Change in the decomposition mode of 1-propanamine due to the presence of cations in MFI zeolite

The adsorption and thermal analysis of 1-propanamine has been compared over MFI zeolites which contain H, Ga, and In cations. In the case of H⁺-containing materials, NH₃ and propene are simultaneously desorbed above 600 K. This behavior, is well known and characteristic of the Hofmann elimination reaction. However, a distinctly different mode of reaction is observed in the case of Ga and In containing materials. NH₃ is released below 600 K, propene and other products are released above 600 K, and a stable residue remains above 800 K. It is suggested that such behavior results from Lewis acid interactions of Ga or In cations with propanamine.On leave from the Bulgarian Academy of Sciences, Institute of Organic Chemistry.     

二流量试井工艺及资料解释分析方法

描述了二流量试井工艺的实现，从常规分析和双对数曲线拟合两上方面，给出了二流量试井的资料解释分析方法，分析认为二流量试井同样可以计算出正常关井测压力恢复（或压力降落）资料所解释的油藏及流体参数。这种试井方法不但可以减少因正常关井测压对产油量和注水量的影响，而且可以减缓因突然关、开井造成的套管变形或损坏。实践证明，该试井技术方法具有较好的经济效益和应用前景。     

Valid parameter range analyses for chemical reaction kinetic models

The present work quantifies the relations between the structure of a chemical reaction kinetic model, its valid parameter range, and the truncation error tolerance of the model. General methods are presented to solve the three important problems of valid parameter range analysis: (1) identification of the valid parameter range of a kinetic model, (2) estimation of the error tolerance required when applying a kinetic model over a specified parameter range, and (3) improvement of existing model generation algorithms to construct more robust models. Finally, the relationship between a model's structure, its valid parameter range, and the truncation error tolerance are illustrated by the flexibility-tolerance-model graph. The new methods are applied to pyrolysis of methane/ethane mixtures.     

工业固体核磁Magmonitor用于聚烯烃质量参数测试方法的建立

利用实际采集的系列试样 ,在工业固体核磁Magmonitor(IMR)上建立了标准曲线 ;在IMR上运行标样的核磁信号后 ,对FID信号与实验数值之间的匹配使用 32个误差分析因子进行分析 ,并在Cregcon软件下运行回归分析 ,将结果转化成仪器预测模型。结果表明 ,测试相对偏差在 10 %以内 ,数据重现性好 ,而粉料与共聚物的测试误差有待改进。将IMR测试结果与不同测试方法进行比较 ,建议测试前对粉料进行脱气与脱水处理     

电站装备失效分析及其预防

简叙了电站装备失效分析程序、失效原因及其失效机理。大量的各种各样的失效，常常涉及一种或多种的失效机理。在众机理中，主要是：腐蚀失效、环境断裂失效、变形失效和断理解失效。     

连续流动分析仪应用于水中硫化物的测定

对连续流动法测定硫化物进行初步探讨和研究。同时与其他几种测定硫化物的方法进行了比较。实验结果表明，连续流动法对硫化物分析在线性、稳定性、最低检测限、准确性和精密度等方面均优于其他方法。     

石油化工蒸汽系统顶层分析研究与应用

介绍石油化工蒸汽系统顶层分析，并通过实例分析阐明，在顶层分析的指导下进行蒸汽系统优化可以给工厂带来可观的经济效益。     

Monitoring Power Dissipation for Fault Detection

In this paper, we suggest that the dynamic power dissipation of acircuit can be used for fault detection. Even those faults which do notaffect static power dissipation can be detected by monitoring dynamic powerdissipation. We discuss how stuck-at, stuck-open, and redundant faults maybe detected by monitoring dynamic power dissipation. In many cases, theFourier spectra of the supply currents in the good and faulty circuits willalso be very different. Further, specific tests can be applied so as toimprove fault coverage. Power monitoring is verified using simulation, andalso experimentally, for example circuits.     

高砂比压裂技术研究

应用由美国ＮＳＩ公司引进的“ｓｔｉｍｐｌａｎ”拟三维压裂设计软件，对影响裂缝内支撑剂铺置浓度的诸因素进行了灰色关联度分析，从中找出了主要的影响因素。并以高砂比压裂的技术指标为依据，研究了在目前压裂工艺水平下，进行高砂比压裂所必须遵循的原则。文中还对国内的高砂比压裂进行了实例分析，进一步论证了文中的观点。     

露采边坡渗流的有限元分析及其实例

介绍了应用有限元法求解渗流问题的原理及其实例。