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31.
Anionic copolymerizations of styrene (M1) with excess 1-(4-dimethyl-aminophenyl)-1-phenylethylene (M2) were conducted in benzene at 25°C for 24h, using sec-butyllithium as initiator. Narrow molecular weight distribution copolymers with M?;n = 16.1 × 103 g/mol (M?w/M?n = 1.04) and 38.2 × 103g/mol (M?w/M?n = 1.05), and 24 and 38 moles of M2 per macromolecule, respectively, were characterized by size exclusion chromatography, 1H NMR spectroscopy and DSC. The monomer reactivity ratio, r1 = 5.6, was obtained from the copolymer composition at complete consumption of M1, assuming that the rate constant k22 =0,i.e. r2 =0. The polymers exhibited Tg values of 128 and 119°C, respectively, which correspond to an estimated Tg = 217°C for the hypothetical homopolymer of M2. 相似文献
32.
It is demonstrated that glassy carbon powder can be thermochemically activated. During activation, a film with open pores is created on the glassy carbon particles. This film has a large internal surface area, which is accessible to liquids and gases. A simple model for the evolution of the internal surface area in glassy carbon powder during thermochemical gas-phase oxidation is also presented and compared with experimental data. Experimental results are in qualitative agreement with the model. We found that a sharp particle size distribution is desirable with regard to potential technical applications. 相似文献
33.
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35.
Amjad B. Soulaka William R. Morrison 《Journal of the science of food and agriculture》1985,36(8):709-718
Starches isolated from 23 bread wheats (Triticum aestivum) and 26 durum wheats (T. durum) contained 26.3-30.6% (mean 29.1%) total amylose, 19.3–25.1% (mean 22.9%) apparent amylose and 783–1144mg 100g?1 (mean 977 mg 100g?1) lysophos-pholipids. Gelatinisation temperatures were 57.3–64.9°C (mean 61.8°C) and enthalpies 6.4–11.8 Jg?1 (mean 9.7Jg?1) in excess water, measured by differential scanning calorimetry. There were no correlations between any of these parameters. Starch granule size distributions were determined with a Coulter Counter and 100–channel analyser. A-granule mean volumes were 1235–2585μm3 (av. 1778), modal volumes 863–1804μm3 (av. 1264), mean diameters 13.9–16.0μm (av. 13.99), and specific surface areas 0.236–0.302m2g?1. B-granule mean volumes were 35.4–100.4μm3 (av. 55.9), modal volumes 16.5–54.5μm3 (av. 27.7), mean diameters 3.66–5.07μm (av. 4.09), and specific surface areas 0.684–0.920m2g?1. The B-granule contents of the starches were 12.8–34.6% (av. 27.3) by weight (sedimentation method) and 13.0–37.3% (av. 24.0) by volume (Coulter method), the latter being the more accurate method. 相似文献
36.
济钢350m^3高炉高富氧生产技术 总被引:1,自引:1,他引:0
分析了济钢350m^3高炉高富氧对产量,理论燃烧温度,炉况顺行状况,焦比和生产效益的影响,高富氧可提高产量,但升高焦比和高炉理论燃烧温度,一定程度上影响高炉顺行,存在富氧效益最大化的适宜富氧率.高炉生产应低富氧高喷煤,根据钢目前的情况,富氧率经2%-3%为宜. 相似文献
37.
In this paper we design a dynamic dictionary for
the priced information model initiated by Charikar et al. Assume that a set S consisting of n elements is given such that
each element has an associated price, a positive real number. The cost of performing an operation on elements of S is a function
of their prices. The cost of an algorithm is the sum of the costs of
all operations it performs. The objective is to design algorithms
which incur low cost. In this model we propose a dynamic dictionary, supporting
search, insert and delete, for keys drawn from a linearly ordered set.
As an application we show that the dictionary can be used in
computing the trapezoidal map of a set of line segments, a fundamental problem in
computational geometry. 相似文献
38.
MODELING LIQUID MASS TRANSFER IN HIGEE SEPARATION PROCESS 总被引:1,自引:0,他引:1
Correspondence concerning this paper should be addressed to Professor Richard S.H. Mah. Hsien-Hsin Tung is now affiliated with Department of Chemical Engineering, California Institute of Technology
Penetration theory is used to describe the liquid mass transfer in Higee separation process. Within a possible range of effective areas, it is shown that the predicted mass transfer coefficients are in reasonable agreement with the estimated mass transfer coefficients. The estimated coefficients were calculated from the experimental data and the possible effective areas. Hence it is concluded the penetration theory is generally applicable to describe liquid mass transfer in Higee separation process. The comparison also suggests that liquid mixing at the junctions of packing materials may be more complete in Higee process than in traditional process. 相似文献
Penetration theory is used to describe the liquid mass transfer in Higee separation process. Within a possible range of effective areas, it is shown that the predicted mass transfer coefficients are in reasonable agreement with the estimated mass transfer coefficients. The estimated coefficients were calculated from the experimental data and the possible effective areas. Hence it is concluded the penetration theory is generally applicable to describe liquid mass transfer in Higee separation process. The comparison also suggests that liquid mixing at the junctions of packing materials may be more complete in Higee process than in traditional process. 相似文献
39.
Optimizing of laminar viscous flow through a pipe by two dimensionless values is investigated analytically. Dimensionless entropy generation and pumping power to heat transfer rate ratio are used as basis for constant viscous and the temperature dependence on the viscosity. For this matter we calculate entropy generation and pumping power for a fully developed in a pipe subjected to constant wall temperature for either constant viscosity and the variable viscosity. The variation entropy generation increase along the pipe length for viscous fluid is drawn, either the variation summation dimensionless entropy generation and the pumping power to heat transfer rate ratio are varying the fluid inlet temperature for fixed pipe length and are varying pipe length for fixed fluid inlet temperature are drawn. For low heat transfer conditions the entropy generation due to viscosity friction becomes dominant and the dependence of viscosity with the temperature becomes essentially important to be considered. 相似文献
40.
T. M. Morris 《Journal of the Institute of Brewing》1987,93(1):13-17
Haze measurements have been obtained for suspensions of polystyrenelatex particles of known diameter using two light scattering instruments which measure at angles of 90° and 13° respectively. The results agree well with the theory of light scattering and demonstrate the significant effects of particle size and angle of detection upon the instrumental values for haze. This information has been used to correlate the particle size distributions of a number of beers, as measured by Coulter Counter, with the corresponding, measured haze values. 相似文献