高能球磨LaNi5-34%(质量分数)Mg的相组成与热稳定性能

采用X射线衍射仪(XRD)、扫描电子显微镜(SEM)、差热分析(DTA)等方法研究了高能球磨及热处理等对新型合金LaNi5-34％(质量分数)Mg的相组成、形貌及热稳定性能等的影响。结果表明：经100r／min球磨100h及190r／min球磨100h后,样品由La、Mg、Ni等非晶。微量的晶体Ni和MgNi2相组成,所得粉末的形状大多为规则的球形或近球形,其颗粒直径范围为0．05～33．0μm。球磨样品具有较好的室温活化特性，其最大电化学放电容量为460mAh／g。该样品经763K保温35d后，得到热稳定性较好的具有纳米尺度的MgNi2、Mg2Ni、Mg2NiLa三相组织，其平均晶粒直径为21.3nm。     

诺砂的特性及综合利用

在研究诺砂特性的基础上论述了诺砂综合利用的各种途径，给出了实际利用中应注意的问题．     

Growth of aluminum nitride thin films prepared by plasma-enhanced atomic layer deposition

Aluminum nitride (AlN) thin films were deposited by atomic layer deposition from aluminum chloride (AlCl₃) and an ammonia/hydrogen plasma. The most important role of the ammonia/hydrogen plasma was to act as a reducing agent to extract Cl from AlCl₃, and to form AlN subsequently. The growth rate was saturated at ∼0.042 nm/cycle, and the thickness was proportional to the number of reaction cycles. Repeating this reaction cycle led to precisely controlled growth. The film properties were analyzed using Auger electron spectroscopy, X-ray photoelectron spectroscopy, Rutherford backscattering spectroscopy and time-of-flight elastic recoil detection analysis. The concentration of chlorine and hydrogen impurities was 0.23 and 2.01 at.%, respectively. AlN films showed good anti-oxidation properties when O₂ was annealed at 650 °C for 30 min.     

柴油机喷雾特性的传统及现代测试方法

介绍了近现代内燃机工作者为了研究柴油机喷雾特性所应用和研究开发的一系列测试柴油机喷雾场的方法及其工作原理，并比较了各种方法的优越性及局限性．最后提出了一个研究出一种能实现瞬态喷雾全场雾滴尺寸及速度同时测量的在线实时测量新技术必要性的观点。     

Characterization of Clay Particle Surfaces for Contaminant Sorption in Soil Barriers Using Flow Microcalorimetry

Clays such as kaolinite and bentonite are widely used in various industries as sorbents. The sorptive characteristics of clays are exploited when they are used in contaminant barrier systems. To use clays effectively, their surface characteristics need to be known; especially, when they are used for contaminant sorption. Available surface area of clay minerals and the characteristics that depend on it are very sensitive to environmental changes such as those that can be induced by changes in the composition of pore fluid. Flow microcalorimetry with a down-stream concentration was used to determine the heats and amounts of adsorption of acids and bases on the clays. Test results presented herein revealed that both kaolinite and bentonite exhibit significantly different adsorption isotherms and heat of wetting under high pH and low pH conditions. Kaolinite has the capacity to adsorb both acidic and basic molecules almost equally. However, it has a tendency to adsorb more base than acid because of its stronger complexation capacity with acids than with bases. On the other hand, bentonite has a tendency to adsorb more acidic than basic molecules per gram. These results also indicate that both kaolinite and bentonite have different heats of wetting characteristics. As the concentrations of the acids and bases increase, the heat of wetting of kaolinite decreases while that of bentonite increases.     

面包车尾部造型对其气动特性的影响

为了研究面包车气动特性的影响因素,以国产某小客车简化模型为研究对象,在对基础模型进行试验验证的基础上,通过数值模拟的方法,计算后风窗角度、背部角度和底部上翘角度改变以后面包车的气动阻力和升力,得到其变化规律,并把各种角度相互组合,得出最佳的尾部造型.模拟结果表明:上述3种因素对面包车的气动特性均有很大的影响,在设计过程...     

龙南稀土矿区周边水体污染特征及风险评价

为研究龙南稀土矿区地表水和地下水污染物迁移规律及污染成因机制,开展了矿区周边地表水、地下水水质现状监测工作,对研究区周边地表水、地下水中pH、硫酸盐、硝酸盐、亚硝酸盐、氨氮浓度进行分析测定,运用改进内梅罗综合污染指数法和健康风险评价模型对水体污染程度及不同年龄段人群健康风险进行评估。结果表明,地表水料坑处的综合污染指数最高,达到54.19,属于严重污染程度;关西翰岗桥处综合污染指数最低,仅为2.119,属于较清洁程度;料坑、黄沙河和临塘一处理站下游的综合污染指数均达到严重污染程度;地下水采样点综合污染指数均达标,水质清洁。健康风险评价结果表明,研究区地表水及地下水中的硝酸盐对人体造成的健康风险较大,亚硝酸盐与氨氮次之;经非致癌健康风险计算,饮用地下水和地表水对不同年龄人群的影响程度为幼儿＞青年＞成人,因此应对龙南稀土矿区周边0~6岁幼儿用水安全给予更多关注。     

金峰铜业有限公司双侧吹熔池熔炼工艺试生产总结

介绍了金峰铜业有限公司双侧吹熔池熔炼工艺试生产情况,列举了主要的生产数据和技术经济指标,总结了工艺的特点。     

Study on characteristics of Ni-W-B composites containing CeO2 nano-particles prepared by pulse electrodeposition

Ni-W-B composites containing CeO2 nano-particles on the surface of 45 steel were prepared by pulse electrodeposition,and the in-fluence of pulse frequency,pulse duty circle and heat treatment temperature on the structures and properties were investigated.The results in-dicated that the pulse co-deposition of Ni,W,B and CeO2 nano-particles led to Ni-W-B/CeO2 composites possessing higher microhardness and better wear resistance when heat-treated at 400 oC for 1 h.The microhardness of 636 HV and the deposition rate of 0.0281 mm/h of the as-deposited alloy were the highest at pulse frequency of 1000 Hz,pulse duty circle of 10% and pulse average current density of 10 A/dm2.The composites were mainly in the amorphous state and were partially crystallized as-deposited,and the crystallization trend was strength-ened when heat-treated at 400 oC.Decreasing pulse duty cycle from 75% to 10% was favorable to the refinement in grain structures and im-provement of microstructures.The crystal sizes of the composites were smaller by means of pulse electrodeposition.