高温合金中微量铈的快速测定

采用DBC-偶氮胂[3-(2-胂酸基苯偶氮)-6-(2，6-二溴-4氮苯偶氮)-4，5二经基2，7-萘二磺酸]直接测定高温合金钢中微量铈和碳钢、低合金中的铈，获得满意结果。     

微量银的分析与测定

评述了近些年来国内外对于微量银的分析测定技术，包括分光光度法、电化学分析法、原子吸收分光光度法和发射光谱法等，对当前广泛应用的技术提出了改进的意见并对这类研究的发展前景做出展望。     

Projection center calibration by motion

Camera calibration is the first step of three-dimensional machine vision. A fundamental parameter to be calibrated is the position of the camera projection center with respect to the image plane. This paper presents a method for the computation of the projection center position using images of a translating rigid object, taken by the camera itself.

Many works have been proposed in literature to solve the calibration problem, but this method has several desirable features. The projection center position is computed directly, independently of all other camera parameters. The dimensions and position of the object used for calibration can be completely unknown.

This method is based on a geometric relation between the projection center and the focus of expansion. The use of this property enables the problem to be split into two parts. First a suitable number of focuses of expansion are computed from the images of the translating object. Then the focuses of expansion are taken as landmarks to build a spatial back triangulation problem, the solution of which gives the projection center position.     

Convergence of iterated boolean sums of simultaneous approximants

Explicit error estimates are given for the iterated Boolean sum of a sequence of simultaneous approximants; the rate of convergence is shown to be improved for smooth functions. The general results are applied in the case of the Bernstein, Durrmeyer and Stancu operators.     

DETERMINATION OF TOTAL NITROGEN IN BARLEY AND MALT BY COMBUSTION METHOD—COLLABORATIVE TRIAL

A combustion method, relying on the Dumas principle, for the determination of total nitrogen in barley and malt, has been collaboratively tested by the Analysis Committee of the European Brewery Convention. Repeatability, r₉₅, and reproducibility, R₉₅, values were 0.063 and 0.116% of dry matter, respectively, for samples with nitrogen contents in the range 1.23 to 1.86% N of dry matter. There was no significant difference between these values for barley and malt. The Analysis Committee approved the adoption of the combustion method for inclusion in Analytica EBC as an alternative method.     

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本文通过对在用钻机井架的现场实际测试,建立数据库、测评模型,对实测的数据用计算机技术进行分析,提出了初始弯曲应力;数据正态分布检验——x～2检验;建立回归方程;在给定置信度下测评当前承载能力的技术概念。解决了在用钻机A型井架的安全性评估问题,是一种较为合理、可靠、科学的测评技术和方法。     

树脂悬浮光度法测定微量银

在ｐＨ６．９的缓冲溶液中，银与硫代米Ｃｈｉ酮（ＴＭＫ）形成的螯合物在树脂甘油相中悬浮富集，用光度法测定银在波长４６１ｎｍ处有最大吸收，银在０～６μｇ／１０ｍＬ范围内遵守比尔定律，可用于样品中微量银的测定。     

含碳冷固结团矿还原性测定方法探讨

含碳冷固结团矿与天然铁矿石、烧结矿、氧化球团矿不同、其还原性不能用减量法直接测定，需要根据还原后试样的化学成分计算获得，或根据试样中碳量的变化和试样的减量计算获得，但还原速率指数无法得到，本文以沙城铁厂试样为例进行了说明。     

高效液相色谱法测定头孢拉定制剂方法的改进

目的:改进头孢拉定制剂含量测定方法。方法:高效液相色谱条件:以Shim—Pack CLC—ODS(250mm×4.6mm)为色谱柱;柱温为35℃;流动相为水—甲醇—3.86％醋酸钠溶液-4％醋酸溶液(1364:500:30:6);流速为0.8mL·min~(-1);检测波长为254nm。结果:头孢拉定峰形良好,分离度和柱效满足药典要求,保留时间由原来的21.32min缩短至8.06min,提高了分析速度,含量测定结果与中国药典无显著差异。结论:该方法快速、准确、能更好地适用于常规检验工作和大批量生产时的质量控制。