荧光增敏法测定保健品中的镁

在pH=10.0的缓冲溶液中,于激发波长275 nm、发射波长360 nm处测定时,邻菲啰啉溶液的荧光强度因与镁发生反应生成了络合物而得到增敏,其增敏程度（ΔF）与镁的质量浓度在0.1~2.0mg/L的范围内呈线性关系。用此方法测定了3种保健品中镁的含量,测定值的相对标准偏差在0.15%~0.59%之间。同时做了加标回收试验,其回收率在93.30%~103.9%之间,结果满意。     

典型煤种CO_2气化过程中产物的析出特性

CO2气氛下在热重分析仪上对3种典型煤种分别进行了气化实验,与便携红外分析仪连用,详细研究了煤气化产物与温度、煤种的关系。结果表明：气化温度在500～800℃之间,C煤的甲烷生成速率较高,但焦炭与水蒸气的气化反应较慢,但温度达到1 000℃时甲烷会分解;在热重分析仪中,高灰分阻碍了气化反应的进行,400～1000℃过程中失重曲线较平缓,在1 000℃之后,TG曲线有了明显的变化;煤化程度越低,越有利于挥发分的析出,有利于提高气化过程中CO和CH4的析出量,而且降低了有机硫（COS）的析出量。     

气象集合预报的研究进展

集合预报是数值预报发展的一个重要方向,相对于单一的确定性预报,它考虑了初值及模式的不确定性,其结果反映了未来天气的多种状况,能为用户提供确定性预报所不能提供的信息(如预报结果的可信度等)。降水信息是水文预报系统的核心输入,单一的降水预报存在着不确定性,从而使得水文预报也存在不确定性。这种不确定性制约了水利工程调度的科学性。集合预报在一定程度上能解决这种不确定性。从而在水文领域,气象集合预报具有较高的应用价值。为了水文工作者能够更好地应用集合预报,本文首先基于系统的角度,对集合预报系统中的初值扰动、模式扰动和集合预报产品等研究现状及成果进行了评述,然后分析了降水集合预报产品在水文预报领域中的应用情况,最后对集合预报在水文领域中的应用进行了展望。     

Performance of Sewage Sludge Treatment and Electricity Generation by Different Configuration Microbial Fuel Cells

This paper compared the degradation efficiency of sludge organic matters and electric-production by two typical microbial fuel cells——dual-chamber microbial fuel cell(DMFC)and single chamber air cathode microbial fuel cell(SAMFC),and the variations of sludge protein,polysaccharide and ammonia nitrogen within the systems were also investigated.The results showed that the concentration of sludge soluble chemical oxygen demand,protein and carbohydrate of DMFC are higher than these of SAMFC during the systems operation,while DMFC can achieve a better ammonia nitrogen removal than SAMFC.Under the same operation condition,the stable voltage output of DMFC and SAMFC is 0.61 V and 0.37 V;the maximum power density of DMFC and SAMFC is 2.79 W/m3and 1.25 W/m3;TCOD removal efficiency of DMFC and SAMFC is 34.14%and 28.63%for 12 d,respectively.Meanwhile,DMFC has a higher coulomb efficiency than SAMFC,but both are less than5%.The results showed that DMFC present a better performance on sludge degradation and electric-production.     

Deterioration mechanism of sulfate attack on concrete under freeze-thaw cycles

The experiments of concrete attacked by sulfate solution under freeze-thaw cycles were investigated. The sulfate solution includes two types of 5% Na2SO4 and 5% MgSO4. Through the experiment, microstructural analyses such as SEM, XRD and TGA measurements were performed on the selected samples after freeze-thaw cycles. The corrosion products of the concrete were distinguished and quantitatively compared by the thermal analysis. Besides, the damage mechanism considering the dynamic modulus of elastically of concrete under the coupling effect was also investigated. The experimental results show that, under the action of freeze-thaw cycles and sulfate attack, the main attack products in concrete are ettringite and gypsum. The corrosion products exposed to MgSO4 solution are more than those to Na2SO4 solution. Furthermore, the content of gypsum in concrete is less than that of ettringite in test, and some of gypsum can be observed only after a certain corrosion extent. It is also shown that MgSO4 solution has a promoting effect to the damage of concrete under freeze-thaw cycles. Whereas for Na：SO4 solution, the damage of concrete has restrained before 300 freeze-thaw cycles, but the sulfate attack accelerates the deterioration process in its further test period.     

杏酒中有机酸类化合物的RP—HPLC法测定

建立了反相高效液相色谱测定杏酒中有机酸类化合物的方法．以金太阳杏为原料,经液体发酵法精心酿制成的低度杏酒作为检测样品,测定了杏酒中9种有机酸类化合物．采用AgilentC18色谱柱（4．6mm×250mm）分离,流动相2％的甲醇-0．01mol／L（NH4）2HPO4（pH2．8）洗脱,流速1mL／min,检测器波长为210nm,柱温30℃,采用色谱峰保留时间定性,面积外标法定量,并比较了不同杏发酵产品中有机酸的种类和含量,各成分的线性相关系数均大于0．99．方法的回收率大部分都在94％以上,RSD均在3％以下,说明该方法具有快速、分辨率高、重复性好等优点,可用于杏酒中有机酸类化合物的检测．     

微生态制剂在水产养殖中的应用

主要从防治鱼病的发生及减少抗生素滥用、改良水质和防治有害蓝藻等三个方面的作用综述了微生物制剂在水产养殖中的应用现状及研究进展,分析了目前微生物制剂研究及生产中存在的问题,并对微生物制剂在水产养殖中的研究及应用发展趋势作了进一步的展望。     

扬州“小巷游”产品开发初探

本文通过实地调研、访谈及查阅前人研究成果,对扬州小巷这一实物旅游资源进行目标市场调研与价值评价,进而探索塑造扬州"小巷游"品牌的有效方法,使其区别于上海小巷、北京胡同,自成一派,为扬州旅游业注入新鲜血液,从而提升扬州古城的整体旅游价值。     

乳化剂对坎利酮增溶及生物转化的影响

探索不同乳化剂sp60、sp80、tw60、tw80及其复合乳化剂对坎利酮羟基化的影响。结果表明乳化剂对坎利酮有增溶作用,且tw80、复合乳化剂tw80—sp60对坎利酮微生物转化有促进作用。其中单组分乳化剂tw80的最佳质量分数为0．18％,转化率为90．32％;复合乳化剂tw80-sp60,最佳质量分数为0．09％,转化率为92．22％。     

CDS在虚拟服务或产品与资源池中的安全应用研究

虚拟基础架构作为现当今主要的虚拟化技术应用,其快速、高效的特点是其他虚拟技术无法比拟的。但是在信息化高速发展的今天,安全是一个普遍性问题,因为它涉及到网络中的所有东西。本文应用"Castle Defense System"(城堡防御系统理论)简称CDS,针对虚拟基础架构中的两个最重要环节:资源池、虚拟服务或产品,进行全面的安全应用的理论研究。