/Cu纳米多层膜的制备及巨磁阻性能的研究 总被引:9,自引:0,他引:9
采用恒电位双电解槽法在硼酸镀液体系中,以单晶Si(111)为基底电沉积制备Co/Cu多层膜,确定了双槽法制备多层膜的工艺条件,为得到优良的多层膜巨磁阻材料,镀液体系中加入了自制的添加剂。并用扫描电镜(SEM)表征了多层膜的断面形貌,小角度X射线衍射(LXRD)谱图中出现了2个衍射峰,大角度X射线衍射(MXRD)谱图中强衍射峰的两侧出现了卫星峰,表明多层膜具有超晶格结构。用物性测量系统(PPMS)测试了Co/Cu多层膜的巨磁阻(GMR)性能,GMR值达到52.52%。 相似文献
413.
J. W. Lynn J. A. Borchers Q. Huang A. Santoro R. W. Erwin 《Journal of research of the National Institute of Standards and Technology》2001,106(6):953-963
Magnetic neutron scattering plays a central role in determining and understanding the microscopic properties of a vast variety of magnetic systems, from the fundamental nature, symmetry, and dynamics of magnetically ordered materials to elucidating the magnetic characteristics essential in technological applications. From the early days of neutron scattering measurements at NBS/NIST, magnetic diffraction studies have been a central theme involving many universities, industrial and government labs from around the United States and worldwide. Such measurements have been used to determine the spatial arrangement and directions of the atomic magnetic moments, the atomic magnetization density of the individual atoms in the material, and the value of the ordered moments as a function of thermodynamic parameters such as temperature, pressure, and applied magnetic field. These types of measurements have been carried out on single crystals, powders, thin films, and artificially grown multilayers, and often the information collected can be obtained by no other experimental technique. This article presents, in an historical perspective, a few examples of work carried out at the NIST Center for Neutron Research (NCNR), and discusses the key role that the Center can expect to play in future magnetism research. 相似文献
414.
采用多靶磁控溅射制备了 W/SiC纳米多层膜。并用 XRD和 TEM研究了 W/SiC纳米多层膜的微结构。研究表明,W/SiC纳米多层膜的调制结构界面平直、清晰、周期性好;SiC调制层为非晶态,W调制层在大调制周期为纳米晶,并随调制周期减小逐渐转变为非晶态。 相似文献
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A study of microstructural effects in finite layered media containing single and periodically distributed cracks is carried out based on an exact elasticity solution. First, the effect of microstructural refinement of a multilayer comprised of alternating hard and soft layer pairs on the stress intensity factors and crack-opening displacements of a single crack embedded in the middle of the layered structure is studied. The results indicate that the crack-opening displacements converge to the corresponding ones in the fully homogenized configuration with increasing microstructural refinement. In contrast, the stress intensity factors asymptotically converge to values that depend on the layer stiffness. For configurations with many layers, partial homogenization efficiently captures these microstructural effects and preserves the homogenization’s efficiency. Then the exact elasticity solution is employed to study the response of a homogeneous solid with elastic properties degraded by periodically aligned cracks. The effective properties obtained from a homogenization scheme are used to quantify the convergence behavior of the stress intensity factors of cracks far and near the bounding surface of the periodically cracked solid as a function of different levels of partial homogenization. 相似文献
420.
Nanoparticles made from poly(dl-lactide-co-glycolide) (PLGA) are used to deliver a wide range of bioactive molecules, due to their biocompatibility and biodegradability. This study investigates the surface modification of PLGA nanoparticles via the layer-by-layer (LbL) deposition of polyelectrolytes, and the effects of these coatings on the release behavior, cytotoxicity, hemolytic activity, and cellular uptake efficiency. PLGA nanoparticles are modified via LbL adsorption of two polyelectrolyte pairs: 1) poly(allylamine hydrochloride) (PAH) and poly(styrene sulfonate) (PSS) and 2) poly(L-lysine hydrobromide) (PLL) and dextran sulfate (DES). It is demonstrated that both PAH/PSS and PLL/DES coatings suppress the burst release usually observed for unmodified PLGA nanoparticles and that the release behavior can be adjusted by changing the layer numbers, layer materials, or by crosslinking the layer constituents. Neither bare nor polyelectrolyte-modified PLGA nanoparticles show any signs of cytotoxicity. However, nanoparticles with a positively charged polyelectrolyte as the outermost layer induce hemolysis, whereas uncoated particles or particles with a negatively charged polyelectrolyte as the outermost layer show no hemolytic activity. Furthermore, particles with either PAH or PLL as the outermost layer also demonstrate a higher uptake efficiency by L929 fibroblast cells, due to a higher cell-particle affinity. This study suggests that LbL coating of PLGA nanoparticles can control the release behavior of bioactive molecules as well as the surface activity, therefore providing a promising strategy to enhance the efficiency of nanoparticulate drug-delivery systems. 相似文献