浅谈酶在非接触印刷废纸脱墨中的应用

简要地介绍了纤维素酶、半纤维素酶和淀粉酶在非接触印刷废纸脱墨中的研究及其应用     

锅炉对流管爆裂原因分析

采用化学分析、金相检验及力学性能测定等方法，对锅炉对流管爆裂原因进行了分析。结果表明，长期超温运行而引起的蠕变是导致爆裂的主要原因。     

可靠性试验样本量和截尾时间的计算

可靠性寿命试验中，一般都因受到费用和时间的限制，因此要用截尾试验获得信息，再据此对其可靠性进行统计推断，用非参数估计的方法探讨了进行可靠性试验的样本量或截尾时间的估计方法。     

沸石加氢处理催化剂的制备方法

考察了渣油加氢处理催化剂制备过程中引入一种低硅铝比沸石的情况，它不仅提高催化剂的酸性，而且由于引入的分子筛孔径集中，最终使催化剂具有集中的孔分布，弥补了制备高活性催化剂采用混捏法的不足，制备出来的催化剂性能更优异。     

絮凝剂品种对水下不分散混凝土性能影响的比较

通过电荷中和、吸附架桥和表面吸附分析了絮凝剂作用机理 ,运用絮凝机理进一步分析了絮凝剂在水泥体系中的作用以及絮凝剂对流动度的影响 ,从而对掺加JHP (纤维素类 )和Pj (丙烯类 )絮凝剂的水下不分散混凝土性能作了综合比较。掺Pj絮凝剂的混凝土 ,其坍扩度损失大 ,抗分散性能不如掺JHP絮凝剂的好 ;掺JHP絮凝剂的混凝土坍扩度在 3h内损失很小     

A STUDY ON ACIDITY AND CATALYTIC PROPERTY OF [B] ZSM-5 CATALYST MODIFIED WITH SILICON COMPOUND BY CHEMICAL SURFACE DEPOSITION OF LIQUID-PHASE TECHNIQUE

The boron heteroatom zeolite catalyst has been modified with silicon compound by Chemical Surface Deposition of Liquid-phase (CLD) technique and the catalytic property of the modified catalyst is studied. Meanwhile, the acidity of the modified zeolite catalysts is characterized through TPD and IR technique, and the fluid adsorption method is used to determine its pore structure. The relationship between the catalytic property of the zeolite catalyst and its pore structure, its acidity has been found. The results of toluene-ethylene alkylation reaction indicate that the selectivity of p-ethyltoluene on the modified zeolite catalyst is higher than that on the zeolite catalyst before silanizated, reaching 94.14%.     

Synthesis, Characterization, and Formation Process of Na-X Zeolite from Coal Fly Ash

Using the SiO₂ and Al₂O₃ components of the amorphous phase in coal fly ash (Fa), Fa was converted to Na-X zeolites in NaOH-NaAlO₂ solutions by stirring at 35°C for 72 hr and then aging at 85°C for a given period. The molar ratio SiO₂/Al₂O₃ of the starting materials was controlled from 2.0 to 13.2. The resulting materials were characterized by various means. Increasing the SiO₂/Al₂O₃ ratio of the starting material increased the degree of crystallinity of faujasite, exhibiting a maximum at SiO₂/Al₂O₃ = 8.0. The faujasite formed was identified as Na-X zeolite with Si/Al = 1.20. The amorphous phase in Fa was dissolved during the stirring to form a precursor of zeolite, such as amorphous aluminosilicate. The Na-X zeolite was formed by aging for 24 hr, and the degree of crystallinity of this material was increased with the increasing aging period. The cation exchange capacity and specific surface area were increased with the increasing degree of crystallinity of the Na-X zeolites.     

KZON-50/120空分设备的安装调试及设计改造

在KZON-50/120空分设备的安装调试和试运行过程中,对其机械和电器部分进行了多处改造,克服了原设计中存在的不足之处。改造后,机械和电器性能更加趋于合理,操作简单,便于维护,降低了制气费用,提高了制气纯度和经济效益,保证了空分设备更加安全可靠运行。     

Morphology and properties of poly[2‐methoxy‐5‐(2′‐ethyl‐hexyloxy)‐para‐phenylene vinylene]/silica nanoparticle hybrid films

Poly[2‐methoxy‐5‐(2′‐ethyl‐hexyloxy)‐para‐phenylene vinylene] (MEH‐PPV)/silica nanoparticle hybrid films were prepared and characterised. Three kinds of materials were compared: parent MEH‐PPV, MEH‐PPV/silica (hybrid A films), and MEH‐PPV/coupling agent MSMA/silica (hybrid B films), in which MSMA is 3‐(trimethoxysilyl) propyl methacrylate. It was found that the hybrid B films could significantly prevent macrophase separation, as evidenced by scanning electron and fluorescence microscopy. Furthermore, the thermal characteristics of the hybrid films were largely improved in comparison with the parent MEH‐PPV. The UV‐visible absorption spectra suggested that the incorporation of MSMA‐modified silica into MEH‐PPV could confine the polymer chain between nanoparticles and thus increase the conjugation length. The photoluminescence (PL) studies also indicated enhancement of the PL intensity and quantum efficiency by incorporating just 2 wt% of MSMA‐modified silica into MEH‐PPV. However, hybrid A films did not show such enhancement of optoelectronic properties as the hybrid B films. The present study suggests the importance of the interface between the luminescent organic polymers and the inorganic silica on morphology and optoelectronic properties. Copyright © 2004 Society of Chemical Industry     

基于双因子认证技术的网络身份识别

本文提出了一种基于动态双因子认证技术的网络身份识别方法,用户每次登录的口令是利用系统时间和用户ID通过MD5加密算法计算得到,其通过MD5加密后生成的登录口令是随机的,这将进一步提高开放网络环境下身份识别的可靠性和安全性。同时,本文还提出网络身份识别技术可以应用到各类网站的服务器上,用来完成对用户身份的识别,以提高网络系统的安全性。