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71.
用直接合成法制备了不同铝硅物质的量比Al-SBA-15(β)(β=n(Al)/n(Si)=0,0.02,0.03,0.05)介孔分子筛,并采用浸渍法制备了金属负载量m=35%的CZZ/Al-SBA-15(β)负载型介孔催化剂,考察了Al/Si比对负载催化剂结构和性能的影响。采用N_2吸附-脱附、X射线衍射(XRD)、H_2程序升温还原(H_2-TPR)、CO_2吸附(CO_2-TPD)、NH3吸附(NH3-TPD)和透射电子显微镜(TEM)等手段对样品进行了表征,在固定床反应器上评价了其CO_2加氢合成甲醇的催化性能。实验结果表明,CZZ/Al-SBA-15(β)具有介孔结构,Al的引入不但增加了载体表面酸性位点,同时还提高了催化剂表面铜分散度(DCu%)和铜比表面积(SCu)以及促进了Cu~+-O-Zn活性位的形成,从而大大提高了催化剂的活性。其中CZZ/Al-SBA-15(0.03)催化剂的甲醇选择性达到26%,与不掺铝的CZZ/Al-SBA-15(0)催化剂相比,甲醇选择性提高了11%,但随着掺Al量的继续增加,酸性太强,CO_2吸附能力下降,活性反而降低。 相似文献
72.
采用电极感应熔炼气雾化(EIGA)法制备了激光3D打印用TA15钛合金粉末,研究了熔炼功率对粉末收得率、粒径分布、粉末形貌、松装密度和流动性等特征的影响。结果表明,随着感应熔炼功率增大,粉末收得率和平均粒径减小,当熔炼功率为65kW时,粉末收得率超过62%,中值粒径D_(50)小于100μm,松装密度为2.731g/cm3,流动性为22.46s/50g。对粒径50~180μm的粉末采用激光3D打印,激光直接沉积成形的TA15钛合金样品表面无宏观裂纹和气孔等缺陷,金相组织为细晶网篮组织,制备的TA15钛合金粉末具有良好的可打印性。 相似文献
73.
T. Hoang Ngan Le Chia-Chen Lin Chin-Chen Chang Hoai Bac LeAuthor vitae 《Digital Signal Processing》2011,21(6):734-745
Many secret sharing schemes for digital images have been developed in recent decades. Traditional schemes typically must deal with the problem of computational complexity, and other visual secret sharing schemes come with a higher transmission cost and storage cost; that is, each shadow size is m times as big as the original secret image. The new (2,n) secret sharing scheme for grayscale images proposed in this paper is based a combination of acceptable image quality using block truncation coding (BTC), high compression ratio discrete wavelet transform (DWT) and good subjective performance of the vector quantization (VQ) technique. Experimental results confirm that our proposed scheme not only generates a high quality reconstructed original image but also generates small, random-like grayscale shadows. 相似文献
74.
On the convective nature of the instability of a front undergoing a supercritical Turing bifurcation
Fronts are traveling waves in spatially extended systems that connect two different spatially homogeneous rest states. If the rest state behind the front undergoes a supercritical Turing instability, then the front will also destabilize. On the linear level, however, the front will be only convectively unstable since perturbations will be pushed away from the front as it propagates. In other words, perturbations may grow but they can do so only behind the front. It is of interest to show that this behavior carries over to the full nonlinear system. It has been successfully done in a case study by Ghazaryan and Sandstede [A. Ghazaryan, B. Sandstede, Nonlinear convective instability of Turing-unstable fronts near onset: a case study, SIAM J. Appl. Dyn. Syst. 6 (2007) 319–347]. In the present paper, analogous results are obtained for the same system as in Ghazaryan and Sandstede (2007), but for a different parameter regime. 相似文献
75.
Hou-Biao Li Ting-Zhu Huang Yong Zhang Xing-Ping Liu Hong Li 《Mathematics and computers in simulation》2009
In this paper, to obtain an efficient parallel algorithm to solve sparse block-tridiagonal linear systems, stair matrices are used to construct some parallel polynomial approximate inverse preconditioners. These preconditioners are suitable when the desired goal is to maximize parallelism. Moreover, some theoretical results concerning these preconditioners are presented and how to construct preconditioners effectively for any nonsingular block tridiagonal H-matrices is also described. In addition, the validity of these preconditioners is illustrated with some numerical experiments arising from the second order elliptic partial differential equations and oil reservoir simulations. 相似文献
76.
The paper forecasts conditional correlations between three classes of international financial assets, namely stock, bond and foreign exchange. Two countries are considered, namely Australia and New Zealand. Forecasting will be conducted using three multivariate GARCH models, namely the CCC model [T. Bollerslev, Modelling the coherence in short-run nominal exchange rates: a multivariate generalized ARCH model, Rev. Econ. Stat. 72 (1990) 498–505], VARMA-GARCH model [S. Ling, M. McAleer, Asymptotic theory for a vector ARMA-GARCH model, Econometric Theory 19 (2003) 280–310], and VARMA-AGARCH model [M. McAleer, S. Hoti, F. Chan, Structure and asymptotic theory for multivariate asymmetric volatility, Econometric Rev., in press]. A rolling window technique is used to forecast 1-day ahead conditional correlations. To evaluate the impact of model specification on conditional correlations forecasts, this paper calculates and compares the correlations between conditional correlations forecasts resulted from the three models. The paper finds the evidence of volatility spillovers and asymmetric effect of negative and positive shock on the conditional variance in most pairs of series. However, it suggests that incorporating volatility spillovers and asymmetric do not contribute to better conditional correlations forecasts. 相似文献
77.
78.
Xiaojun Ban 《International journal of systems science》2016,47(15):3646-3655
In this paper, the control problem for a class of linear parameter varying (LPV) plant subject to actuator saturation is investigated. For the saturated LPV plant depending on the scheduling parameters in linear fractional transformation (LFT) fashion, a gain-scheduled output feedback controller in the LFT form is designed to guarantee the stability of the closed-loop LPV system and provide optimised disturbance/error attenuation performance. By using the congruent transformation, the synthesis condition is formulated as a convex optimisation problem in terms of a finite number of LMIs for which efficient optimisation techniques are available. The nonlinear inverted pendulum problem is employed to demonstrate the effectiveness of the proposed approach. Moreover, the comparison between our LPV saturated approach with an existing linear saturated method reveals the advantage of the LPV controller when handling nonlinear plants. 相似文献
79.
设计了一款模拟昆虫飞行方式的微小型扑翼机,仿照蜻蜓的两翼,直升机式尾翼,以STC15F2K60S2为主控芯片,应用主流无线模块来完成实现遥控仿生扑翼机的设计与制作,经过实际测试能够满足飞行要求. 相似文献
80.
Jianer Chen Qilong FengYang Liu Songjian LuJianxin Wang 《Theoretical computer science》2011,412(23):2503-2512
Based on the method of (n,k)-universal sets, we present a deterministic parameterized algorithm for the weighted rd-matching problem with time complexity O∗(4(r−1)k+o(k)), improving the previous best upper bound O∗(4rk+o(k)). In particular, the algorithm applied to the unweighted 3d-matching problem results in a deterministic algorithm with time O∗(16k+o(k)), improving the previous best result O∗(21.26k). For the weighted r-set packing problem, we present a deterministic parameterized algorithm with time complexity O∗(2(2r−1)k+o(k)), improving the previous best result O∗(22rk+o(k)). The algorithm, when applied to the unweighted 3-set packing problem, has running time O∗(32k+o(k)), improving the previous best result O∗(43.62k+o(k)). Moreover, for the weighted r-set packing and weighted rd-matching problems, we give a kernel of size O(kr), which is the first kernelization algorithm for the problems on weighted versions. 相似文献