Effect of deposition conditions on the properties and annealing behavior of cold-sprayed copper

The deposition of copper by cold gas dynamic spraying has attracted much interest in recent years due to the capability to deposit low-porosity oxide-free coatings. However, it is generally found that as-deposited copper has a signicantly greater hardness, and potentially lower ductility, than bulk material. In this article, copper was deposited by cold spraying using helium as the driving gas at both 298 and 523 K. Evidence is presented indicating that the material sprayed at the lower temperature exhibits a lower dislocation density throughout the grain structure than the material sprayed at the higher temperature. The low stacking fault energy of copper restricts recovery during annealing, and thus microstructural changes during annealing only proceed once recrystallization begins. The material sprayed at low temperature (with the low dislocation density) exhibited recrystallization at annealing temperatures as low as 373 K with a corresponding reduction in hardness. However, the copper sprayed with helium at 523 K was resistant to annealing at temperatures up to 473 K where the dislocations in the structure prevented recrystallization. However, at higher temperatures, recrystallization did proceed (with corresponding reductions in hardness). The fracture behavior of the copper that was cold sprayed with helium at 523 K, both in the as-sprayed condition and following annealing, was measured and explained in terms of the annealing mechanisms proposed. The original version of this paper was published in the CD ROM Thermal Spray Connects: Explore Its Surfacing Potential, International Thermal Spray Conference, sponsored by DVS, ASM International, and HW International Institute of Welding, Basel, Switzerland, May 2–4, 2005, DVS-Verlag GmbH, Düsseldorf, Germany.     

提高磷酸二铵产品质量方法浅析

针对磷酸二铵(DAP)产品养分波动大、含水量偏高、易结块、颜色变化大等缺点,在生产过程中采取了相应的解决措施,如配矿、联产、设备改造、工艺指标调整等,使DAP装置不仅保持了原有的优点,而且产品质量问题也得到了有效解决。养分基本保持在64.0%~64.6%,水分下降到2.1%~2.2%,结块现象较少,颜色也比较统一。     

离心泵性能参数的自动测定和自动控制

通过将计算机技术应用于离心泵性能参数的研究，实现了离心泵性能参数的自动测定和自动控制。     

浅谈化工建设项目竣工预验收程序和内容

结合作者的实际工作 ,总结了对工程建设实施“三道质量控制工序”的经验 ,强调了过程质量控制的重要性 ,较为系统地介绍了化工建设项目预验收工作的程序和内容     

Determination of the solubility parameter of poly(ethylene oxide) at 25°C by gas-liquid chromatography

The solubility parameter of poly(ethylene oxide) at 25°C has been determined using the method developed by DiPaola-Baranyi and Guillet, by the extrapolation of the values of the interaction parameter χ, at high temperatures, ranging from 70°–90°, 90°–110° and 110°–130°C down to 25°C. The values of the solubility parameter obtained, depending on the temperature ranges employed, are 9.8, 9.9 and 10.1, respectively.     

用预分解技术改造Φ4×60m预热器窑的又一成功实例

介绍南京水泥工业设计研究院用预分解生产技术对山东水泥厂Φ4×60m预热器窑烧成系统进行的成功技术改造。技改设计指标为：熟料产量保证指标1500t／d，争取指标1700t／d，熟料热耗＜3762kJ／kg，熟料28d抗压强度＞60MPa。整个工程停产施工耗时仅用48d，烧成系统技改共耗资约3000万元。技改后一次点火投料成功，且点火当月即实现72h达标考核，所有设计指标均达标。     

如何提高预焙铝电解槽阳极质量

预焙阳极的质量已严重制约铝电解技术的发展，必须予以足够的重视．国外在提高阳极质量方面的有效措施，可以供国内阳极工厂技术改造及科研攻关借鉴．     

化肥企业质检机构的管理

针对我国化肥生产企业质检机构的现状 ,结合国家相关政策的要求 ,就如何搞好化肥企业质检机构的管理提出了诸多指导性意见     

企业核心竞争力关键要素——质量

介绍了如何体现产品质量及如何控制产品质量。