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目的建立测定负载化硅胶的相对分子质量的凝胶色谱法。方法使用凝胶色谱法测定负载化硅胶的相对分子质量,选取已知不同分子量的聚乙二醇高聚物作为标准品,对检测结果进行标准曲线拟合,得到最佳拟合标曲,采用Shoedex SB-802 HQ凝胶色谱柱分离,示差折光检测器检测,测得准确负载化硅胶的相对分子质量。结果使用本方法测得未知负载化硅胶样品相对分子量为6.326×103,相对标准偏差(relative standard deviation, RSD)为1.45%。结论该方法简单、可靠,可用于测定负载化硅胶的相对分子质量。 相似文献
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We investigate the problem of reflection and refraction of thermoelastic waves at a magnetized solid-liquid interface in presence of initial stress. In the context of Green-Lindsay and coupled thermoelastic theories of thermoelasticity, the problem has been solved and the effect of magnetic field, external heat sources, and initial stress on p-, T-, and SV-waves propagation have been discussed. The boundary conditions at the interface for displacement continuity, vanishing the tangential displacement, continuity of normal force, tangential force, and continuity of temperature are applied. The amplitudes ratios for the incident p-, T-, and SV-waves have been obtained. The effect of the initial stress, heat sources, and magnetic field on the reflection and transmitted coefficients for the incident waves have been discussed. 相似文献
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《Journal of the European Ceramic Society》2020,40(4):1592-1601
Porous ceramic diesel particulate filters (DPFs) are extruded products that possess macroscopic anisotropic mechanical and thermal properties. This anisotropy is caused by both morphological features (mostly the orientation of porosity) and crystallographic texture. We systematically studied those two aspects in two aluminum titanate ceramic materials of different porosity using mercury porosimetry, gas adsorption, electron microscopy, X-ray diffraction, and X-ray refraction radiography. We found that a lower porosity content implies a larger isotropy of both the crystal texture and the porosity orientation. We also found that, analogous to cordierite, crystallites do align with their axis of negative thermal expansion along the extrusion direction. However, unlike what found for cordierite, the aluminium titanate crystallite form is such that a more pronounced (0 0 2) texture along the extrusion direction implies porosity aligned perpendicular to it. 相似文献
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In this paper, the multiple refraction phenomenon is investigated on the boundary of a scalar impedance surface (SIS) and a tensor impedance surface (TIS). When a surface wave (SW) propagates on the SIS and radiates to the boundary of the TIS, the propagation direction of it is changed and the refraction phenomenon is accrued. The method that is proposed in this paper can predict the multiple refraction for the SW. Moreover, another analytical method is introduced for designing the proposed structure which the double refraction (DR) occurs at arbitrary angles on it. Using it, a sample of the structure is designed by printed circuits in 15.2GHz and the results are verified by the full‐wave simulation and measurement. The results are shown that in the structure, DR is occurred in 2° and 22° as predicted. The proposed method can provide many applications such as design of SW power dividers based on the TISs, impedance surface based waveguides, holographic antennas, and feeding of array antennas. 相似文献