金属基BSiN薄膜结合力测试及AES分析

我们采用低温等离子体ＣＶＤ技术在金属表面成功地淀积了ＢＮ－ＳｉＮ复合陶瓷薄膜。并用ＢＦ－１型薄膜附着力测定仪测试了它的结合力，以及用俄歇电子能谱（ＡＥＳ）分析其成键状态。结果表明：这种薄膜与基体之间具有较强的Ｆｅ－Ｂ键结合力。     

壳聚糖固定化单宁酸酶的特性研究

研究了以壳聚糖为载体交联-吸附单宁酸酶后的化学特性。结果表明：固定化单宁酸酶（简称“ITA”）的最适反应pH为3.0,原酶（简称“TA”）为5．5;ITA最适反应温度为50℃,TA为40℃;ITA的Km（app）为1．3845×10(-1)mol／L,TA为6．7500×10(-5)mol/L;ITA在pH3．0～8．0的范围内残存酶活大于60％,ITA在pH3．0～6.0范围内残存酶活大于60％;ITA在80℃的水浴中保温1h,酶活力仍未见下降,而TA在60℃水浴中保温30min酶已失活;ITA和TA在4℃和30℃的条件下,贮藏20d后,ITA的残存活性大于40％,TA的残存活性小于20％。     

点火药粒度变化对产品性能的影响研究

为研究点火药粒度变化对产品性能的影响,采用扫描电镜与激光衍射粒度仪测量了原料粒径,将4种不同粒度的Si粉分别与3.59μm的Pb3O4混合,制得无气体延期点火药Si-Pb3O4,进行了产品发火感度试验和作用时间试验.试验结果表明,随着Si粉粒度的减小,产品发火感度升高,发火能量降低;产品作用时间缩短.并从理论上对试验结果进行了分析.     

影响挤压小吃食品品质的因素

试验结果表明,影响挤压小吃食品品质的因素主要包括：原料中水分含量、直链淀含量、蛋白质及脂肪含量、膨化机的挤出温度等。     

An adaptive measurement scheme based on compressed sensing for wideband spectrum detection in cognitive WSN

An Adaptive Measurement Scheme (AMS) is investigated with Compressed Sensing (CS) theory in Cognitive Wireless Sensor Network (C-WSN). Local sensing information is collected via energy detection with Analog-to-Information Converter (AIC) at massive cognitive sensors, and sparse representation is considered with the exploration of spatial temporal correlation structure of detected signals. Adaptive measurement matrix is designed in AMS, which is based on maximum energy subset selection. Energy subset is calculated with sparse transformation of sensing information, and maximum energy subset is selected as the row vector of adaptive measurement matrix. In addition, the measurement matrix is constructed by orthogonalization of those selected row vectors, which also satisfies the Restricted Isometry Property (RIP) in CS theory. Orthogonal Matching Pursuit (OMP) reconstruction algorithm is implemented at sink node to recover original information. Simulation results are performed with the comparison of Random Measurement Scheme (RMS). It is revealed that, signal reconstruction effect based on AMS is superior to conventional RMS Gaussian measurement. Moreover, AMS has better detection performance than RMS at lower compression rate region, and it is suitable for large-scale C-WSN wideband spectrum sensing.     

Ferroelectric Materials: Probing Local and Global Ferroelectric Phase Stability and Polarization Switching in Ordered Macroporous PZT (Adv. Funct. Mater. 5/2011)

We describe the characterization, ferroelectric phase stability and polarization switching in strain‐free assemblies of PbZr_0.3Ti_0.7O₃ (PZT) nanostructures. The 3‐dimensionally ordered macroporous structures present uniquely large areas and volumes of PZT where the microstructure is spatially modulated and the composition is homogeneous. Variable temperature powder X‐ray diffraction (XRD) studies show that the global structure is crystalline and tetragonal at room temperature and undergoes a reversible tetragonal to cubic phase transition on heating/cooling. The measured phase‐transition temperature is 50–60 °C lower than bulk PZT of the same composition. The local ferroelectric properties were assessed using piezoresponse force spectroscopy that reveal an enhanced piezoresponse from the nanostructured films and demonstrate that the switching polarization can be spatially mapped across these structures. An enhanced piezoresponse is observed in the nanostructured films which we attribute to the formation of strain free films, thus for the first time we are able to assess the effects of crystallite‐size independently of internal stress. Corresponding polarization distributions have been calculated for the bulk and nanostructured materials using a direct variational method and Landau‐Ginzburg‐Devonshire (LGD) theory. By correlating local and global characterization techniques we have for the first time unambiguously demonstrated the formation of tetragonal and ferroelectric PZT in large volume nanostructured architectures. With the wide range of materials available that can be formed into such controlled architectures we conclude that this study opens a pathway for the effective studies of nanoscale ferroelectrics in uniquely large volumes.     

自主知识产权产品LIP封装

为解决QFN成本较高的问题和进一步提高产品可靠性,华天科技突破了传统思想的束缚,在产品结构的设计上进行了创新。引脚在封装本体内式封装(LIP:Lead In Package)是一种新型的封装形式,它是针对目前QFN(Quad Flat No-lead)在封装高成本问题而重新选择的设计方案。     

基于小波域的水印最佳嵌入位置的研究

本文通过分析小波变换的系数分布特点,结合人眼视觉特性和带载图像抗攻击能力,论证了小波变换第二层的代表水平细节的HL2和代表垂直细节的LH2N水印嵌入的相对最佳嵌入位置。实验结果表明,在此位置嵌入水印,可以保证水印的隐蔽性和稳健性。     

一种保持直方图特性的JPEG图像掩密算法

传统的JPEG图像掩密算法往往因为改变了载体图像的DCT系数直方图而不能抵抗各种基于直方图的攻击,或者为了矫正直方图而降低了隐藏容量,该文提出一种新的保持直方图特性的算法。该算法在嵌入秘密消息时,动态建立Adjust_info表记录系数直方图被改变的情况,然后根据该表调整系数的变化方向,这样不但可以补偿直方图的改变,而且并不降低隐藏容量。对多幅图像的实验表明,该算法不但能够达到13%的高隐藏容量(压缩因子为75),而且掩密后图像总体DCT系数直方图的平均失真率为0.81%。由改进算法掩密后图像低频DCT系数直方图的最大失真率为3.83%,平均失真率只有1.98%,仅对直方图做了微小的改变,因此可以有效抵御各种直方图攻击,从而为安全掩密提供了可靠保证。     

固定电子分立元器件用胶粘剂E—4X的研制

介绍了一种不同于灌封材料，具有触变性，粘接性能优良，使用方便的固定电子分立元器件用胶粘剂Ｅ－４Ｘ。与国外同类产品Ｅｐ－４３３ｘ胶粘剂对比，其综合性能优于Ｅｐ－４３３胶粘剂。