ULTRA‐FINE TRACKING CONTROL ON PIEZOELECTRIC ACTUATED MOTION STAGE USING PIEZOELECTRIC HYSTERETIC MODEL

The tracking control accuracy of the piezoelectric actuator (PEA) is limited due to its inherent hysteresis nonlinearity. A new piezoelectric‐actuator model is synthesized based on two first‐order transfer systems in parallel with two tuned parameters determined from one experiment. Two open‐loop tracking controllers are implemented with the proposed model to compensate the hysteresis of linear positioning. Numerical simulations and experimental tests on the tracking of sinusoidal and triangular waveforms with signal frequencies ranging from 1Hz to 30 Hz are revisited and compared with the conventional Bouc‐Wen and Duhem models. Experimental results reveal that the RMS tracking error can be reduced to less than 2% of the maximum traveling distance without any feedback sensor. When a piezoelectric actuated on a two Degree‐Of‐Freedom (DOF) monolithic motion stage was employed, the RMS tracking error was 50 nm within the measured sensor accuracy.     

紫杉醇硅胶表面分子印迹纳米颗粒的制备

以紫杉醇为模板分子,紫杉醇上的羟基与异氰酸酯丙基三乙氧基硅烷(IPTS)反应形成共价复合物,然后和交联剂正硅酸乙酯(TEOS)通过溶胶-凝胶的方法涂覆在纳米硅胶表面上,以热裂解的方式去除模板分子后形成紫杉醇硅胶表面分子印迹纳米颗粒。通过吸附实验分析研究了紫杉醇硅胶表面分子印迹纳米颗粒的亲和性能,结果表明印迹纳米颗粒对紫杉醇有良好的亲和性。     

纳米隔热材料在水泥厂中的设计应用

纳米隔热材料具有良好的隔热性能和热稳定性,在水泥厂高温部分使用可有效降低系统表面散热。本文通过建立设计模型量化散热量,对纳米隔热材料使用规格、部位作进一步优化。     

液相法制备纳米钯粉的工艺研究

采用液相法,以Pd粉为原料,分别用HCHO,HCOOM,C2H4H2O作还原剂,把钯还原成纳米粉末。通过控制反应体系的pH值、浓度、温度及还原剂的种类和还原时间来控制粉末的粒径大小及其分布.实验结果表明:利用本法制备的Pd粉粒径在9 nm~20 nm,粒度分布均匀而且重现性好,适用于制造钯银导体浆料.     

Fischer-Tropsch Performance of an SiO2-Supported Co-Based Catalyst Prepared by Hydrogen Dielectric-Barrier Discharge Plasma

A silica-supported cobalt catalyst was prepared by hydrogen dielectric-barrier dis- charge （H2-DBD） plasma. Compared to thermal hydrogen reduction, H2-DBD plasma treatment can not only fully decompose the cobalt precursor but also partially reduce the cobalt oxides at lower temperature and with less time. The effect of the discharge atmosphere on the property of the plasma-prepared catalyst and the Fischer-Tropsch synthesis activity was studied. The re- sults indicate that H2-DBD plasma treatment is a promising alternative for preparing Co/SiO2 catalysts from the viewpoint of energy savings and efficiency.     

乙酰丙酮改性硅胶制备及在焦化废水处理的应用

用乙酰丙酮改性硅胶合成了一种新型固相萃取材料β-二酮改性硅胶,制备的材料用漫反射红外光谱进行表征,并将其用于固相萃取焦化废水中的痕量重金属元素。实验详细考察了溶液pH值、进样条件、洗脱条件以及共存离子干扰等因素对3种重金属离子镉、铅和汞的吸附效率的影响。结果表明,在优化的实验条件下,大部分的重金属离子都可以被定量除去。制备的β-二酮改性硅胶材料可以用盐酸再生,该方法快速、经济、选择性好,适用于固相萃取焦化废水中重金属离子。     

异氰酸酯增强二氧化硅气凝胶的力学性能

采用有机无机复合的方式,制得异氰酸酯增强的SiO2气凝胶。将硅酸甲酯(TMOS)、甲基三甲氧基硅烷(MTMS)、3-氨丙基三乙氧基硅烷(APTES)配成混合硅源,经水解缩聚后形成凝胶,老化后浸泡在含六亚甲基二异氰酸酯单体(HDI)的乙腈溶液中,最后经CO₂超临界干燥,获得了具有良好机械性能的SiO₂气凝胶。制备过程中引入的MTMS增加了凝胶与有机物间的浸润性,与使用有机物低聚体相比,使用单体可使有机物更易进入凝胶网络,反应更充分,形成纳米尺度更均匀的复合气凝胶。复合后的气凝胶密度为330 mg/cm³、比表面积为446.3 m²/g、热导率为0.068 W•m^-1•K^-1,该气凝胶良好的力学性能(压缩强度为19.96 MPa、压缩模量为82.37 MPa)使气凝胶的机械加工成为可能。     

Research Profiling of Nano-enchanced Molecular Imaging Technology

Molecular imaging, as an emerging technique in current medical diagnostics, therapy and biology science, has received more and more attention in academia, industry, as well as medical practices. And the applications of nanotechnology in this field stimulate its development. This paper explores the development of the basic research and applied research on nano-enhanced molecular imaging, and does the in-depth analysis by adopting the bibliometrics method. The results show that the US is the leader in this field, who has the absolute advantages. Germany, UK and France and Japan are the followed ones. The rapidly developing Asian countries , China and South Korea might become the potential competitors. Research network analysis draws the conclusion that the other countries and regions share the same research interests with the US. The US not only take the lead in the researching number, but also directing the future orientation of this field. However, the US has not much international collaboration. The collaboration within the country and regions show that collaboration in this field is limited to the regional adjacency. Disciplinary analysis reveals that the major subjects which relate intimately to the nano-enhanced molecular imaging are chemistry, biomedical science and material science.     

掺杂Co的纳米TiO2光催化降解水中五氯苯酚的研究

采用溶胶-凝胶法制备的掺杂Co纳米TiO2粉体(Co/TiO2),在紫外光照射下光催化降解水中五氯苯酚(PCP).研究了光照反应时间、催化剂加入量、PCP溶液初始浓度等因素对纳米Co/TiO2光催化降解五氯苯酚的影响.在溶液中五氯苯酚初始浓度为0.01 mg/mL,pH=9～10,纳米Co/TiO2加入量达到0.25 ...     

Preparation,characterization of Y~(3+)-doped TiO_2 nanoparticles and their photocatalytic activities for methyl orange degradation

A series of pure and Y3+-doped TiO2 nanoparticles with high photocatalytic activities were prepared by a sol-gel method using tetra-n-butyl titanate as precursor.The as-prepared catalysts were characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM) and diffuse reflectance spectroscopy(DRS).The results indicated that yttrium doping could effectively reduce the crystalline size,inhibit the anatase-to-rutile phase transformation and surppress the recombination of the photogenerated electron-h...