巴洛沙星的合成研究

巴洛沙星是一种新型喹诺酮类抗感染药物。从反应温度、反应时间、反应物料摩尔配比和反应溶剂等对合成的影响进行了详细研究。结果表明,其优惠工艺合成条件为:以S1为溶剂,反应温度40℃,反应时间4 h,反应物料摩尔配比n螯合物Ⅰ∶nMAP=1∶1,产品收率79.5%,含量91.4%。     

MC(Mid-Century)催化氧化过程的研究进展

介绍了MC催化氧化过程规律；从催化荆体系的改进、新型溶剂体系的开发、反应器构型和配套设施的改进、富氧氧化技术的开发等方面综述了近年来MC技术的发展；探讨了MC液相催化氧化技术应用范围的拓展以及MC液相催化氧化过程的发展方向。     

Performance analysis for range expansion in heterogeneous networks

In this paper, the uplink and downlink performance of a two-tier heterogeneous network （HetNet） with range expansion （RE） is analyzed. Different from previous works, base stations （BSs） are modeled as a spatial Poisson point process. This model can not only capture the irregularity of the BS deployment but also lead to closed form expressions. With the analytical results, the impacts of several key parameters on the coverage and throughput performance are investigated. Our results justifies the effectiveness of RE and Pico deployment. Based on our analyses, certain attention should be made on the RE design to balance the uplink and downlink performance. Our analyses are corroborated by simulations and can thus serve as a flexible and quick guidance for system design without complicated and time-consuming system-level platform construction and simulation.     

三氯异氰尿酸生产技术研究

对三氯异氰尿酸合成反应过程中的主要工艺参数进行分析和实验研究,并成功地开发出了连续法生产三氯异氰尿酸的新工艺,该工艺和传统工艺相比,具有生产安全、高效、节能的特点。     

Incremental join view maintenance on distributed log-structured storage

Modern database systems desperate for the ability to support highly scalable transactions and efficient queries simultaneously for real-time applications. One solution is to utilize query optimization techniques on the on-line transaction processing (OLTP) systems. The materialized view is considered as a panacea to decrease query latency. However, it also involves the significant cost of maintenance which trades away transaction performance. In this paper, we examine the design space and conclude several design features for the implementation of a view on a distributed log-structured merge-tree (LSMtree), which is a well-known structure for improving data write performance. As a result, we develop two incremental view maintenance (IVM) approaches on LSM-tree. One avoids join computation in view maintenance transactions. Another with two optimizations is proposed to decouple the view maintenance with the transaction process. Under the asynchronous update, we also provide consistency queries for views. Experiments on TPC-H benchmark show our methods achieve better performance than straightforward methods on different workloads.     

Estimation of access failure probability in D2D underlaid cellular networks

Device-to-Device (D2D) communication can reduce the mobile devices' energy consumption and increase the spectral efficiency in D2D underlaid cellular networks. However, D2D users will interfere with co-channel cellular users, which can lead to cellular communication access failures. There are two reasons for cellular communication access failures: (1)D2D interference and (2)insufficient spectrum resources. To address the absence of research on the performance of cellular services' access in D2D underlaid cellular networks, this paper defines the new services' access failure probability and handoff services' access failure probability to evaluate the effect of both D2D interference and limited resources on cellular communication access. Based on the stochastic geometry and stochastic process, a random network model is presented to estimate the access failure probabilities, which can provide guidelines for network design to ensure cellular services' access. The accuracy of the estimated access failure probability is validated through extensive simulations.     

Connecting parameters optimization on unsymmetrical twin-tower structure linked by sky-bridge

Based on a simplified 3-DOF model of twin-tower structure linked by a sky-bridge, the frequency response functions, the displacement power spectral density （PSD） functions, and the time-averaged total vibration energy were derived, by assuming the white noise as the earthquake excitation. The effects of connecting parameters, such as linking stiffness ratio and linking damping ratio, on the structural vibration responses were then studied, and the optimal connecting parameters were obtained to minimize the vibration energy of either the independent monomer tower or the integral structure. The influences of sky-bridge elevation position on the optimal connecting parameters were also discussed. Finally, the distribution characteristics of the top displacement PSD and the structural responses, excited by El Centro, Taft and artificial waves, were compared in both frequency and time domain. It is found that the connecting parameters at either end of connection interactively affect the responses of the towers. The optimal connecting parameters can greatly improve the damping connections on their seismic reduction effectiveness, but are unable to reduce the seismic responses of the towers to the best extent simultaneously. It is also indicated that the optimal connecting parameters derived from the simplified 3-DOF model are applicable for two multi-story structures linked by a sky-bridge with dampers. The seismic reduction effectiveness obtained varies from 0.3 to 1.0 with different sky-bridge mass ratio. The displacement responses of the example structures are reduced by approximately 22% with sky-bridge connections.     

基于模糊层次分析的动态联盟伙伴选择策略

论述了基于模糊层次分析(AHP)的动态联盟伙伴选择策略。综合运用AHP方法和模糊决策方法构建了动态联盟伙伴选择的排序模型 ,通过求解该模型来得到参考排序值 ,力求使排序的结果能够客观、公正地反映不精确决策所蕴含的客观规律 ,以保证选择策略的准确性     

基于KBE的冲压工艺知识表示方法研究

根据冲压成形工艺的特点 ,研究了冲压工艺知识的分类 ,采用面向对象的方法 ,探讨了基于规则与基于实例的冲压工艺知识描述和自动获取技术 ,并在此基础上建立了基于知识驱动的冲压工艺特征模型。