Effects of calcination temperature on phase and microstructure evolution of BaTi4O9 powders

Calcining of the mixture of BaCO₃ and TiO₂ with a ratio 1:4 at different temperatures was carried out to synthesize BaTi₄O₉ powders. Phase evolution of the samples was studied using the differential thermal analysis (DTA) and X-ray diffractometry (XRD). Both techniques confirmed that the formation of BaTi₄O₉ started around 1000 °C. The XRD peaks showed that BaTi₄O₉ was most pronounced at 1250 °C. X-ray line broadening methods were employed to study the variation of particle size and microstrain of the BaTi₄O₉ powders. The Voigt function in a single line and the pseudo-Voigt function in the variance methods were used in our case. We found that both functions resulted in the same trends, i.e., the particle size increased with the temperature with the biggest size of 180 and 160 nm, whilst the microstrain yielded the opposite trend with the lowest values of 6.2 × 10^–3 and 1.1 × 10^–3. The scanning electron microscopy (SEM) study revealed the size of the large particles formed, due to agglomeration, to be about 0.5–1.9 μm. Furthermore, it was shown that irregular shapes of BaTi₄O₉ powders necked to each other appeared at 1000 °C and grew into ellipse and rod shapes at 1250 °C. Electronic Publication     

二维加速度激光传感器的设计

以角锥棱镜作为惯性元件,利用光学干涉原理,可以实现对运动物体的二维加速度测量。本文给出了二维加速度激光传感器的设计理论和测量原理。     

Boundary-integral equation analysis of twisted internally cracked axisymmetric bimaterial elastic solids

 Green's function is obtained for the infinite bimaterial elastic solid, containing an internal circular interface crack, loaded by a unit tangential co-axial circular source. An axisymmetric direct boundary integral equation (BIE) is used for the analysis of a finite bimaterial axisymmetric body containing an internal circular interface crack and a finite homogeneous cracked cylinder, both under torsional loading. Using the proposed technique, no discretization of the crack surface is necessary. Numerical results for both examples as obtained by the proposed method are presented and discussed. Received: 29 October 2001 / Accepted: 29 May 2002     

A study on time schemes for DRBEM analysis of elastic impact wave

 The precise integration and differential quadrature methods are two new unconditionally stable numerical schemes to approximate time derivative with more than the second order accuracy. Recent studies showed that compared with the Houbolt and Newmark methods, they produced more accurate solutions with large time step for the problems where response is primarily dominated by low and intermediate frequency modes. This paper aims to investigate these time schemes in the context of the dual reciprocity BEM (DRBEM) formulation of various shock-excited scalar elastic wave problems, where high modes have important affect on traction response. The Houbolt method was widely recommended in many literatures for such DRBEM dynamic formulations. However, this study found that the damped Newmark algorithm was the most efficient and accurate for impact traction analysis in conjunction with the DRBEM. The precise integration and differential quadrature methods are shown inapplicable for such shock-excited problems due to the absence of numerical damping. On the other hand, we also found that to achieve the same order of accuracy, the differential quadrature method required much less computing effort than the precise integration method due to the use of the Bartels–Stewart algorithm solving the resulting Lyapunov matrix analogization equation. Received 6 November 2000     

The boundary contour method for two-dimensional Stokes flow and incompressible elastic materials

 A variant of the boundary element method, called the boundary contour method (BCM), offers a further reduction in dimensionality. Consequently, boundary contour analysis of two-dimensional (2-D) problems does not require any numerical integration at all. While the method has enjoyed many successful applications in linear elasticity, the above advantage has not been exploited for Stokes flow problems and incompressible media. In order to extend the BCM to these materials, this paper presents a development of the method based on the equations of Stokes flow and its 2-D kernel tensors. Potential functions are derived for quadratic boundary elements. Numerical solutions for some well-known examples are compared with the analytical ones to validate the development. Received 28 August 2001 / Accepted 15 January 2002     

贵溪冶炼厂闪速炉炉体第二次改造

介绍贵冶闪速炉炉体两次改造 ,炉体冷却元件的设置及设计特点 ,阐明了设置冷却元件必要性及使用的实际效果。     

基于有限元分析的金刚石钻头强度验算公式

在对81／2B125金刚石钻头进行有限元计算分析后，找出最大应力点在金刚石钻头冠部切削告处。通过改变各相关尺寸和结构型式，用有限元法模拟试验过程，在给定结构参数和工艺参数情况下获得多组数据。根据专业知识，参考有限元计算获取的各组数据变化特征，选出拟合较好的公式类型，再采用回归分析方法确定待定系数，最后得出工程上实用的金刚石钻头强度验算公式。用这个公式对81／2B461W和121／4B331金刚石钻头进行了强度验算，经改进设计后钻头在现场使用取得了良好的效果。     

计算机辅助设计中浓淡曲线的设计

本文介绍利用Super Frame软件进行色彩浓淡设计的原理、方法和步骤。据此原理和方法,使用C语言设计开发出了应用实例——折线浓淡分布曲线。     

Electrochemical impedance spectroscopy of a free-standing oxide film

The corrosion of low carbon steel in natural sea-water is characterized by the formation and growth of compact and thick layers composed of oxides, insoluble salts and organic materials. These layers are the result of corrosion processes induced by local environmental conditions, water oxygen supply; ionic species; bacteria and organic matter. The exchange of various species (ions, molecules, gas) between sea-water and the rust layers or the metal depends both on the kinetics of the Faradaic reactions of the entities with either the oxides or the metal, as well as on their transport properties through the different strata of the rust layers. In this work, an impedance study was carried out using the 4-electrodes cell arrangement with corrosion products picked up on steel sheet piling immersed for 25 years and analyzed as free standing membranes. This new approach is a good way to reach the specific transport and transfer properties of the oxide without being blurred by the metal influence. The physical model developed in this work was based on a transmission line, and accurately described the experimental diagrams. The electronic resistivity of the oxide layer, its porosity, the mean pore size and the reaction kinetics parameters could be determined from the fittings.