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91.
Analysis of lipid classes by solid-phase extraction and high-performance size-exclusion chromatography 总被引:1,自引:0,他引:1
Anu I. Hopia Vieno I. Piironen Pekka E. Koivistoinen Lea E. T. Hyvönen 《Journal of the American Oil Chemists' Society》1992,69(8):772-776
An improved method to analyze lipid classes of edible oils and fats by solid-phase extraction (SPE) and high-performance size-exclusion chromatography (HPSEC) is presented. A mixture of lipid standards was fractionated by the solid-phase extraction procedure (NH2 phase) into polar and nonpolar fractions; these were then submitted to analysis by HPSEC. The size-exclusion chromatographic columns were three styrene/divinylbenzene columns with pore sizes of 100 Å and 50 Å. Light-scattering was used for the detection system, and the parameters of the detector were optimized to minimize the difference between the responses of the compounds studied. With this procedure it was possible to separate the following lipid classes: triacylglycerols, diacylglycerols, monoacylglycerols and free fatty acids, sterols, sterol esters, tocopherols and carotenoids. Quantitative analysis was studied for a light-scattering detector with several lipid standards of different molecular weights and unsaturation levels. 相似文献
92.
微波萃取在食品化学中的应用 总被引:16,自引:0,他引:16
介绍了微波萃取技术在食品化学中的应用。其实质是用微波对萃取溶剂及物料加热,使溶剂的渗透率和扩散率大大提高,因此对食品营养成分或风味物质可以有铲地萃取分离。 相似文献
93.
94.
95.
R.A. Jacques J.G. Santos C. Dariva J. Vladimir Oliveira E.B. Caramo 《The Journal of Supercritical Fluids》2007,40(3):354-359
This work presents a study concerning the chemical characteristics and analytical separation process of the essential oil obtained from high-pressure carbon dioxide extraction of Ilex paraguariensis. The experiments were performed in a laboratory-scale unit in the temperature range of 20–40 °C, from 100 to 250 bar. A blend of the I. paraguariensis extracts was percolated through a preparative chromatographic column, containing silica gel, and successively eluted with 150 mL of each of the following solvents: hexane, toluene, dichloromethane, ethyl acetate, acetone and methanol. The raw extract and its fractions were analyzed by gas chromatography coupled to mass spectrometry detection (GC/MS). The fractionation procedure showed to be a good clean up technique due to the isolation of different classes of compounds in each fraction. Chromatographic analyses allowed the identification of caffeine, fatty acids and esters, phytol, squalene, Vitamin E, stigmasterol derivatives and saturated hydrocarbons. 相似文献
96.
97.
Optimal Locations of Groundwater Extractions in Coastal Aquifers 总被引:1,自引:0,他引:1
A regional water supply management model for coastal aquifers was developed. One of its outcomes is the definition of the
optimized locations for groundwater withdrawal. Such a tool permits the analysis of alternative plans for groundwater extraction
and the sustainable use of water resources in a coastal aquifer subject to saltwater intrusion. The principal components are
the evolutionary optimization and the analytical/numerical simulation models. The optimization technique looks for the best
well locations taking into consideration the economic results and the satisfaction of the societal water demand. However these
two concerns are conditioned by trying to control the saltwater intrusion, i.e., preserving the environmental equilibrium.
The simulation model uses the governing mathematical equations for groundwater movement to find the interface between freshwater
and saltwater. Because of the non-linearity in the system and the possibility of a jumping interface, a security distance
was defined. This is a controlling variable which can be set by the decision makers. The model was applied to a typical case
with interesting results. For example, diagrams showing the relationship between the location of the wells and the security
distance(s) are of importance to the managers. It was also crucial to have an understanding of the tradeoffs between groundwater
withdrawals, positions of the wells from the coast line, and the security distance. The model was also applied to a real case
in order to relate the extractions, distances and artificial recharge (not presented in this paper). 相似文献
98.
In this paper, we propose an approach that combines the unsupervised and supervised learning techniques for unconstrained
handwritten numeral recognition. This approach uses the Kohonen self-organizing neural network for data classification in
the first stage and the learning vector quantization (LVQ) model in the second stage to improve classification accuracy. The
combined architecture performs better than the Kohonen self-organizing map alone. In the proposed approach, the collection
of centroids at different phases of training plays a vital role in the performance of the recognition system. Four experiments
have been conducted and experimental results show that the collection of centroids in the middle of the training gives high
performance in terms of speed and accuracy. The systems developed also resolve the confusion between handwritten numerals. 相似文献
99.
耐高温绝缘GFRP管的真空辅助树脂传递成型工艺研究 总被引:3,自引:0,他引:3
阐述了耐高温绝缘GFRP管的成型工艺及原材料选择,并对影响成型工艺的主要因素作了理论分析及试验验证。研究表明,以TDE-85/DDS体系为为基体,以无碱无捻玻璃纤维方格布为增强材料,用VARTM工艺成型的石油勘探高性能平衡管完全满足技术要求。 相似文献
100.
铜萃取剂BK992和LIX984的性能研究 总被引:11,自引:1,他引:10
研究羟肟类铜萃取剂的结构与性能的关系。试验研究了铜萃取剂BK992和LIX984的对比萃取及混合萃取性能指标 ,试验表明BK992与LIX984的使用性能相当 ,两种铜萃取剂相互混合不影响使用性能指标。 相似文献