球化处理对氢化脱氢钛粉特性及其注射成形喂料流变性能的影响

氢化脱氢(HDH)钛粉形状不规则、流动性较差,不利于注射成形和提高其制品性能。本文通过PCS系统对HDH钛粉末进行球化处理,考察了球化处理对HDH钛粉特性及其注射成形喂料流变性能的影响。结果表明:球化处理后的HDH钛粉末变为近球形,粉末的流动性显著提高,其注射成形喂料的流变性能得到明显改善;同时,球化处理后钛粉的烧结组织明显细化,致密度大幅度提高。     

合金化和球化工艺对超高碳钢组织和性能的影响

 研究了合金化和球化工艺对超高碳钢组织和性能的影响。用扫描电子显微镜、透射电子显微镜和能谱仪观察了钢的组织形貌和元素分布。结果表明：在碳和铬含量相同的超高碳钢中加入同量的合金元素铝和硅时,铝可明显抑制锻造组织中网状或粗大的颗粒状碳化物的析出、细化珠光体组织和控制石墨形成。UHCS 213Si和UHCS 261Al钢经850 ℃×3 h球化退火处理后,都能得到较好的球化组织,其力学性能分别为：UHCS 213Si钢,Rm=1 033 MPa,Re=734 MPa,A=149%;UHCS 261Al钢,Rm=973 MPa,Re=677 MPa,A=182%。     

Correlation of Microstructure and Hydrogen Delayed Fracture for 1GPa Steels

Automobile industry tries to reduce the weight of automobile using high-strength steels.However,the high-strength steels are highly susceptible to delayed-fracture caused by hydrogen embrittlement.With increasing the strength,hydrogen embrittlement is more sensitive to diffusible hydrogen.The mechanism of delayed-fracture and the relationship with the microstructure and alloying elements are still ambiguous.This study analyzed the effect of the size and the spheroidization rate for the carbides on hydrogen-induced delayed fracture for 1GPa TS steel.     

珠光体球化的分形研究

珠光体球化反映到金相上，是一种不规则图像的变化，并且具有分形的特征，可望用分形几何的方法来进行描述。以Cr-Mo钢的珠光体球化为例，用分形维数来描述珠光体球化程度；用小岛法对15CrMo钢的珠光体球化图谱进行了测量。实验表明，珠光体球化从1级到6级，其相应的分形维数范围为1.3156-1.9282。从电厂运行了10^5h的15CrMo钢管上取样，实测了该试样的珠光体球化等级，结果表明，以分形维数表示的球化程度与按图谱评定的球化等级完全吻合。     

大挤压形变AZ91 D镁合金半固态等温组织演变

通过液淬法获得挤压比为40的AZ91D镁合金等温处理过程中的半固态组织,研究其球化机制.结果表明:密集位错促使再结晶速度加快,球化时间缩短.球化机制为等温过程中再结晶导致形变组织粒化,晶界低熔点组份聚集处以及位错密度相对较高的区域熔化,形成蜂巢状组织;固液界面张力和曲率过热促使多边形晶粒进一步球化.     

汽车右下悬臂件的断裂分析

对进口飞鹰牌轿车右下悬臂件的断裂问题进行了宏观分析,确定了其断裂原因。     

高强度轮毂的化学成分和熔炼处理工艺的研究

分析了轮毂的工作条件和基本性能要求,从保证其有良好强度和塑性韧性方面,采用强韧性较好的铸态铁素体球墨铸铁制造。对轮毂的化学成分进行设计,确定了其化学成分范围。选用低稀土镁合金的球化剂Re3Mg8,并采用冲入法进行球化处理,同时采用多次孕育处理及增加终硅量,强化孕育效果,使球墨铸铁的强度和塑性韧性得到提高。     

Fabrication of zinc‐loaded hollow glass microspheres (HGMs) for hydrogen storage

The greatest challenge for a feasible hydrogen economy lies on the production of pure hydrogen and the materials for its storage with controlled release at ambient conditions. Hydrogen with its great abundance, high energy density and clean exhaust is a promising candidate to meet the current global challenges of fossil fuel depletion and green house gases emissions. Extensive research on hollow glass microspheres (HGMs) for hydrogen storage is being carried out world‐wide, but the right material for hydrogen storage is yet underway. But many other characteristics, such as the poor thermal conductivity etc. of the HGMs, restrict the hydrogen storage capacity. In this work, we have attempted to increase the thermal conductivity of HGMs by ZnO doping. The HGMs with Zn weight percentage from 0 to 10 were prepared by flame spheroidization of amber‐colored glass powder impregnated with the required amount of zinc acetate. The prepared HGMs samples were characterized using field emission‐scanning electron microscope (FE‐SEM), environmental SEM (ESEM), high‐resolution transmission electron microscopy (HRTEM), Fourier transform infrared spectroscopy and X‐ray diffraction (XRD) techniques. The deposition of ZnO on the microsphere walls was observed using FE‐SEM, ESEM and HRTEM which was further confirmed using the XRD and ultraviolet–visible absorption data. The hydrogen storage studies done on these samples at 200 °C and 10‐bar pressure for 5 h showed that the hydrogen storage increased when the Zn percentage in the sample increased from 0 to 2%. The percentage of zinc beyond 2, in the microspheres, showed a decline in the hydrogen storage capacity. The closure of the nanopores due to the ZnO nanocrystal deposition on the microsphere surface reduced the hydrogen storage capacity. The hydrogen storage capacity of HAZn2 was found 3.26 wt% for 10‐bar pressure at 200 °C. Copyright © 2015 John Wiley & Sons, Ltd.     

感应等离子体球化法制备球形金属粉体材料的研究进展

原料粉体的质量已经成为制约金属3D打印发展的瓶颈因素。感应等离子体球化法制备所得的金属粉体材料具有球化率高、球形度高、杂质含量低和粒径可控等优点,是当前最有希望实现3D打印用高性能球形金属粉体大规模工业化生产的技术。本文阐述了感应等离子球化技术的工作原理、发展历程和技术特点,着重介绍了利用该技术制备钨、钼、钛等金属球形粉体的研究现状,在此基础上探讨了感应等离子球化技术函待解决的难点问题以及未来的发展趋势。     

新型Ti5321合金片层组织的热变形行为

为研究具有原始粗片层组织的Ti5321合金热压缩变形过程中流变应力、显微组织等随变形条件的变化,在Gleeble-2800型热模拟试验机上进行高温热压缩试验,试验温度790~850 ℃,应变速率为0.01~1 s-1,变形量为30%~70%。结果表明：Ti5321合金的软化机制与片层组织球化和动态再结晶有关,变形量和变形温度是影响合金片层组织球化及β再结晶的主要因素。同一变形温度和应变速率下,随着变形量的增大.会出现片层α相球化及β相再结晶现象。当应变速率和变形量相同时,低温变形主要发生的是片层α相球化行为,高温变形发生的是β相的再结晶。