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31.
32.
Zinc Coated Steel/Epoxy Adhesive Systems: Investigation of the Interfacial Zone by FTIR Spectroscopy
The present study takes advantage of the ability of Fourier Transform Infrared Spectroscopy (FTIR) for the analysis of ultrathin organic films on metals. FTIR in the reflection mode (IRRAS) is used in order to study the interaction of ultrathin films of dicyandiamide (hardener of most one-pack epoxy resins) with various substrates, model ones such as gold or zinc and industrial ones such as steel and zinc-coated steels.
Pure zinc surfaces and, to a lesser extent, zinc-coated steels are shown to react with dicyandiamide after heating at 180°C, as evidenced by the frequency shift of the absorption band (at about 2200 cm-1) characteristic for nitrile groups. As real systems consist of thick layers of a fully formulated adhesive cured onto a metallic substrate, the direct investigation of such a buried interphase is no longer possible by FTIR and by most of the known spectroscopies. Some mechanically tested specimens are then analysed, after failure, by FTIR microspectrometry. The spectra obtained, corresponding to the fracture initiation zone which is about 100 μm in diameter, advocate for the presence of an ultrathin layer of modified polymer still covering the substrate. 相似文献
Pure zinc surfaces and, to a lesser extent, zinc-coated steels are shown to react with dicyandiamide after heating at 180°C, as evidenced by the frequency shift of the absorption band (at about 2200 cm-1) characteristic for nitrile groups. As real systems consist of thick layers of a fully formulated adhesive cured onto a metallic substrate, the direct investigation of such a buried interphase is no longer possible by FTIR and by most of the known spectroscopies. Some mechanically tested specimens are then analysed, after failure, by FTIR microspectrometry. The spectra obtained, corresponding to the fracture initiation zone which is about 100 μm in diameter, advocate for the presence of an ultrathin layer of modified polymer still covering the substrate. 相似文献
33.
An alternative test method to the traditional 180° “T” peel test has been developed for the measurement of interlaminar bonding in three-ply (polyester/aluminium/polypropylene) flexible-packaging, laminate materials. The new test is thought to involve mixed mode I (opening) and mode II (shearing) failure, and takes into account the yielding of the polypropylene layer during testing. The method allows more direct comparisons between materials to be made, and allows the measurement of strong bonds, where a peel test would result in yield or fracture of the substrate arms before debonding. 相似文献
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35.
高强度快干变性淀粉粘合剂的研究及在纸制品包装中的应用 总被引:2,自引:0,他引:2
本文介绍了高强度快干变性淀粉的制备原理和工艺,以及用该变性淀粉调配瓦楞纸板用粘合剂的方法和应用情况。讨论了变性淀粉粘合剂的初粘力,干燥速度等并与普通淀粉粘合剂作了比较。 相似文献
36.
介绍一种新型酚醛--丁腈并用耐高温高强度单组分浆状结构胶粘剂和组成比例以及固化条件对粘接强度的影响,该胶适用于粘接刹车制动蹄和飞机轻金属结构等。 相似文献
37.
38.
快固化淀粉粘合剂的研究 总被引:3,自引:0,他引:3
介绍了快固化玉米淀粉粘合剂的制备工艺,对制备参数进行了优化,可使粘合剂的初粘速度和干燥速度显著提高。 相似文献
39.
聚醋酸乙烯乳液缩醛化的改性研究 总被引:4,自引:1,他引:4
本文介绍了为提高聚醋酸乙烯乳液稳定性、耐水性和防冻性而进行缩醛化改性的原理,并确定了最佳工艺条件即甲醛与聚乙烯醇的配比为0.45~0.50。 相似文献
40.
This paper presents an experimental investigation into various aspects of epoxy-bonded polymethylmethacrylate (PMMA) and PMMA-to-aluminium joints. The effects of adhesive thickness, overlap area, surface roughness, and environmental exposure on the joint strength were studied. Results indicated that the joint strength was not directly proportional to the overlap area, while sanding had a positive effect on the joint strength. A negative effect was observed when adhesive thickness was increased. The fatigue behaviour of adhesively-bonded joints under dynamic loading was found to be independent of frequency, for the range of values tested; however, it was dependent on the test temperature with greater reduction in fatigue life observed in PMMA-to-aluminium joints at higher temperature. Empirical equations from which the fatigue life of joints can be predicted were obtained by regression analysis. Intermittent fatigue testing of the joints was also performed. The epoxy adhesive tested proved to be a satisfactory choice for outdoor exposure. The rate of degradation of the adhesive was slow with the adherend itself degrading at a faster rate than the adhesive or the bondline. 相似文献